ChemicalBook > CAS DataBase List > 2,3-Dibromo-5-chloropyridine
2,3-Dibromo-5-chloropyridine
- Product Name
- 2,3-Dibromo-5-chloropyridine
- CAS No.
- 137628-17-2
- Chemical Name
- 2,3-Dibromo-5-chloropyridine
- Synonyms
- 2,3-Dibromo-5-chL;7-Bromopicolinic acid;Atogepant Impurity 25;3-Dibromo-5-chloropyridine;5-CHLORO-2,3-DIBROMOPYRIDINE;2,3 DIBROMO-5-CHLORO PYRIDINE;2,3-DIBROMO-5-DICHLOROPYRIDINE;Pyridine, 2,3-dibromo-5-chloro-;2,3-Dibromo-5-chloropyridine>2,3-Dibromo-5-chloropyridine 98%
- CBNumber
- CB4843265
- Molecular Formula
- C5H2Br2ClN
- Formula Weight
- 271.34
- MOL File
- 137628-17-2.mol
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2,3-Dibromo-5-chloropyridine Property
- Melting point:
- 41.0 to 45.0 °C
- Boiling point:
- 259.9±35.0 °C(Predicted)
- Density
- 2.136±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- -3.85±0.20(Predicted)
- color
- White to Light yellow to Light orange
- InChI
- InChI=1S/C5H2Br2ClN/c6-4-1-3(8)2-9-5(4)7/h1-2H
- InChIKey
- GDUFWKJMOOVEMX-UHFFFAOYSA-N
- SMILES
- C1(Br)=NC=C(Cl)C=C1Br
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Safety
- Hazard Codes
- Xi,T
- Risk Statements
- 36/37/38-25
- Safety Statements
- 26-37-45
- RIDADR
- UN 2811 6.1 / PGIII
- HazardClass
- IRRITANT
- HS Code
- 2933399990
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N-Bromosuccinimide Price
TCI Chemical
- Product number
- D4381
- Product name
- 2,3-Dibromo-5-chloropyridine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $35
- Updated
- 2024/03/01
TCI Chemical
- Product number
- D4381
- Product name
- 2,3-Dibromo-5-chloropyridine
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $152
- Updated
- 2024/03/01
TRC
- Product number
- D425215
- Product name
- 2,3-Dibromo-5-chloropyridine
- Packaging
- 25g
- Price
- $275
- Updated
- 2021/12/16
TRC
- Product number
- D425215
- Product name
- 2,3-Dibromo-5-chloropyridine
- Packaging
- 5G
- Price
- $220
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD75498
- Product name
- 2,3-Dibromo-5-chloropyridine
- Packaging
- 50g
- Price
- $632.5
- Updated
- 2021/12/16
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2,3-Dibromo-5-chloropyridine Chemical Properties,Usage,Production
Uses
2,3-Dibromo-5-chloropyridine has been used as a reactant for regiospecific Grignard reactions with lactones.
Synthesis
3-Bromo-5-chloropyridone (8.0 g, 38.4 mmole) was dissolved in dimethylformamide (60 ml) at ambient temperature. Phosphorus (V) tribromide oxide (16.5 g, 57.6 mmoles) was added and the reaction heated to 80° C for 72 hours. After cooling, the reaction was poured onto 800 g of ice. Vacuum filtration provided the product as a dark solid (6.85 g). Hexane (225 ml) and decolorizing carbon was added to the crude product and the contents heated to reflux and then filtered through celite. The clear colorless filtrate was stripped under vacuum to yield 2,3-Dibromo-5-chloropyridine as a white solid (5.3 g, 51%).
2,3-Dibromo-5-chloropyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,3-Dibromo-5-chloropyridine manufacturers
Henan Fengda Chemical Co., Ltd
- Product
- 2,3-Dibromo-5-chloropyridine 137628-17-2
- Price
- US $8.00-0.80/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-22
Shaanxi Dideu Medichem Co. Ltd
- Product
- 2,3-DibroMo-5-chloropyridine 137628-17-2
- Price
- US $1.00/Kg
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2019-12-26
Shaanxi Dideu Medichem Co. Ltd
- Product
- 5-CHLORO-2,3-DIBROMOPYRIDINE 137638-17-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2019-12-30
137628-17-2, 2,3-Dibromo-5-chloropyridineRelated Search:
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