3-BROMO-2-METHYLPHENOL

Product Name: 3-BROMO-2-METHYLPHENOL
CAS No.: 7766-23-6
Chemical Name: 3-BROMO-2-METHYLPHENOL
Synonyms: 2-Methyl-3-broMophenol;3-BROMO-2-METHYLPHENOL;Phenol, 3-bromo-2-methyl-;2-Bromo-6-hydroxytoluene, 3-Bromo-o-cresol
CBNumber: CB42455882
Molecular Formula: C7H7BrO
Formula Weight: 187.03
MOL File: 7766-23-6.mol

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3-BROMO-2-METHYLPHENOL Property

Melting point:: 95°C
Boiling point:: 220.79°C (rough estimate)
Density: 1.3839 (rough estimate)
refractive index: 1.5772 (estimate)
storage temp.: Inert atmosphere,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
pka: 9.35±0.10(Predicted)
color: Off-White

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Safety

HS Code: 2908190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B697423
Product name: 3-Bromo-2-methylphenol
Packaging: 250mg
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140241
Product name: 3-Bromo-2-methylphenol
Packaging: 1g
Price: $80
Updated: 2021/12/16

AK Scientific

Product number: J51151
Product name: 3-Bromo-2-methylphenol
Packaging: 5g
Price: $110
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140241
Product name: 3-Bromo-2-methylphenol
Packaging: 2g
Price: $140
Updated: 2021/12/16

AK Scientific

Product number: W8421
Product name: 3-Bromo-2-methylphenol
Packaging: 5g
Price: $147
Updated: 2021/12/16

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3-BROMO-2-METHYLPHENOL Chemical Properties,Usage,Production

Synthesis

55289-36-6

7766-23-6

General procedure for the synthesis of 3-bromo-2-methylphenol from 3-bromo-2-methylaniline: a solution of sodium was slowly added to a solution of 3-bromo-2-methylaniline (6 g, 32.2 mmol) in sulfuric acid (38.7 mL, 38.7 mmol) at 0 °C. The reaction mixture was stirred at 0°C for 15 minutes before sulfuric acid (13.75 mL, 258 mmol) was added, followed by warming the reaction system to 100°C and heating for 1 hour. After completion of the reaction, the mixture was diluted with water and extracted with ether (Et2O). The organic phase was dried and concentrated and purified by silica gel column chromatography to afford the target product 3-bromo-2-methylphenol (light brown solid, 4.92 g, 82% yield).

References

[1] Chemical Communications, 2003, # 10, p. 1170 - 1171
[2] Patent: US2011/82165, 2011, A1. Location in patent: Page/Page column 46
[3] Journal of Medicinal Chemistry, 2017, vol. 60, # 4, p. 1417 - 1431
[4] European Journal of Organic Chemistry, 2018, vol. 2018, # 17, p. 2013 - 2021
[5] Patent: US6831106, 2004, B1. Location in patent: Page column 19

3-BROMO-2-METHYLPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BROMO-2-METHYLPHENOL Suppliers

China 130 India 1 United Kingdom 3 United States 8 Global 142

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View Lastest Price from 3-BROMO-2-METHYLPHENOL manufacturers

Henan Bao Enluo International TradeCo.，LTD

Product: 3-BROMO-2-METHYLPHENOL 7766-23-6
Price: US $10.00/kg
Min. Order: 1kg
Purity: 99.99%
Supply Ability: 50000tons
Release date: 2023-08-15

Career Henan Chemical Co

Product: 3-BROMO-2-METHYLPHENOL 7766-23-6
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-01-12

7766-23-6, 3-BROMO-2-METHYLPHENOLRelated Search:

2-BROMO-6-METHOXYBENZOIC ACID 3,4,5,6-TETRABROMO-O-CRESOL 6-BROMO-2-HYDROXY-3-METHOXYBENZALDEHYDE 2,3-DIBROMO-6-HYDROXY-5-METHOXY-BENZALDEHYDE 5-BROMO-1,3-BENZODIOXOLE-4-CARBOXYLIC ACID 6-BROMO-2,3-DIHYDROXYBENZALDEHYDE 2,3-DIBROMO-5-ETHOXY-6-HYDROXYBENZALDEHYDE 1-BROMO-3,4-DIMETHOXY-2-METHYLBENZENE 5-BROMO-25,26,27,28-TETRAPROPOXYCALIX[4]ARENE 6-BROMO-3-ETHOXY-2-HYDROXYBENZALDEHYDE 2,4-DIBROMO-6-HYDROXYBENZONITRILE AKOS BBS-00001989 RARECHEM AL BO 2066 2-BROMO-6-HYDROXY-5-METHOXY-3-NITRO-BENZALDEHYDE VITAS-BB TBB000554 AKOS BBS-00001986 VITAS-BB TBB000564

3-BROMO-2-METHYLPHENOL

Phenol, 3-bromo-2-methyl-

2-Bromo-6-hydroxytoluene, 3-Bromo-o-cresol

2-Methyl-3-broMophenol

7766-23-6