ChemicalBook > CAS DataBase List > 2-Methyl-4-phenyl-1H-imidazole

2-Methyl-4-phenyl-1H-imidazole

Product Name
2-Methyl-4-phenyl-1H-imidazole
CAS No.
13739-48-5
Chemical Name
2-Methyl-4-phenyl-1H-imidazole
Synonyms
2-Methyl-4-phenylimidazole;2-Methyl-5-phenyliMidazole;4-(2-Methyl Phenyl)IMidazole;2-METHYL-4-PHENYL-1H-IMIDAZOLE;2-methyl-4-phenyl-3H-imidazole;2-methyl-5-phenyl-1H-imidazole;1H-Imidazole, 2-methyl-5-phenyl-;1H-imidazole, 2-methyl-4-phenyl-;2-methyl-4-phenyl-1H-imidazole(SALTDATA: FREE)
CBNumber
CB3755312
Molecular Formula
C10H10N2
Formula Weight
158.2
MOL File
13739-48-5.mol
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2-Methyl-4-phenyl-1H-imidazole Property

Melting point:
159-160.5 °C
Boiling point:
396.2±11.0 °C(Predicted)
Density 
1.109±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
14.13±0.10(Predicted)
Appearance
White to light yellow Solid
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Safety

Risk Statements 
36
Safety Statements 
26
HazardClass 
IRRITANT
HS Code 
2933299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B399925
Product name
2-Methyl-4-phenyl-1H-imidazole
Packaging
100mg
Price
$65
Updated
2021/12/16
TRC
Product number
B399925
Product name
2-Methyl-4-phenyl-1H-imidazole
Packaging
500mg
Price
$220
Updated
2021/12/16
Apolloscientific
Product number
OR942345
Product name
2-Methyl-4-phenyl-1H-imidazole
Purity
95%
Packaging
1g
Price
$235
Updated
2021/12/16
Matrix Scientific
Product number
061241
Product name
2-Methyl-4-phenyl-1H-imidazole
Packaging
500mg
Price
$315
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-1-JA
Product name
2-Methyl-4-phenyl-1H-imidazole
Purity
95%
Packaging
1g
Price
$376
Updated
2021/12/16
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2-Methyl-4-phenyl-1H-imidazole Chemical Properties,Usage,Production

Synthesis

451-50-3

13739-48-5

Using stilbene (150 mL) as solvent, benzoylacetamide (10.15 mmol), ammonium acetate (64.86 mmol) and acetic acid (166.6 mmol) were added and the mixture was heated to reflux and azeotropized to remove the water, and the reaction lasted for 6 hours. Upon completion of the reaction, the reaction mixture was cooled to room temperature and washed with 25 mL of water followed by distillation to remove the solvent to give the crude product. The crude product was purified by column chromatography using silica gel (60-120 mesh) as stationary phase and a solvent mixture of dichloromethane and methanol (100:5, v/v) as mobile phase to give the final target compound 2-methyl-4-phenyl-1H-imidazole.

References

[1] Patent: WO2009/137081, 2009, A2. Location in patent: Page/Page column 49-51

2-Methyl-4-phenyl-1H-imidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Methyl-4-phenyl-1H-imidazole Suppliers

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13739-48-5, 2-Methyl-4-phenyl-1H-imidazoleRelated Search:


  • 2-METHYL-4-PHENYL-1H-IMIDAZOLE
  • 1H-imidazole, 2-methyl-4-phenyl-
  • 2-methyl-4-phenyl-1H-imidazole(SALTDATA: FREE)
  • 4-(2-Methyl Phenyl)IMidazole
  • 2-Methyl-5-phenyliMidazole
  • 2-methyl-5-phenyl-1H-imidazole
  • 2-methyl-4-phenyl-3H-imidazole
  • 2-Methyl-4-phenylimidazole
  • 1H-Imidazole, 2-methyl-5-phenyl-
  • 13739-48-5
  • Imidazoles & Benzimidazoles