2-(BOC-AMINO)-3-METHYLPYRIDINE

Product Name: 2-(BOC-AMINO)-3-METHYLPYRIDINE
CAS No.: 138343-75-6
Chemical Name: 2-(BOC-AMINO)-3-METHYLPYRIDINE
Synonyms: 112777;BUTTPARK 92\50-22;2-BOC-Amino-3-picoline;N-Boc-3-methylpyridin-2-amine;2-(BOC-AMINO)-3-METHYLPYRIDINE;N-Boc-3-isopropylpyridin-2-amine;2-(N-Boc-Amino)-3-methylpyridine;2-(Boc-amino)-3-methylpyridine 97%;t-Butyl 3-methylpyridin-2-ylcarbamate;2-(N-BOC-AMINO)-3-METHYLPYRIDINE, 97%
CBNumber: CB4307903
Molecular Formula: C11H16N2O2
Formula Weight: 208.26
MOL File: 138343-75-6.mol

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2-(BOC-AMINO)-3-METHYLPYRIDINE Property

Melting point:: 134-138 °C (lit.)
Boiling point:: 268.5±28.0 °C(Predicted)
Density: 1.108±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: solid
pka: 12.56±0.70(Predicted)
Appearance: White to off-white Solid
InChIKey: MJPLUXLNYQHWIU-UHFFFAOYSA-N

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Safety

Hazard Codes: Xn
Risk Statements: 22-36-43
Safety Statements: 26-36/37
WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 643920
Product name: 2-(Boc-amino)-3-methylpyridine
Purity: 97%
Packaging: 25g
Price: $293
Updated: 2023/06/20

TCI Chemical

Product number: B6201
Product name: tert-Butyl (3-Methylpyridin-2-yl)carbamate
Packaging: 5G
Price: $25
Updated: 2025/07/31

TCI Chemical

Product number: B6201
Product name: tert-Butyl (3-Methylpyridin-2-yl)carbamate
Packaging: 25G
Price: $74
Updated: 2025/07/31

TRC

Product number: B423328
Product name: tert-Butyl3-Methylpyridin-2-ylcarbamate
Packaging: 100mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: Z0166
Product name: 2-BOC-Amino-3-picoline
Packaging: 1g
Price: $21
Updated: 2021/12/16

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2-(BOC-AMINO)-3-METHYLPYRIDINE Chemical Properties,Usage,Production

Synthesis Reference(s)

Tetrahedron, 64, p. 500, 2008 DOI: 10.1016/j.tet.2007.11.011

Synthesis

1603-40-3

24424-99-5

138343-75-6

General procedure for the synthesis of 2-(Boc-amino)-3-methylpyridine from 2-amino-3-methylpyridine and di-tert-butyl dicarbonate: di-tert-butyl dicarbonate (50.0 g) was dissolved in n-hexane (55 mL), heated to 58 °C with continuous stirring. Subsequently, a solution of ethyl acetate (20 mL) of 2-amino-3-methylpyridine (15.5 g) was added slowly and dropwise to this solution. The reaction mixture was heated and stirred at 58°C for 3 hours and then cooled to room temperature. The reaction mixture was diluted by addition of hexane (30 mL) and stirring was continued for 1.5 hours. The precipitated white solid precipitate was collected by filtration and dried to give 25.8 g of 2-(Boc-amino)-3-methylpyridine in 86% yield. Mass spectrometry (FAB) analysis showed m/z: 209 (M + H)+.

References

[1] Organic Process Research and Development, 2010, vol. 14, # 1, p. 168 - 173
[2] Patent: EP1764360, 2007, A1. Location in patent: Page/Page column 195
[3] Synthesis, 1996, # 7, p. 877 - 882
[4] Tetrahedron, 2008, vol. 64, # 3, p. 500 - 507
[5] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 21, p. 6582 - 6591

2-(BOC-AMINO)-3-METHYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(BOC-AMINO)-3-METHYLPYRIDINE Suppliers

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View Lastest Price from 2-(BOC-AMINO)-3-METHYLPYRIDINE manufacturers

Dideu Industries Group Limited

Product: 2-(BOC-AMINO)-3-METHYLPYRIDINE 138343-75-6
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-27

Career Henan Chemical Co

Product: 2-BOC-Amino-3-picoline 138343-75-6
Price: US $8.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 100kg
Release date: 2019-07-04

138343-75-6, 2-(BOC-AMINO)-3-METHYLPYRIDINERelated Search:

tert-butyl (3-formyl-4-hydroxyphenyl)carbamate tert-butyl (3-fluoropropyl)(2-hydroxyethyl)carbamate BOC-TRANS-4-AMINOCYCLOHEXANOL tert-butyl 1H-pyrrol-2-ylcarbamate Carbamic acid, 3-azabicyclo[3.1.0]hex-6-yl-, 1,1-dimethylethyl ester, N-(3-AMino[1,1'-biphenyl]-4-yl)-carbaMic Acid tert-Butyl Ester tert-butyl (2-bromo-3-fluorophenyl)carbamate tert-Butyl(3-formylbicyclo[1.1.1]pentan-1-yl)carbamate tert-butyl (3-(hydroxymethyl)bicyclo[1.1.1]pentan-1-yl)carbamate tert-butyl (2,2,3,3-tetramethylcyclopropyl)carbamate tert-butyl (3,5-dibromopyrazin-2-yl)carbamate 2-(tert-Butyloxycarbonyl-methylamino)-5-iodo-3-methylpyridine 2-(N-METHYL-N-BOC-AMINO)-3-METHYLPYRIDINE-5-BORONIC ACID PINACOL ESTER 2-N-Boc-amino-3-formylpyridine 2-(BOC-AMINO)-3-METHYLPYRIDINE (3-HYDROXYMETHYL-PYRIDIN-2-YL)-CARBAMIC ACID TERT-BUTYL ESTER 8-N-BOC-5,6,7,8-TETRAHYDRO-1,8-NAPHTHYRIDIN-2-METHYLAMINE 7-METHYL-3,4-DIHYDRO-2H-[1,8]NAPHTHYRIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

(3-METHYLPYRIDINE-2-YL)CARBAMIC ACID TERT-BUTYL ESTER

Carbamic acid, N-(3-methyl-2-pyridinyl)-, 1,1-dimethylethyl ester

2-tert-butoxycarbonylamino-3-methylpyridine

N-Boc-3-isopropylpyridin-2-amine

N-Boc-3-methylpyridin-2-amine

2-BOC-Amino-3-picoline

t-Butyl 3-methylpyridin-2-ylcarbamate

tert-butyl N-(3-Methylpyridin-2-yl)carbaMate

tert-butyl (3-Methylpyridin-2-yl)carbaMate

Carbamic acid, (3-methyl-2-pyridinyl)-

2-(Boc-amino)-3-methylpyridine 97%

BUTTPARK 92\50-22

2-(BOC-AMINO)-3-METHYLPYRIDINE

2-(N-BOC-AMINO)-3-METHYLPYRIDINE, 97%

Carbamic acid, (3-methyl-2-pyridinyl)-, 1,1-dimethylethyl ester (9CI)

112777

2-(BOC-AMINO)-3-METHYLPYRIDINE ISO 9001：2015 REACH

tert-butyl N-(3-methyl-2-pyridyl)carbamate

2-(N-Boc-Amino)-3-methylpyridine

138343-75-6

C9 to C46

Building Blocks

Pyridines

Heterocyclic Building Blocks

N-BOC

pharmacetical

C9 to C46

Heterocyclic Building Blocks

Pyridines

Heterocyclic Compounds