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4-NITRO-1-PHENYLIMIDAZOLE

Product Name
4-NITRO-1-PHENYLIMIDAZOLE
CAS No.
41384-83-2
Chemical Name
4-NITRO-1-PHENYLIMIDAZOLE
Synonyms
4-NITRO-1-PHENYLIMIDAZOLE;4-nitro-1-phenyl-1H-iMidazole;1H-Imidazole, 4-nitro-1-phenyl-
CBNumber
CB4849843
Molecular Formula
C9H7N3O2
Formula Weight
189.17
MOL File
41384-83-2.mol
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4-NITRO-1-PHENYLIMIDAZOLE Property

Melting point:
187 °C(Solv: methanol (67-56-1))
Boiling point:
374.6±15.0 °C(Predicted)
Density 
1.33±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
-1.24±0.61(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
2786AL
Product name
4-Nitro-1-phenyl-1H-imidazole
Packaging
1g
Price
$358
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0034863
Product name
4-NITRO-1-PHENYLIMIDAZOLE
Purity
95.00%
Packaging
5G
Price
$1357.07
Updated
2021/12/16
Ambeed
Product number
A103958
Product name
4-Nitro-1-phenyl-1H-imidazole
Purity
95%
Packaging
250mg
Price
$70
Updated
2021/12/16
Ambeed
Product number
A103958
Product name
4-Nitro-1-phenyl-1H-imidazole
Purity
95%
Packaging
1g
Price
$189
Updated
2021/12/16
Alichem
Product number
41384832
Product name
4-Nitro-1-phenyl-1h-imidazole
Packaging
1g
Price
$190.16
Updated
2021/12/16
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4-NITRO-1-PHENYLIMIDAZOLE Chemical Properties,Usage,Production

Synthesis

3034-38-6

98-80-6

41384-83-2

1. 1.6 mmol of 4-nitroimidazole (1a-e), 2.6 mmol of phenylboronic acid (2a-n), 1.6 mmol of sodium hydroxide, 0.2 mmol of CuCl2 and 15 mL of methanol were added to the reaction flask. 2. The reaction mixture was heated and refluxed under air bulge conditions. 3. The progress of the reaction was monitored by TLC, and after completion of the reaction the solvent was removed under reduced pressure using a rotary evaporator to remove the solvent under reduced pressure.4. The crude product was purified by silica gel column chromatography using 5:95 (v/v) methanol/chloroform as eluent to obtain the target product 4-nitro-1-phenylimidazole.5. The final product was purified by crystallization through a solvent mixture of methanol/water.

References

[1] Beilstein Journal of Organic Chemistry, 2013, vol. 9, p. 1517 - 1525
[2] Patent: WO2017/109488, 2017, A1. Location in patent: Page/Page column 41
[3] Patent: WO2018/65768, 2018, A1. Location in patent: Page/Page column 89

4-NITRO-1-PHENYLIMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-NITRO-1-PHENYLIMIDAZOLE Suppliers

China 26 India 2 United States 6 Global 34
Synthonix Inc
Tel
--
Fax
--
Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
AlliChem, LLC
Tel
--
Fax
--
Email
sales@allichemllc.com
Country
United States
ProdList
6516
Advantage
60
3B Scientific Corporation
Tel
--
Fax
--
Email
sales@3bsc.com
Country
United States
ProdList
6718
Advantage
47
APAC Pharmaceutical, LLC
Tel
--
Fax
--
Email
sales@apacpharma.com
Country
United States
ProdList
6322
Advantage
38
ChemPacific Corporation
Tel
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Fax
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Email
sales@chempacific.com
Country
United States
ProdList
6891
Advantage
51

41384-83-2, 4-NITRO-1-PHENYLIMIDAZOLERelated Search:

Imipenem 1-Phenylimidazole Nitrefazole 6,8-DIMETHOXY-3-NITROIMIDAZO[5,1-C][1,2,4]BENZOTRIAZINE 4-NITRO-1-PHENYLIMIDAZOLE

  • 4-nitro-1-phenyl-1H-iMidazole
  • 4-NITRO-1-PHENYLIMIDAZOLE
  • 1H-Imidazole, 4-nitro-1-phenyl-
  • 41384-83-2