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Diethylene glycol diethyl ether

Uses
Product Name
Diethylene glycol diethyl ether
CAS No.
112-36-7
Chemical Name
Diethylene glycol diethyl ether
Synonyms
DIETHYLENE GLYCOL DIETHYL ETHER;DIETHYL CARBITOL;Diethyl carbito;BIS(2-ETHOXYETHYL) ETHER;Diethyldigol;ethyldiglyme;Ethyl diglyme;DIETHYLDIGLYCOL;DIETHOXYDIGLYCOL;DIETHYL CARBITOL(R)
CBNumber
CB4669548
Molecular Formula
C8H18O3
Formula Weight
162.23
MOL File
112-36-7.mol
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Diethylene glycol diethyl ether Property

Melting point:
-44.3 °C
Boiling point:
180-190 °C(lit.)
Density 
0.909 g/mL at 25 °C(lit.)
vapor density 
5.6 (vs air)
vapor pressure 
0.5 mm Hg ( 20 °C)
refractive index 
n20/D 1.412(lit.)
Flash point:
160 °F
storage temp. 
Store below +30°C.
solubility 
Chloroform (Sparingly), Methanol (Slightly)
form 
Liquid
color 
Clear
Relative polarity
3.9
explosive limit
6.2%
Water Solubility 
SOLUBLE
λmax
λ: 260 nm Amax: 1.00
λ: 300 nm Amax: 0.10
λ: 320 nm Amax: 0.04
λ: 350-400 nm Amax: 0.01
Merck 
14,3118
BRN 
1699259
Dielectric constant
5.7000000000000002
Stability:
Stable. Combustible. Incompatible with strong oxidizing agents. May form peroxides on exposure to air - test for their presence before heating.
InChIKey
RRQYJINTUHWNHW-UHFFFAOYSA-N
LogP
0.39 at 25℃
CAS DataBase Reference
112-36-7(CAS DataBase Reference)
NIST Chemistry Reference
Ethane, 1,1'-oxybis[2-ethoxy-(112-36-7)
EPA Substance Registry System
Diethylene glycol diethyl ether (112-36-7)
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Safety

Hazard Codes 
Xi
Risk Statements 
36-19
Safety Statements 
26-36
WGK Germany 
2
RTECS 
KN3160000
Autoignition Temperature
174 °C
TSCA 
Yes
HS Code 
29091900
Hazardous Substances Data
112-36-7(Hazardous Substances Data)
Toxicity
LD50 orally in rats: 4.97 g/kg (Smyth)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
E4658
Product name
Diethylene glycol diethyl ether
Purity
reagent grade, ≥98%
Packaging
1l
Price
$237
Updated
2024/03/01
Sigma-Aldrich
Product number
E4658
Product name
Diethylene glycol diethyl ether
Purity
reagent grade, ≥98%
Packaging
18L
Price
$1920
Updated
2024/03/01
Sigma-Aldrich
Product number
8.02932
Product name
Diethylene glycol diethyl ether
Purity
for synthesis
Packaging
1L
Price
$158
Updated
2024/03/01
Sigma-Aldrich
Product number
308277
Product name
Diethylene glycol diethyl ether
Purity
for HPLC, ≥99%
Packaging
1l
Price
$195.6
Updated
2024/03/01
Sigma-Aldrich
Product number
8.02932
Product name
Diethylene glycol diethyl ether
Purity
for synthesis
Packaging
250ML
Price
$53.1
Updated
2023/06/20
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Diethylene glycol diethyl ether Chemical Properties,Usage,Production

Uses

Diethylene Glycol Diethyl Ether is a very useful organic solvent. It has a high boiling point and has been used to study the activities of enzymes in aqueous organic mixtures.

Description

Diethylene glycol diethyl ether, or 2-Ethoxyethyl ether, is an organic solvent used to study the activities of enzymes in aqueous organic mixtures. Diethylene glycol diethyl ether is a solvent for reactions performed at higher temperatures. It is involved in the preparation of nitrocellulose, resins, and adhesives. It is a scrubbing medium to absorb carbonyl sulfide (COS), an impurity in petroleum refineries. It could be used as an absorbent for CO2. This absorbent has a high boiling point (462 K, in SciFinder), indicating that energy for absorbent regeneration and loss were saved. In addition, this absorbent is chemically and thermally stable, non-corrosive, and has low density and viscosity. It is rich in philic-CO2 groups, which makes Diethylene glycol diethyl ether more effective for CO2 capture. Li et al. found that carbonyl and ether groups in the absorbents improved CO2 solubility, and the carbonyl group was more effective than the ether group[1].

