1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)
- Product Name
- 1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)
- CAS No.
- 54384-74-6
- Chemical Name
- 1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI)
- Synonyms
- 1,5-DiMethylpyrazole-3-carboxaMide;1,5-Dimethyl-1H-pyrazole-3-carboxamide;1H-Pyrazole-3-carboxamide, 1,5-dimethyl-;1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI);1,5-Dimethyl-1H-pyrazole-3-carboxylic acid amide
- CBNumber
- CB41297825
- Molecular Formula
- C6H9N3O
- Formula Weight
- 139.16
- MOL File
- 54384-74-6.mol
1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Property
- Boiling point:
- 288.7±28.0 °C(Predicted)
- Density
- 1.28±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 15.85±0.50(Predicted)
N-Bromosuccinimide Price
- Product number
- D480233
- Product name
- 1,5-Dimethyl-1H-pyrazole-3-carboxamide
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- Z2263
- Product name
- 1,5-Dimethyl-1H-pyrazole-3-carboxylicacidamide
- Packaging
- 50mg
- Price
- $103
- Updated
- 2021/12/16
- Product number
- JK189065
- Product name
- 1,5-Dimethyl-1H-pyrazole-3-carboxamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $271
- Updated
- 2021/12/16
- Product number
- 4H48-1-DH
- Product name
- 1,5-Dimethyl-1H-pyrazole-3-carboxamide
- Packaging
- 1g
- Price
- $360
- Updated
- 2021/12/16
- Product number
- 085387
- Product name
- 1,5-Dimethyl-1H-pyrazole-3-carboxamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $561
- Updated
- 2021/12/16
1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Chemical Properties,Usage,Production
Chemical Properties
White crystals
Synthesis
5744-59-2
54384-74-6
General procedure for the synthesis of 1,5-dimethyl-1H-pyrazole-3-carboxamide from 1,5-dimethyl-1H-pyrazole-3-carboxylic acid: 1,5-dimethyl-1H-pyrazole-3-carboxylic acid (10 g, 71.43 mmol) was mixed with sulfinyl chloride (SOCl2, 25.5 g, 214.29 mmol), and the reaction was carried out at reflux for 2 hours. After completion of the reaction, the mixture was concentrated under vacuum. Subsequently, 200 mL of ammonia (NH3-H2O) was slowly added dropwise to the residue at 0 °C and the reaction was carried out under stirring. At the end of the reaction, the solid product was collected by filtration to afford 8 g (81% yield) of 1,5-dimethyl-1H-pyrazole-3-carboxamide as a white solid.
References
[1] Patent: WO2009/139834, 2009, A1. Location in patent: Page/Page column 128-129
1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
1H-Pyrazole-3-carboxamide,1,5-dimethyl-(9CI) Suppliers
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