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D-CYCLOHEXYLGLYCINOL

Product Name
D-CYCLOHEXYLGLYCINOL
CAS No.
85711-13-3
Chemical Name
D-CYCLOHEXYLGLYCINOL
Synonyms
D-Chg-OL;H-D-CHG-OL;D-CYCLOHEXYLGLYCINOL;(R)-CYCLOHEXYLGLYCINOL;-2-Amino-2-cyclohexylethanol;D-2-aMino-2-cyclohexyl-ethanol;R-2-AMINO-2-CYCLOHEXANEETHANOL;D-CYCLOHEXYLGLYCINOL USP/EP/BP;(R)-2-AMINO-2-CYCLOHEXYL-ETHANOL;(2R)-2-amino-2-cyclohexyl-ethanol
CBNumber
CB4733940
Molecular Formula
C8H17NO
Formula Weight
143.23
MOL File
85711-13-3.mol
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D-CYCLOHEXYLGLYCINOL Property

Melting point:
72-74℃
Boiling point:
274℃
Density 
0.999
Flash point:
119℃
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
pka
12.85±0.10(Predicted)
Appearance
White to yellow Solid
InChI
InChI=1/C8H17NO/c9-8(6-10)7-4-2-1-3-5-7/h7-8,10H,1-6,9H2/t8-/s3
InChIKey
VJJORIDDPKCJTI-SBYBRXNCNA-N
SMILES
[C@@H](CO)(N)C1CCCCC1 |&1:0,r|
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Safety

Risk Statements 
36
Safety Statements 
26
HS Code 
2906190090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P233Keep container tightly closed.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P309+P311IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC
Product number
C986170
Product name
D-Cyclohexylglycinol
Packaging
50mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC56309
Product name
D-Cyclohexylglycinol
Packaging
1g
Price
$90
Updated
2021/12/16
Chem-Impex
Product number
16574
Product name
D-Cyclohexylglycinol,97%(NMR)
Purity
97%(NMR)
Packaging
250MG
Price
$98.56
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC56309
Product name
D-Cyclohexylglycinol
Packaging
2g
Price
$125
Updated
2021/12/16
AK Scientific
Product number
J94613
Product name
D-Cyclohexylglycinol
Packaging
1g
Price
$150
Updated
2021/12/16
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D-CYCLOHEXYLGLYCINOL Chemical Properties,Usage,Production

Synthesis

14328-52-0

85711-13-3

Step 1: D-cyclohexylglycine (1 g, 6.36 mmol) was added batchwise to a stirred suspension of anhydrous tetrahydrofuran (THF, 20 mL) of lithium aluminum hydride (LiAlH4, 724 mg, 19.08 mmol) at room temperature. The reaction mixture was heated to 80 °C and kept for 4 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and then water (1 mL), 1 M aqueous sodium hydroxide (NaOH) (1 mL) and water (3 mL) were added slowly in sequence to quench the reaction. The mixture was filtered and the filtrate was extracted by partitioning with dichloromethane (DCM), 1 M aqueous NaOH and saturated aqueous sodium potassium tartrate. The organic phase was separated and further washed with 1 M NaOH aqueous solution. The organic phase was dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to afford the crude product (R)-2-amino-2-cyclohexylethanol (400 mg) without further purification. It was detected by liquid chromatography-mass spectrometry (LCMS, ESI) at m/z 144 ([M + H]+).

References

[1] Chemische Berichte, 1986, vol. 119, # 7, p. 2191 - 2207
[2] Journal of Organic Chemistry, 1983, vol. 48, # 13, p. 2195 - 2202
[3] Patent: EP2766359, 2016, B1. Location in patent: Paragraph 0536

D-CYCLOHEXYLGLYCINOL Preparation Products And Raw materials

Raw materials

Preparation Products

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D-CYCLOHEXYLGLYCINOL Suppliers

Canada 1 China 81 Germany 1 India 2 Japan 2 United Kingdom 3 United States 10 Global 100
Service Chemical Inc.
Tel
--
Fax
--
Email
sales@chemos-group.com
Country
Germany
ProdList
6350
Advantage
71
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View Lastest Price from D-CYCLOHEXYLGLYCINOL manufacturers

Sichuan HongRi Pharma-Tech Co.,Ltd
Product
D-Chg-OL 85711-13-3
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1T+
Release date
2024-01-18
Sichuan Jiaying Lai Technology Co.,LTD
Product
D-Chg-OL 85711-13-3
Price
US $1.00/g
Min. Order
1g
Purity
98%
Supply Ability
100KG
Release date
2019-07-23
Career Henan Chemical Co
Product
D-CYCLOHEXYLGLYCINOL 85711-13-3
Price
US $500.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
10tons
Release date
2018-08-04

85711-13-3, D-CYCLOHEXYLGLYCINOLRelated Search:

FMOC-D-CHG-OH FMOC-CHG-OH N-BOC-D-CYCLOHEXYLGLYCINOL,BOC-D-CYCLOHEXYLGLYCINOL,N-T-BUTOXYCARBONYL-D-CYCLOHEXYLGLYCINOL,N-T-BOC-D-CYCLOHEXYLGLYCINOL Z-D-PHG-OH D-alpha-Cyclohexylglycine Boc-alpha-Cyclohexyl-D-glycine N-BOC-L-CYCLOHEXYLGLYCINOL,N-T-BUTOXYCARBONYL-L-CYCLOHEXYLGLYCINOL,N-T-BOC-L-CYCLOHEXYLGLYCINOL SR 48692 SR142948 D-CYCLOHEXYLGLYCINOL (S)-CYCLOHEXYLGLYCINOL,L-CYCLOHEXYLGLYCINOL BOC-L-CYCLOHEXYLGLYCINOL Cilobamine N-CARBOBENZOXY-D-CYCLOHEXYLGLYCINOL methyl 1-adamantyl(amino)acetate (R)-N-BOC-2-AMINO-2-CYCLOHEXYL-PROPANOIC ACID IFLAB-BB F1913-0002 Acetyl 2-aminoadamantane-2-carboxylic acid

  • (R)-CYCLOHEXYLGLYCINOL
  • R-2-AMINO-2-CYCLOHEXANEETHANOL
  • (R)-2-AMINO-2-CYCLOHEXYL-ETHANOL
  • H-D-CHG-OL
  • D-CYCLOHEXYLGLYCINOL
  • (R)-2-2-Amino-2-Cyclohexyl-Ethanol
  • D-Chg-OL
  • (R)-(-)-2-Amino-2-cyclohexylethan-1-ol
  • D-2-aMino-2-cyclohexyl-ethanol
  • (R)-b-AMino-cyclohexaneethanol HCl
  • (2R)-2-amino-2-cyclohexyl-ethanol
  • -2-Amino-2-cyclohexylethanol
  • Cyclohexaneethanol, β-amino-, (βR)-
  • (R)-b-Amino-cyclohexaneethanol hydrochloride
  • D-CYCLOHEXYLGLYCINOL USP/EP/BP
  • (R)-beta-amino-Cyclohexaneethanol
  • (R)-2-Amino-2-cyclohexylethan-1-ol - [A90928]
  • 85711-13-3
  • pharmacetical
  • Peptide