2-Chloro-5-iodobenzotrifluoride
- Product Name
- 2-Chloro-5-iodobenzotrifluoride
- CAS No.
- 260355-20-2
- Chemical Name
- 2-Chloro-5-iodobenzotrifluoride
- Synonyms
- 1-chloro-4-iodo-2-(trifluoromethyl)benzene;2-Chloro-5-iodobenzotrifluoride;5-iodo-2-chlorobenzotrifluoride;2-Chloro-5-iodobenzotrifluoride >2-chloro-5-iodo-trifluoromethylbenzene;Benzene, 1-chloro-4-iodo-2-(trifluoromethyl)-
- CBNumber
- CB41216132
- Molecular Formula
- C7H3ClF3I
- Formula Weight
- 306.45
- MOL File
- 260355-20-2.mol
2-Chloro-5-iodobenzotrifluoride Property
- Melting point:
- 28 °C
- Boiling point:
- 235 ºC
- Density
- 1.952
- Flash point:
- 28 °C
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to lump
- color
- White to Light yellow
- InChIKey
- MCIFWVOVVPVBRJ-UHFFFAOYSA-N
Safety
- HS Code
- 2903998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- C2196
- Product name
- 2-Chloro-5-iodobenzotrifluoride
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $28
- Updated
- 2025/07/31
- Product number
- C2196
- Product name
- 2-Chloro-5-iodobenzotrifluoride
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $98
- Updated
- 2025/07/31
- Product number
- C428750
- Product name
- 2-Chloro-5-iodobenzotrifluoride
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- B378
- Product name
- 2-Chloro-5-iodobenzotrifluoride
- Packaging
- 25g
- Price
- $67
- Updated
- 2021/12/16
- Product number
- 083752
- Product name
- 2-Chloro-5-iodobenzotrifluoride
- Purity
- 97%
- Packaging
- 1g
- Price
- $83
- Updated
- 2021/12/16
2-Chloro-5-iodobenzotrifluoride Chemical Properties,Usage,Production
Chemical Properties
liquid
Synthesis
1132942-88-1
260355-20-2
General procedure for the synthesis of 2-chloro-5-iodobenzotrifluoride from 2-trifluoromethyl-4-iodophenol: 4-iodo-2-trifluoromethylphenol (10 mmol) obtained in 1.1 was dissolved in 20 mL of N,N-dimethylformamide (DMF). Subsequently, phosphorous trichloride (10.5 mmol) was added, and the reaction system was placed in a microwave reactor, heated to 130 °C, and kept for 1 hour. After the reaction was completed, the system was cooled to room temperature, 30 mL of water was added and stirred for 10 minutes. The reaction mixture was extracted with 30 mL of dichloromethane and the organic phase was dried with anhydrous sodium sulfate. After filtration, the filtrate was concentrated under reduced pressure. Purification by fast column chromatography using petroleum ether as eluent gave 2.1 g of light yellow solid 1-chloro-4-iodo-2-trifluoromethylbenzene in 69% yield.
References
[1] Patent: CN108184888, 2018, A. Location in patent: Paragraph 0014
[2] Patent: CN108338175, 2018, A. Location in patent: Paragraph 0019
[3] Patent: CN108353907, 2018, A. Location in patent: Paragraph 0015-0016
[4] Patent: CN108353920, 2018, A. Location in patent: Paragraph 0014
[5] Patent: CN108432777, 2018, A. Location in patent: Paragraph 0016
2-Chloro-5-iodobenzotrifluoride Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Chloro-5-iodobenzotrifluoride manufacturers
- Product
- 2-Chloro-5-iodobenzotrifluoride 260355-20-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-10
- Product
- 2-Chloro-5-iodobenzotrifluoride 260355-20-2
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 97-99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-19
- Product
- 2-Chloro-5-iodobenzotrifluoride 260355-20-2
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 500KG
- Release date
- 2019-04-16