thiomorpholin-3-one

Product Name: thiomorpholin-3-one
CAS No.: 20196-21-8
Chemical Name: thiomorpholin-3-one
Synonyms: THIOMORPHOLINONE;hiomorpholin-3-one;3-Thiomorpholinone;thiomorpholin-3-one
CBNumber: CB4891781
Molecular Formula: C4H7NOS
Formula Weight: 117.17
MOL File: 20196-21-8.mol

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thiomorpholin-3-one Property

Melting point:: 87-89 °C(Solv: ethyl acetate (141-78-6))
Boiling point:: 185 °C(Press: 18 Torr)
Density: 1.189±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 14.19±0.20(Predicted)
Appearance: Light yellow to yellow Solid
LogP: 0.059 (est)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: B585710
Product name: Thiomorpholin-3-one
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: B585710
Product name: Thiomorpholin-3-one
Packaging: 500mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: B143
Product name: Thiomorpholin-3-one
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: B143
Product name: Thiomorpholin-3-one
Packaging: 5g
Price: $240
Updated: 2021/12/16

Matrix Scientific

Product number: 135718
Product name: Thiomorpholin-3-one
Purity: 95%+
Packaging: 1g
Price: $332
Updated: 2021/12/16

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thiomorpholin-3-one Chemical Properties,Usage,Production

Synthesis

105-39-5

60-23-1

20196-21-8

To a mixed solution of 2-aminoethane-1-thiol (4.5 g, 40 mmol, 1.0 eq.) and potassium carbonate (K2CO3, 5.5 g, 40 mmol, 1.0 eq.) in ethanol (EtOH, 80 mL) was slowly added ethyl chloroacetate (40 mmol, 1.0 eq.). The reaction mixture was stirred at room temperature for 2 hours, followed by warming to 75 °C and continued stirring for 24 hours. Upon completion of the reaction, the insoluble material was removed by filtration and all volatile solvents were removed by rotary evaporator under reduced pressure. The crude product was purified by fast column chromatography (silica gel, ethyl acetate as eluent) to give the final thiomorpholin-3-one as a white solid in 18% yield.

References

[1] Tetrahedron, 2015, vol. 71, # 37, p. 6349 - 6353

thiomorpholin-3-one Preparation Products And Raw materials

Raw materials

Preparation Products

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thiomorpholin-3-one Suppliers

China 41 Germany 1 India 1 Ukraine 1 United States 8 Global 52

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View Lastest Price from thiomorpholin-3-one manufacturers

Career Henan Chemical Co

Product: thiomorpholin-3-one 20196-21-8
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-02-13

20196-21-8, thiomorpholin-3-oneRelated Search:

Thiomorpholine DIETHYL METHYLTHIOMETHYLPHOSPHONATE ThioMorpholine-1-oxide HCl Thiomorpholine-1,1-dioxide THIOMORPHOLINE 1,1-DIOXIDE HYDROCHLORIDE thiomorpholin-3-one 2-PHENYLTHIOMORPHOLIN-3-ONE Phenythilone 4-(2,4-DICHLOROPHENYL)-3,5-THIOMORPHOLINEDIONE 4-(2,4-DIFLUOROPHENYL)-3,5-THIOMORPHOLINEDIONE 4-(4-CHLOROPHENYL)-1LAMBDA4,4-THIAZINANE-1,3,5-TRIONE 4-(3,4-DICHLOROPHENYL)-3,5-THIOMORPHOLINEDIONE 4-(4-METHYLPHENYL)-3,5-THIOMORPHOLINEDIONE 4-(3,4-DICHLOROPHENYL)-1LAMBDA4,4-THIAZINANE-1,3,5-TRIONE 4-(4-METHOXYPHENYL)-1LAMBDA4,4-THIAZINANE-1,3,5-TRIONE 4-(3-CHLOROPHENYL)-3,5-THIOMORPHOLINEDIONE 4-(4-METHYLPHENYL)-1LAMBDA4,4-THIAZINANE-1,3,5-TRIONE 4-PHENYL-3,5-THIOMORPHOLINEDIONE

thiomorpholin-3-one

THIOMORPHOLINONE

3-Thiomorpholinone

hiomorpholin-3-one

20196-21-8