D-CYCLOHEXYLGLYCINOL

Product Name: D-CYCLOHEXYLGLYCINOL
CAS No.: 85711-13-3
Chemical Name: D-CYCLOHEXYLGLYCINOL
Synonyms: D-Chg-OL;H-D-CHG-OL;D-CYCLOHEXYLGLYCINOL;(R)-CYCLOHEXYLGLYCINOL;-2-Amino-2-cyclohexylethanol;D-2-aMino-2-cyclohexyl-ethanol;R-2-AMINO-2-CYCLOHEXANEETHANOL;D-CYCLOHEXYLGLYCINOL USP/EP/BP;(R)-2-AMINO-2-CYCLOHEXYL-ETHANOL;(2R)-2-amino-2-cyclohexyl-ethanol
CBNumber: CB4733940
Molecular Formula: C8H17NO
Formula Weight: 143.23
MOL File: 85711-13-3.mol

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D-CYCLOHEXYLGLYCINOL Property

Melting point:: 72-74℃
Boiling point:: 274℃
Density: 0.999
Flash point:: 119℃
storage temp.: Keep in dark place,Inert atmosphere,2-8°C
pka: 12.85±0.10(Predicted)
Appearance: White to yellow Solid
InChI: InChI=1/C8H17NO/c9-8(6-10)7-4-2-1-3-5-7/h7-8,10H,1-6,9H2/t8-/s3
InChIKey: VJJORIDDPKCJTI-SBYBRXNCNA-N
SMILES: [C@@H](CO)(N)C1CCCCC1 |&1:0,r|

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Safety

Risk Statements: 36
Safety Statements: 26
HS Code: 2906190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P233Keep container tightly closed.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P309+P311IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: C986170
Product name: D-Cyclohexylglycinol
Packaging: 50mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC56309
Product name: D-Cyclohexylglycinol
Packaging: 1g
Price: $90
Updated: 2021/12/16

Chem-Impex

Product number: 16574
Product name: D-Cyclohexylglycinol,97%(NMR)
Purity: 97%(NMR)
Packaging: 250MG
Price: $98.56
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC56309
Product name: D-Cyclohexylglycinol
Packaging: 2g
Price: $125
Updated: 2021/12/16

AK Scientific

Product number: J94613
Product name: D-Cyclohexylglycinol
Packaging: 1g
Price: $150
Updated: 2021/12/16

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D-CYCLOHEXYLGLYCINOL Chemical Properties,Usage,Production

Synthesis

14328-52-0

85711-13-3

Step 1: D-cyclohexylglycine (1 g, 6.36 mmol) was added batchwise to a stirred suspension of anhydrous tetrahydrofuran (THF, 20 mL) of lithium aluminum hydride (LiAlH4, 724 mg, 19.08 mmol) at room temperature. The reaction mixture was heated to 80 °C and kept for 4 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and then water (1 mL), 1 M aqueous sodium hydroxide (NaOH) (1 mL) and water (3 mL) were added slowly in sequence to quench the reaction. The mixture was filtered and the filtrate was extracted by partitioning with dichloromethane (DCM), 1 M aqueous NaOH and saturated aqueous sodium potassium tartrate. The organic phase was separated and further washed with 1 M NaOH aqueous solution. The organic phase was dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to afford the crude product (R)-2-amino-2-cyclohexylethanol (400 mg) without further purification. It was detected by liquid chromatography-mass spectrometry (LCMS, ESI) at m/z 144 ([M + H]+).

