ChemicalBook > CAS DataBase List > 7-NITROINDOLE-3-CARBOXALDEHYDE

7-NITROINDOLE-3-CARBOXALDEHYDE

Product Name
7-NITROINDOLE-3-CARBOXALDEHYDE
CAS No.
10553-14-7
Chemical Name
7-NITROINDOLE-3-CARBOXALDEHYDE
Synonyms
Zinc02572407;7-NITROINDOLE-3-ALDEHYDE;3-Carboxy-7-nitro-1H-indole;7-NITROINDOLE-3-CARBOXALDEHYDE;7-NITROINDOLE-3-CARBOXYALDEHYDE;7-NITRO-1H-INDOLE-3-CARBALDEHYDE;7-Nitroindole-3-carboxaldehyde 98%;7-Nitro-1H-indole-3-carboxaldehyde;7-Nitroindole-3-carboxaldehyde,97%;(7-nitro-3-indolylidene)methanolate
CBNumber
CB4316686
Molecular Formula
C9H6N2O3
Formula Weight
190.16
MOL File
10553-14-7.mol
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7-NITROINDOLE-3-CARBOXALDEHYDE Property

Boiling point:
441.5±25.0 °C(Predicted)
Density 
1.516±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
12.47±0.30(Predicted)
form 
Solid
Appearance
Light yellow to yellow Solid
InChI
InChI=1S/C9H6N2O3/c12-5-6-4-10-9-7(6)2-1-3-8(9)11(13)14/h1-5,10H
InChIKey
ADGKBVRTGVODMM-UHFFFAOYSA-N
SMILES
N1C2=C(C=CC=C2[N+]([O-])=O)C(C=O)=C1
CAS DataBase Reference
10553-14-7(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
N900623
Product name
7-Nitro-1H-indole-3-carbaldehyde
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
N900623
Product name
7-Nitro-1H-indole-3-carbaldehyde
Packaging
100mg
Price
$60
Updated
2021/12/16
Apolloscientific
Product number
OR1670
Product name
7-Nitro-1H-indole-3-carboxaldehyde
Purity
95+%
Packaging
1g
Price
$48
Updated
2021/12/16
SynQuest Laboratories
Product number
4H55-1-W9
Product name
7-Nitro-1H-indole-3-carboxaldehyde
Purity
95.0%
Packaging
1g
Price
$53
Updated
2021/12/16
Matrix Scientific
Product number
071712
Product name
7-Nitroindole-3-carboxyaldehyde
Purity
95+%
Packaging
1g
Price
$231
Updated
2021/12/16
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7-NITROINDOLE-3-CARBOXALDEHYDE Chemical Properties,Usage,Production

Synthesis

6960-42-5

68-12-2

10553-14-7

Phosphorus oxychloride (POCl3, 0.418 mL, 3.13 mmol) was slowly added dropwise to N,N-dimethylformamide (DMF, 2.08 mL) at 0°C and under argon protection. After stirring the reaction mixture for 5 min, a DMF solution of 7-nitroindole (200 mg, 1.25 mmol) was added (at a concentration of 10 mL of DMF per 1 g of indole). Subsequently, the reaction mixture was gradually warmed to room temperature and stirring was continued for 3 hours. After completion of the reaction, 3.8 M aqueous potassium hydroxide solution (3.29 mL, 12.5 mmol) was added to the mixture and stirring was continued for 15 hours. Next, saturated aqueous sodium bicarbonate and ethyl acetate (EtOAc) were added to the reaction system until the mixture became clarified, followed by separation of the organic layer. The aqueous phase was extracted with ethyl acetate and the combined organic layers were washed with brine, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure. Finally, the residue was purified by silica gel column chromatography (eluent ratio hexane/ethyl acetate = 1/5) to afford the target product 7-nitroindole-3-carbaldehyde (228 mg, 1.20 mmol, 96% yield) as a yellow amorphous solid.

References

[1] Chemical and Pharmaceutical Bulletin, 2018, vol. 66, # 8, p. 810 - 817
[2] European Journal of Medicinal Chemistry, 2013, vol. 65, p. 158 - 167
[3] Tetrahedron Letters, 2009, vol. 50, # 1, p. 75 - 76
[4] Journal of Medicinal Chemistry, 2008, vol. 51, # 23, p. 7541 - 7551
[5] Journal of Organic Chemistry, 2013, vol. 78, # 6, p. 2362 - 2372

7-NITROINDOLE-3-CARBOXALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-NITROINDOLE-3-CARBOXALDEHYDE Suppliers

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View Lastest Price from 7-NITROINDOLE-3-CARBOXALDEHYDE manufacturers

Chemwill Asia Co.,Ltd.
Product
7-Nitroindole-3-carboxaldehyde in stock Factory 10553-14-7
Price
US $1.00/KG
Min. Order
1KG
Purity
TOP 3 Factory in China
Supply Ability
Top 3 largest production capacity Factory
Release date
2019-04-03
Career Henan Chemical Co
Product
7-NITROINDOLE-3-CARBOXALDEHYDE 10553-14-7
Price
US $6.60/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg -1000kg
Release date
2020-01-02

10553-14-7, 7-NITROINDOLE-3-CARBOXALDEHYDERelated Search:

7-NITROINDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTE 1-BENZYL-5-NITROINDOLE-3-CARBOXALDEHYDE 5-METHOXY-1-METHYL-4-NITROINDOLE-3-CARBOXALDEHYDE,5-METHOXY-1-METHYL-4-NITROINDOLE-3-CARBOXALDEHYDE: TECH., 90% 6-Nitroindole-3-carboxaldehyde 2-METHYL-5-NITROINDOLE-3-CARBOXALDEHYDE 5-NITROINDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTE 5-NITROINDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTED 4-Nitroindole-3-carboxaldehyde 5-NITROINDOLE-3-CARBOXALDEHYDE 7-NITROINDOLE-2-CARBOXALDEHYDE 7-NITROINDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTED 7-Aminoindole 7-Nitroindole ETHYL 3-FORMYL-7-NITRO-1H-INDOLE-2-CARBOXYLATE 7-NITROINDOLE-3-CARBOXALDEHYDE

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  • 7-NITROINDOLE-3-ALDEHYDE
  • 7-NITROINDOLE-3-CARBOXALDEHYDE
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  • 7-Nitro-1H-indole-3-carboxaldehyde
  • 7-Nitroindole-3-carboxaldehyde in stock Factory
  • (7-nitro-3-indolylidene)methanolate
  • 1H-Indole-3-carboxaldehyde, 7-nitro-
  • 7-Nitroindole-3-carboxaldehyde,97%
  • 10553-14-7
  • C9H5N2O3
  • Indole