Chemical Properties

colourless liquid

Uses

Solvent; high boiling reaction medium.

Preparation

2-Ethoxyethyl ether could be synthesized by reacting 1, 4-dioxane with diethyl ether. ZSM-5-type zeolite was used as the catalyst. This reaction is performed in an autoclave.

Definition

ChEBI: A polyether that consists of undecane in which the carbon atoms at positions 3, 6 and 9 are replaced by oxygen atoms.

General Description

Clear colorless viscous liquid.

Air & Water Reactions

Highly flammable. May be sensitive to prolonged exposure to air. Can form explosive peroxides. Vapor-air mixtures are explosive above the flash point. Water soluble.

Reactivity Profile

2-Ethoxyethyl ether is incompatible with strong acids. 2-Ethoxyethyl ether is also incompatible with strong oxidizing agents.

Fire Hazard

2-Ethoxyethyl ether is combustible.

Safety Profile

Moderately toxic by ingestion. An experimental teratogen. Other experimental reproductive effects. An eye irritant. Flammable when exposed to heat or flame. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS.

Purification Methods

Dry the ether with MgSO4, then CaH2 or LiAlH4, under N2. If sodium is used, the ether should be redistilled alone to remove any products which may be formed by the action of sodium on the ether. As a preliminary purification, the crude ether (2L) can be refluxed for 12hours with 25mL of conc HCl in 200mL of water, under reduced pressure, with slow passage of N2 to remove aldehydes and other volatile substances. After cooling, add sufficient solid KOH pellets (slowly and with shaking until no more dissolves) to give two liquid phases. The upper of these is decanted, dried with fresh KOH pellets, decanted, then refluxed over, and distilled from sodium. It can be passed through (alkaline) alumina prior to purification. [Beilstein 1 IV 2394.]

References

[1] Yun Li. “Solubilities of CO2 capture absorbents 2-ethoxyethyl ether, 2-butoxyethyl acetate and 2-(2-ethoxyethoxy)ethyl acetate.” Fluid Phase Equilibria 370 (2014): Pages 1-7.

Diethylene glycol diethyl ether Preparation Products And Raw materials

Raw materials

Preparation Products

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Diethylene glycol diethyl ether Suppliers

Anhui Lixing Chemical Co., Ltd.
Tel
+86-0563-8152601 +86-13805622345
Fax
0563-8167310
Email
zhlh@lixingchem.com
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China
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Shanghai Demao Chemical Co.,Ltd.
Tel
+86-021-35121141 18019063037
Email
sh@demchem.com
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China
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243
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Shanghai Boyle Chemical Co., Ltd.
Tel
021-50182298 021-50180596
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+86-21-57758967
Email
sales@boylechem.com
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China
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J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
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China
ProdList
94657
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Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
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40228
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Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
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TCI (Shanghai) Development Co., Ltd.
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021-67121386
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021-67121385
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Sales-CN@TCIchemicals.com
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China
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Beijing HwrkChemical Technology Co., Ltd
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010-89508211 18501085097
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010-89508210
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sales.bj@hwrkchemical.com
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China
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Energy Chemical
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021-021-58432009 400-005-6266
Fax
021-58436166
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sales8178@energy-chemical.com
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China
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Beijing Ouhe Technology Co., Ltd
Tel
010-82967028 13552068683
Fax
+86-10-82967029
Email
2355560935@qq.com
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China
ProdList
12390
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View Lastest Price from Diethylene glycol diethyl ether manufacturers

Speranza Chemical Co., Ltd.
Product
diethylene glycol diethyl ether,99% 112-36-7
Price
US $20.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200 tons/ year
Release date
2020-03-11
Changde Changlian Chemical Co., Ltd.
Product
2-Ethoxyethyl ether 112-36-7
Price
US $0.00/Kg/Drum
Min. Order
1000KG
Purity
99
Supply Ability
10000kg
Release date
2021-09-14
Anhui Royal Chemical Co., Ltd.
Product
2-ETHOXYETHYL ETHER 112-36-7
Price
US $1330.00/kg
Min. Order
900kg
Purity
99%
Supply Ability
10 tons
Release date
2024-04-24

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