PYRIDIN-3-YLMETHYL-HYDRAZINE
- Product Name
- PYRIDIN-3-YLMETHYL-HYDRAZINE
- CAS No.
- 7112-38-1
- Chemical Name
- PYRIDIN-3-YLMETHYL-HYDRAZINE
- Synonyms
- 3-(hydrazinylMethyl)pyridine;PYRIDIN-3-YLMETHYL-HYDRAZINE;Pyridine,3-(hydrazinylmethyl)-;1-(pyridin-3-ylmethyl)hydrazine;PYRIDIN-3-YLMETHYL-HYDRAZINE HCL;Pyridin-3-ylmethyl-hydrazine ,98%
- CBNumber
- CB3698053
- Molecular Formula
- C6H9N3
- Formula Weight
- 123.16
- MOL File
- 7112-38-1.mol
PYRIDIN-3-YLMETHYL-HYDRAZINE Property
- Boiling point:
- 310℃
- Density
- 1.104
- Flash point:
- 141℃
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CHM0102252
- Product name
- 3-(HYDRAZINOMETHYL)PYRIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $465.15
- Updated
- 2021/12/16
- Product number
- 1030AC
- Product name
- 3-(Hydrazinylmethyl)pyridine
- Packaging
- 5g
- Price
- $681
- Updated
- 2021/12/16
- Product number
- CHM0102252
- Product name
- 3-(HYDRAZINOMETHYL)PYRIDINE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1473.14
- Updated
- 2021/12/16
- Product number
- CM175514
- Product name
- 1-((Pyridin-3-yl)methyl)hydrazine
- Purity
- 97%
- Packaging
- 10g
- Price
- $757
- Updated
- 2021/12/16
- Product number
- 7112381
- Product name
- 3-(Hydrazinylmethyl)pyridine
- Packaging
- 5g
- Price
- $815.36
- Updated
- 2021/12/16
PYRIDIN-3-YLMETHYL-HYDRAZINE Chemical Properties,Usage,Production
Synthesis
500-22-1
7112-38-1
General procedure for the synthesis of pyridine-3-methylidenehydrazine (1-(3-pyridyl)methylhydrazine) from 3-pyridinecarboxaldehyde: Hydrazine (1.05 mL, 46.7 mmol) was slowly added to a solution of methanol (100 mL) containing 3-pyridinecarboxaldehyde (5 g, 46.7 mmol). The reaction mixture was stirred continuously for 1 hour at room temperature. Subsequently, the air in the reaction system was replaced with nitrogen and 10% Pd/C catalyst (200 mg) was added. The nitrogen was again replaced with hydrogen and the reaction mixture was stirred overnight at room temperature under hydrogen atmosphere. Upon completion of the reaction, the solid catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give the crude product pyridine-3-methylenehydrazine (Example 85A). This crude product can be used directly in the subsequent reaction without further purification. Yield: 5.2 g (91% yield). Mass spectrometry (DCI) analysis result: m/z 124 ([M+H]+).
References
[1] Patent: WO2007/95628, 2007, A1. Location in patent: Page/Page column 69-70
PYRIDIN-3-YLMETHYL-HYDRAZINE Preparation Products And Raw materials
Raw materials
Preparation Products
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