References

[1] Chemische Berichte, 1986, vol. 119, # 7, p. 2191 - 2207
[2] Journal of Organic Chemistry, 1983, vol. 48, # 13, p. 2195 - 2202
[3] Patent: EP2766359, 2016, B1. Location in patent: Paragraph 0536

D-CYCLOHEXYLGLYCINOL Preparation Products And Raw materials

Raw materials

Preparation Products

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D-CYCLOHEXYLGLYCINOL Suppliers

Canada 1 China 81 Germany 1 India 2 Japan 2 United Kingdom 3 United States 10 Global 100

ShangHai DEMO Chemical Co.,Ltd

Tel: 400-021-7337 2355568890
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Daicel Chiral Technologies (China)CO.,LTD

Tel: 021-50460086-9 15921403865
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9ding chemical ( Shanghai) Limited

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TAIZHOU TIANHONG BIOCHEMICALS CO., LTD

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Email: thbiochem@126.com
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Amatek Scientific Co. Ltd.

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Bide Pharmatech Ltd.

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Wuxi Zhongkun Biochemical Technology Co., Ltd.

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Shandong Welt Chem. Co .Ltd

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Nanjing Derno Pharmaceutical Technology Co., Ltd.

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View Lastest Price from D-CYCLOHEXYLGLYCINOL manufacturers

Sichuan HongRi Pharma-Tech Co.,Ltd

Product: D-Chg-OL 85711-13-3
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1T+
Release date: 2024-01-18

Sichuan Jiaying Lai Technology Co.,LTD

Product: D-Chg-OL 85711-13-3
Price: US $1.00/g
Min. Order: 1g
Purity: 98%
Supply Ability: 100KG
Release date: 2019-07-23

Career Henan Chemical Co

Product: D-CYCLOHEXYLGLYCINOL 85711-13-3
Price: US $500.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 10tons
Release date: 2018-08-04

85711-13-3, D-CYCLOHEXYLGLYCINOLRelated Search:

FMOC-D-CHG-OH FMOC-CHG-OH N-BOC-D-CYCLOHEXYLGLYCINOL,BOC-D-CYCLOHEXYLGLYCINOL,N-T-BUTOXYCARBONYL-D-CYCLOHEXYLGLYCINOL,N-T-BOC-D-CYCLOHEXYLGLYCINOL Z-D-PHG-OH D-alpha-Cyclohexylglycine Boc-alpha-Cyclohexyl-D-glycine N-BOC-L-CYCLOHEXYLGLYCINOL,N-T-BUTOXYCARBONYL-L-CYCLOHEXYLGLYCINOL,N-T-BOC-L-CYCLOHEXYLGLYCINOL SR 48692 SR142948 D-CYCLOHEXYLGLYCINOL (S)-CYCLOHEXYLGLYCINOL,L-CYCLOHEXYLGLYCINOL BOC-L-CYCLOHEXYLGLYCINOL Cilobamine N-CARBOBENZOXY-D-CYCLOHEXYLGLYCINOL methyl 1-adamantyl(amino)acetate (R)-N-BOC-2-AMINO-2-CYCLOHEXYL-PROPANOIC ACID IFLAB-BB F1913-0002 Acetyl 2-aminoadamantane-2-carboxylic acid

(R)-CYCLOHEXYLGLYCINOL

R-2-AMINO-2-CYCLOHEXANEETHANOL

(R)-2-AMINO-2-CYCLOHEXYL-ETHANOL

H-D-CHG-OL

D-CYCLOHEXYLGLYCINOL

(R)-2-2-Amino-2-Cyclohexyl-Ethanol

D-Chg-OL

(R)-(-)-2-Amino-2-cyclohexylethan-1-ol

D-2-aMino-2-cyclohexyl-ethanol

(R)-b-AMino-cyclohexaneethanol HCl

(2R)-2-amino-2-cyclohexyl-ethanol

-2-Amino-2-cyclohexylethanol

Cyclohexaneethanol, β-amino-, (βR)-

(R)-b-Amino-cyclohexaneethanol hydrochloride

D-CYCLOHEXYLGLYCINOL USP/EP/BP

(R)-beta-amino-Cyclohexaneethanol

(R)-2-Amino-2-cyclohexylethan-1-ol - [A90928]

85711-13-3

pharmacetical

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