ChemicalBook > CAS DataBase List > trans-2-Benzylamino-1-cyclohexanol

trans-2-Benzylamino-1-cyclohexanol

Product Name
trans-2-Benzylamino-1-cyclohexanol
CAS No.
40571-86-6
Chemical Name
trans-2-Benzylamino-1-cyclohexanol
Synonyms
amino)cycL;trans-2-(BenzyL;TRANS-2-(BENZYLAMINO)CYCLOHEXANOL;TRANS-2-BENZYLAMINO-1-CYCLOHEXANOL;Trans-2-(N-Benzylamino)cyclohexanol;(1R,2R)-2-(benzylamino)cyclohexanol;(1R,2R)-2-(benzylaMino)cyclopentanol;trans-2-(Benzylamino)cyclohexan-1-ol;Trans-2-benzylamino-1-cyclohexanol, 99+%;(2-hydroxycyclohexyl)-(phenylmethyl)ammonium
CBNumber
CB4668460
Molecular Formula
C13H19NO
Formula Weight
205.3
MOL File
40571-86-6.mol
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trans-2-Benzylamino-1-cyclohexanol Property

Melting point:
69-72 °C
Boiling point:
69-72°C
Density 
0.9923 (rough estimate)
refractive index 
1.5175 (estimate)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
crystal
pka
14.83±0.40(Predicted)
color 
white
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Safety

Risk Statements 
11-36/37/38
Safety Statements 
24/25
TSCA 
No
HS Code 
2921490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
B233868
Product name
trans-2-(Benzylamino)cyclohexanol
Packaging
500mg
Price
$175
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB153893
Product name
trans-2-Benzylamino-1-cyclohexanol
Packaging
5G
Price
$471.25
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CCH0040695
Product name
TRANS-2-(BENZYLAMINO)CYCLOHEXANOL
Purity
95.00%
Packaging
1G
Price
$685.21
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB153893
Product name
trans-2-Benzylamino-1-cyclohexanol
Packaging
10g
Price
$801
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CCH0040695
Product name
TRANS-2-(BENZYLAMINO)CYCLOHEXANOL
Purity
95.00%
Packaging
5G
Price
$1182.44
Updated
2021/12/16
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trans-2-Benzylamino-1-cyclohexanol Chemical Properties,Usage,Production

Chemical Properties

VERY SLIGHTLY YELLOW TO BEIGE CRYSTALLINE POWDER

Uses

suzuki reaction

Synthesis

286-20-4

100-46-9

40571-86-6

General procedure for the synthesis of trans-2-benzylaminocyclohexanol from cyclohexene oxide and benzylamine: cyclohexene oxide (20 g, 204 mmol) was mixed with benzylamine (44 g, 411 mmol), and the reaction was carried out for 6 hours at 80 °C. After completion of the reaction, the excess benzylamine was removed by distillation under reduced pressure. The crude product was purified by silica gel column chromatography with the eluent being a chloroform solution of 5-10% methanol to give (1RS,2RS)-trans-2-benzylaminocyclohexanol (26 g, 127 mmol, 62% yield) as white crystals.

References

[1] Tetrahedron Letters, 2008, vol. 49, # 9, p. 1546 - 1550
[2] Tetrahedron, 2011, vol. 67, # 47, p. 9214 - 9218
[3] Journal of Organic Chemistry, 2007, vol. 72, # 10, p. 3713 - 3722
[4] Tetrahedron Letters, 1990, vol. 31, # 32, p. 4661 - 4664
[5] Synthetic Communications, 2001, vol. 31, # 21, p. 3295 - 3302

trans-2-Benzylamino-1-cyclohexanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from trans-2-Benzylamino-1-cyclohexanol manufacturers

Career Henan Chemical Co
Product
trans-2-Benzylamino-1-cyclohexanol 40571-86-6
Price
US $2.00/KG
Min. Order
1g
Purity
98%min
Supply Ability
ask
Release date
2020-01-08

40571-86-6, trans-2-Benzylamino-1-cyclohexanolRelated Search:

trans,trans-2,4-Undecadienal 2-Aminocyclohexanol trans-4-Aminocyclohexanol Cyclohexanol 1-Methylcyclohexanol 4-Aminocyclohexanol Cyclamic acid Molasses Ethylene glycol TRANS-2-(4-METHOXY-BENZYLAMINO)-CYCLOHEXANOL trans-2-Benzylamino-1-cyclohexanol

  • TRANS-2-BENZYLAMINO-1-CYCLOHEXANOL
  • TRANS-2-(BENZYLAMINO)CYCLOHEXANOL
  • Trans-2-benzylamino-1-cyclohexanol, 99+%
  • (1R,2R)-2-(benzylamino)cyclohexanol
  • (1R,2R)-2-(benzylaMino)cyclopentanol
  • rel-(1R,2R)-2-[(Phenylmethyl)amino]cyclohexanol
  • (2-hydroxycyclohexyl)-(phenylmethyl)ammonium
  • amino)cycL
  • trans-2-(BenzyL
  • Cyclohexanol, 2-[(phenylmethyl)amino]-, (1R,2R)-rel-
  • Trans-2-(N-Benzylamino)cyclohexanol
  • trans-2-(Benzylamino)cyclohexan-1-ol
  • 40571-86-6
  • pharmacetical