DIBUTYLCARBAMYL CHLORIDE
- Product Name
- DIBUTYLCARBAMYL CHLORIDE
- CAS No.
- 13358-73-1
- Chemical Name
- DIBUTYLCARBAMYL CHLORIDE
- Synonyms
- tl459;Brn 2040828;Einecs 236-410-3;DIBUTYLCARBAMYL CHLORIDE;dibutylcarbamoylchloride;dibutyl-carbamoylchlorid;dibutylcarbamic chloride;1,6-dibutyl-carbamicchlorid;Carbamoyl chloride, dibutyl-;Dibutylcarbamic acid chloride
- CBNumber
- CB3783443
- Molecular Formula
- C9H18ClNO
- Formula Weight
- 191.7
- MOL File
- 13358-73-1.mol
DIBUTYLCARBAMYL CHLORIDE Property
- Boiling point:
- 257-260 °C(lit.)
- Density
- 0.985 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.456(lit.)
- Flash point:
- 110 °C
- pka
- -1.85±0.70(Predicted)
Safety
- Hazard Codes
- C
- Risk Statements
- 34
- Safety Statements
- 26-36/37/39-45
- RIDADR
- UN 3265 8/PG 3
- WGK Germany
- 3
- RTECS
- FD2230000
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- FD125484
- Product name
- Dibutylcarbamic chloride
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- FD125484
- Product name
- Dibutylcarbamic chloride
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 065822
- Product name
- Dibutylcarbamic chloride
- Packaging
- 500mg
- Price
- $237
- Updated
- 2021/12/16
- Product number
- FD125484
- Product name
- Dibutylcarbamic chloride
- Packaging
- 1g
- Price
- $255
- Updated
- 2021/12/16
- Product number
- FD125484
- Product name
- Dibutylcarbamic chloride
- Packaging
- 2g
- Price
- $434
- Updated
- 2021/12/16
DIBUTYLCARBAMYL CHLORIDE Chemical Properties,Usage,Production
Uses
It is reported that Dibutylcarbamoyl Chloride is used as a reagent for the preparation of 7-azaindole-1,3-dicarboxamide hydroxyethylamine which exhibited potent BACE-1 enzyme inhibition. Also it is used for the preparation of copper salicylaldehyde semicarbazone complex which showed cytotoxicity in human cancer cells.
Preparation
In a 100 mL roundbottomed flask were placed dibutylamine (6.45 g, 0.05 mol), pyridine (4.0 g, 0.05 mol), N-cyclohexyl-N0,N0,N00,N00-tetraethylguanidine (12.7 g, 0.05 mol), and toluene (40 mL). The resulting solution was cooled to 10 °C using an ice/salt bath and carbon dioxide was bubbled into the cooled solution for 30 min. After this period of time, the pre-formed carbamate solution was added in a single portion via a cannula to a cooled ( 10 °C) solution of thionyl chloride (6 g, 0.05 mol) in toluene (40 mL). The reaction mixture was stirred at 10 °C for 45 min. It was then poured into 0.1 m aq. HCl (100 mL), giving rise to two layers. The organic layer was separated, dried over anhydrous Mg2SO4, filtered, and the solvent was removed in vacuo. The residue was distilled in vacuo (1 mmHg) at 95–98 °C to give 7.62 g (79%) of N,N-dibutyl carbamoyl chloride.
DIBUTYLCARBAMYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from DIBUTYLCARBAMYL CHLORIDE manufacturers
- Product
- Dibutylcarbamyl chloride 13358-73-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2020-01-07