Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI)
- Product Name
- Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI)
- CAS No.
- 5262-63-5
- Chemical Name
- Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI)
- Synonyms
- 2,4-Dimethyl-benzthiazol;2,4-Dimethylbenzothiazole;2,4-DiMethylbenzo[d]thiazole;Benzothiazole, 2,4-dimethyl-;2,4-dimethyl-1,3-benzothiazole;Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI)
- CBNumber
- CB51050803
- Molecular Formula
- C9H9NS
- Formula Weight
- 163.24
- MOL File
- 5262-63-5.mol
Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) Property
- Melting point:
- 33-34 °C
- Boiling point:
- 128-130 °C(Press: 20 Torr)
- Density
- 1.176±0.06 g/cm3(Predicted)
- pka
- 2.19±0.10(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D476730
- Product name
- 2,4-Dimethyl-benzothiazole
- Packaging
- 1g
- Price
- $120
- Updated
- 2021/12/16
- Product number
- D476730
- Product name
- 2,4-Dimethyl-benzothiazole
- Packaging
- 25g
- Price
- $1090
- Updated
- 2021/12/16
- Product number
- CHM0297798
- Product name
- 2,4-DIMETHYLBENZOTHIAZOLE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.37
- Updated
- 2021/12/16
- Product number
- 7440AB
- Product name
- 2,4-Dimethylbenzo[d]thiazole
- Packaging
- 5g
- Price
- $529
- Updated
- 2021/12/16
- Product number
- AA00DHGX
- Product name
- 2,4-Dimethylbenzo[d]thiazole
- Purity
- 95%
- Packaging
- 250mg
- Price
- $81
- Updated
- 2021/12/16
Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) Chemical Properties,Usage,Production
Chemical Properties
White solid
Uses
2,4-Dimethyl-benzothiazole, is used in the preparation of quaternary salts of chalcogenites as photographic sensitizers.
Synthesis
35274-15-8
5262-63-5
[Step 2] Potassium hexacyanoferrate(III) (22.1 g) was mixed with water (35 mL), and a mixture of N-(2-methylphenyl)ethylthioamide (6.60 g), sodium hydroxide (3.69 g), and water (50 mL) made in Step 1 was added. The reaction system was stirred at 40°C for 2 hours. After completion of the reaction, it was cooled to room temperature and extracted twice with ethyl acetate (50 mL). The organic phases were combined, washed with saturated saline (50 mL), dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford 2,4-dimethylbenzothiazole (Compound 13) (2.82 g). The 1H-NMR (CDCl3) data of compound 13 were as follows: δ 7.66 (m, 1H), 7.24 (m, 2H), 2.85 (s, 3H), 2.73 (s, 3H).
References
[1] Bulletin de la Societe Chimique de France, 1956, p. 684,688
[2] Zhurnal Obshchei Khimii, 1957, vol. 27, p. 3097,3103, 1305;engl. Ausg. S. 3138, 3143, 3144
[3] Yakugaku Zasshi, 1950, vol. 70, p. 540
[4] Chem.Abstr., 1951, p. 7111
[5] Patent: WO2015/194676, 2015, A1. Location in patent: Paragraph 0034
Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) manufacturers
- Product
- Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) 5262-63-5
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-12-25
- Product
- Benzothiazole, 2,4-dimethyl- (6CI,7CI,8CI,9CI) 5262-63-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 97-99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-18