3-Bromo-N-methyl-N-boc-propylamine
- Product Name
- 3-Bromo-N-methyl-N-boc-propylamine
- CAS No.
- 828272-19-1
- Chemical Name
- 3-Bromo-N-methyl-N-boc-propylamine
- Synonyms
- tert-Butyl (3-bromopropyl)(methyl)carbamate;-N-boc-propyL;3-Bromo-N-methyL;N-Boc-N-methyl-3-bromopropylamine;3-Bromo-N-methyl-N-boc-propylamine;tert-butyl N-(3-bromopropyl)-N-methylcarbamate;(3-Bromo-propyl)-methyl-carbamic acid tert-butyl ester;Carbamic acid, (3-bromopropyl)methyl-, 1,1-dimethylethyl ester;N-(3-BroMopropyl)-N-MethylcarbaMic Acid 1,1-DiMethylethyl Ester;Carbamic acid, N-(3-bromopropyl)-N-methyl-, 1,1-dimethylethyl ester
- CBNumber
- CB42486949
- Molecular Formula
- C9H18BrNO2
- Formula Weight
- 252.15
- MOL File
- 828272-19-1.mol
3-Bromo-N-methyl-N-boc-propylamine Property
- Boiling point:
- 268.4±19.0 °C(Predicted)
- Density
- 1.254±0.06 g/cm3(Predicted)
- solubility
- Chloroform, Dichloromethane, Ethyl Acetate
- pka
- -1.39±0.70(Predicted)
- InChI
- InChI=1S/C9H18BrNO2/c1-9(2,3)13-8(12)11(4)7-5-6-10/h5-7H2,1-4H3
- InChIKey
- PIUWBRCCWDAPFG-UHFFFAOYSA-N
- SMILES
- C(OC(C)(C)C)(=O)N(CCCBr)C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B685315
- Product name
- 3-Bromo-N-methyl-N-boc-propylamine
- Packaging
- 200mg
- Price
- $1320
- Updated
- 2021/12/16
- Product number
- AS106701
- Product name
- N-Boc-N-methyl-3-bromopropylamine
- Purity
- 97%
- Packaging
- 1g
- Price
- $400
- Updated
- 2021/12/16
- Product number
- 7673DG
- Product name
- 3-Bromo-N-methyl-N-boc-propylamine
- Packaging
- 500mg
- Price
- $700
- Updated
- 2021/12/16
- Product number
- HCH0104275
- Product name
- 3-BROMO-N-METHYL-N-BOC-PROPYLAMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $769.65
- Updated
- 2021/12/16
- Product number
- 7673DG
- Product name
- 3-Bromo-N-methyl-N-boc-propylamine
- Packaging
- 1g
- Price
- $870
- Updated
- 2021/12/16
3-Bromo-N-methyl-N-boc-propylamine Chemical Properties,Usage,Production
Synthesis
Into a 100 mL round-bottom flask were placed tert-butyl (3- hydroxypropyl)(methyl)carbamate (2.00 g, 10.60 mmol, 1.00 equiv), DCM (20.00 mL) and PPh3 (3.67 g, 13.80 mmol, 1.30 equiv). This was followed by addition of CBr4 (5.20 g, 13.80 mmol, 1.30 equiv) at 0 °C. The resulting solution was stirred for 1.5 h at 0 °C. The reaction mixture was quenched with H2O (50.00 mL), extracted with DCM (100 mL*2). The combined organic phase was washed with Na2CO3 (aq), brine and dried over anhydrous sodium sulfate. After filtration, the filtrate was concentrated under reduced pressure. The residue was purified by silica gel column with petroleum ether/ethyl acetate (93%/7%). This resulted in 2.6 g of 3-Bromo-N-methyl-N-boc-propylamine as light yellow oil.
3-Bromo-N-methyl-N-boc-propylamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Bromo-N-methyl-N-boc-propylamine manufacturers
- Product
- 3-Bromo-N-methyl-N-boc-propylamine 828272-19-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 0.1kg
- Purity
- 98%
- Supply Ability
- 100kg
- Release date
- 2023-03-09