1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)

Product Name: 1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)
CAS No.: 54384-74-6
Chemical Name: 1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)
Synonyms: 1,5-DiMethylpyrazole-3-carboxaMide;1,5-Dimethyl-1H-pyrazole-3-carboxamide;1H-Pyrazole-3-carboxamide, 1,5-dimethyl-;1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI);1,5-Dimethyl-1H-pyrazole-3-carboxylic acid amide
CBNumber: CB41297825
Molecular Formula: C6H9N3O
Formula Weight: 139.16
MOL File: 54384-74-6.mol

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1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Property

Boiling point:: 288.7±28.0 °C(Predicted)
Density: 1.28±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.85±0.50(Predicted)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-37/39
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: D480233
Product name: 1,5-Dimethyl-1H-pyrazole-3-carboxamide
Packaging: 500mg
Price: $90
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK189065
Product name: 1,5-Dimethyl-1H-pyrazole-3-carboxamide
Purity: 97%
Packaging: 1g
Price: $73
Updated: 2021/12/16

AK Scientific

Product number: Z2263
Product name: 1,5-Dimethyl-1H-pyrazole-3-carboxylicacidamide
Packaging: 50mg
Price: $103
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK189065
Product name: 1,5-Dimethyl-1H-pyrazole-3-carboxamide
Purity: 97%
Packaging: 5g
Price: $271
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-1-DH
Product name: 1,5-Dimethyl-1H-pyrazole-3-carboxamide
Packaging: 1g
Price: $360
Updated: 2021/12/16

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1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Chemical Properties,Usage,Production

Chemical Properties

White crystals

Synthesis

5744-59-2

54384-74-6

General procedure for the synthesis of 1,5-dimethyl-1H-pyrazole-3-carboxamide from 1,5-dimethyl-1H-pyrazole-3-carboxylic acid: 1,5-dimethyl-1H-pyrazole-3-carboxylic acid (10 g, 71.43 mmol) was mixed with sulfinyl chloride (SOCl2, 25.5 g, 214.29 mmol), and the reaction was carried out at reflux for 2 hours. After completion of the reaction, the mixture was concentrated under vacuum. Subsequently, 200 mL of ammonia (NH3-H2O) was slowly added dropwise to the residue at 0 °C and the reaction was carried out under stirring. At the end of the reaction, the solid product was collected by filtration to afford 8 g (81% yield) of 1,5-dimethyl-1H-pyrazole-3-carboxamide as a white solid.

References

[1] Patent: WO2009/139834, 2009, A1. Location in patent: Page/Page column 128-129

1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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54384-74-6, 1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)Related Search:

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1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)

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