ChemicalBook > CAS DataBase List > 3-Amino-4-methylbenzonitrile

3-Amino-4-methylbenzonitrile

Product Name: 3-Amino-4-methylbenzonitrile
CAS No.: 60710-80-7
Chemical Name: 3-Amino-4-methylbenzonitrile
Synonyms: 3-Amino-p-tolunitrile;2-Amino-4-cyanotoluene;3-AMINO-4-METHYLBENZONITRILE;Benzonitrile, 3-amino-4-methyl-;3-Amino-4-methylbenzonitrile 98%;5-Cyano-2-methylaniline, 2-Amino-4-cyanotoluene
CBNumber: CB4257974
Molecular Formula: C8H8N2
Formula Weight: 132.16
MOL File: 60710-80-7.mol

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3-Amino-4-methylbenzonitrile Property

Melting point:: 81 °C
Boiling point:: 312.8±22.0 °C(Predicted)
Density: 1.10±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 2?+-.0.10(Predicted)
form: crystals
color: White to off white to clear shards
InChI: InChI=1S/C8H8N2/c1-6-2-3-7(5-9)4-8(6)10/h2-4H,10H2,1H3
InChIKey: IEWMNQUBZPVSSV-UHFFFAOYSA-N
SMILES: C(#N)C1=CC=C(C)C(N)=C1
CAS DataBase Reference: 60710-80-7(CAS DataBase Reference)

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Safety

Hazard Codes: T
Risk Statements: 36/37/38
Safety Statements: 26-36
RIDADR: 3276
Hazard Note: Toxic
HazardClass: IRRITANT
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: A898175
Product name: 3-Amino-4-methylbenzonitrile
Packaging: 2.5g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: J55246
Product name: 3-Amino-4-methylbenzonitrile
Packaging: 1g
Price: $10
Updated: 2021/12/16

Matrix Scientific

Product number: 066906
Product name: 3-Amino-4-methylbenzonitrile
Purity: 98%
Packaging: 5g
Price: $13
Updated: 2021/12/16

AK Scientific

Product number: J55246
Product name: 3-Amino-4-methylbenzonitrile
Packaging: 5g
Price: $15
Updated: 2021/12/16

Apolloscientific

Product number: OR4824
Product name: 3-Amino-4-methylbenzonitrile
Purity: 98%
Packaging: 5g
Price: $15
Updated: 2021/12/16

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3-Amino-4-methylbenzonitrile Chemical Properties,Usage,Production

Chemical Properties

off-white crystalline

Uses

3-Amino-4-methylbenzonitrile is an organic compound commonly used as an intermediate in organic synthesis, especially in pharmaceutical and pesticide chemistry.

Synthesis

939-79-7

60710-80-7

C.14.b. Synthesis of 3-amino-4-methylbenzonitrile: 120 g of 3-nitro-4-methylbenzonitrile was suspended in 1.2 L of ethanol, and 7 g of 10% Pd/C catalyst was added and the hydrogenation reaction was carried out in a 50 L hydrogen atmosphere at room temperature. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration, followed by distillation under reduced pressure to remove the solvent to afford 95 g of pure 3-amino-4-methylbenzonitrile in 97% yield. The product was characterized by 1H-NMR (DMSO-d6; δ, ppm): 7.1 (dd, 1H); 6.90 (d, 1H); 6.85 (d, 1H); 5.35 (s, 2H, NH2); 2.15 (s, 3H).

References

[1] Patent: US6455671, 2002, B1
[2] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 8, p. 1203 - 1208
[3] Chemische Berichte, 1903, vol. 36, p. 4359
[4] Chemische Berichte, 1904, vol. 37, p. 1845
[5] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 1997, vol. 53, # 2, p. 141 - 150

3-Amino-4-methylbenzonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Amino-4-methylbenzonitrile Suppliers

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View Lastest Price from 3-Amino-4-methylbenzonitrile manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 3-AMINO-4-METHYLBENZONITRILE 60710-80-7
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-09-22

Milestone Chemical Wuxi Co.,Ltd

Product: 3-AMINO-4-METHYLBENZONITRILE 60710-80-7
Price: US $0.00-0.00/kg T
Min. Order: 1kg T
Purity: 99.9%MIN
Supply Ability: 20TONS
Release date: 2023-03-20

60710-80-7, 3-Amino-4-methylbenzonitrileRelated Search:

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60710-80-7

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