ChemicalBook > CAS DataBase List > 2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)

2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)

Product Name
2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)
CAS No.
99420-75-4
Chemical Name
2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)
Synonyms
5-Methylpyrimidine-2-carboxylic acid;5-Methylpyrimidine-2-carboxylicaci;5-methyl-2-pyrimidinecarboxylicacid;2-PyriMidinecarboxylic acid, 5-Methyl-;2-Pyrimidinecarboxylicacid,5-bethyl-(6CI,9CI);5-methylpyrimidine-2-carboxylic acid - [M11475];2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI);2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) ISO 9001:2015 REACH
CBNumber
CB41081433
Molecular Formula
C6H6N2O2
Formula Weight
138.12
MOL File
99420-75-4.mol
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2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) Property

Melting point:
157-161℃
Boiling point:
363℃
Density 
1.319
Flash point:
173℃
storage temp. 
2-8°C
pka
3.25±0.10(Predicted)
Appearance
White to off-white Solid
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Safety

Safety Statements 
24/25
HS Code 
29335990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
M341120
Product name
5-Methylpyrimidine-2-carboxylicAcid
Packaging
500mg
Price
$330
Updated
2021/12/16
AK Scientific
Product number
Z5426
Product name
5-Methylpyrimidine-2-carboxylicacid
Packaging
250mg
Price
$145
Updated
2021/12/16
Apolloscientific
Product number
OR54460
Product name
5-Methylpyrimidine-2-carboxylicacid
Packaging
250mg
Price
$182
Updated
2021/12/16
SynQuest Laboratories
Product number
4H58-1-QZ
Product name
5-Methylpyrimidine-2-carboxylic acid
Purity
97.0%
Packaging
250mg
Price
$290
Updated
2021/12/16
Apolloscientific
Product number
OR54460
Product name
5-Methylpyrimidine-2-carboxylicacid
Packaging
1g
Price
$435
Updated
2021/12/16
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2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) Chemical Properties,Usage,Production

Synthesis

38275-54-6

99420-75-4

General procedure for the synthesis of 5-methylpyrimidine-2-carboxylic acid from 5-methylpyrimidine-2-carbonitrile: To a solution of 5-methylpyrimidine-2-carbonitrile (2 g, 16.8 mmol, 1.00 equiv) in water (30 mL) was added sodium hydroxide (1.01 g, 25.2 mmol, 1.50 equiv). The reaction mixture was stirred at 50 °C for 3 hours. Upon completion of the reaction, the pH of the solution was adjusted to 4-5 with 3 M hydrochloric acid. the reaction mixture was concentrated under reduced pressure to remove water. The residue was diluted with methanol (50 mL) and the solid product was collected by filtration. The filtrate was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give 5-methylpyrimidine-2-carboxylic acid (2 g, 86.2% yield) as a white solid.LC-MS: m/z = 139 [M + H]+.

References

[1] Patent: US2018/79742, 2018, A1. Location in patent: Paragraph 0418; 019

2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) Suppliers

J & K SCIENTIFIC LTD.
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18210857532; 18210857532
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jkinfo@jkchemical.com
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China
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PharmaBlock Sciences (Nanjing),Inc.
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China
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Hangzhou Sage Chemical Co., Ltd.
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NovoChemy Ltd.
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Germany
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Nanjing Norris-Pharm Technology Co., Ltd
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021-50323701
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China
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Chengdu AstaTech Trading Co., Ltd./AstaTech (Chengdu) Pharma. Co., Ltd.
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Bide Pharmatech Ltd.
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ShangHai AmK Pharmaceutical Technology Co., Ltd.
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View Lastest Price from 2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) manufacturers

Dideu Industries Group Limited
Product
2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) 99420-75-4
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-07
Career Henan Chemical Co
Product
6-CHLORO-3-INDOXYL-BETA-D-GLUCOPYRANOSIDE TRIHYDRATE 99420-75-4
Price
US $1.00/g
Min. Order
1g
Purity
97%
Supply Ability
100kg
Release date
2020-01-09

99420-75-4, 2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)Related Search:


  • 2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI)
  • 5-Methylpyrimidine-2-carboxylic acid
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  • 2-PyriMidinecarboxylic acid, 5-Methyl-
  • 2-Pyrimidinecarboxylicacid,5-bethyl-(6CI,9CI)
  • 5-Methylpyrimidine-2-carboxylicaci
  • 2-Pyrimidinecarboxylic acid, 5-methyl- (6CI,9CI) ISO 9001:2015 REACH
  • 5-methylpyrimidine-2-carboxylic acid - [M11475]
  • 99420-75-4
  • pharmacetical
  • PYRIMIDINE