Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI)
- Product Name
- Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI)
- CAS No.
- 84331-14-6
- Chemical Name
- Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI)
- Synonyms
- 5-Acetyl-2-fluoropyridine;5-Acethyl-2-fluoropyridine;1-(6-Fluoro-3-pyridyl)ethanone;1-(6-Fluoro-3-pyridinyl)-ethanone;Ethanone, 1-(6-fluoro-3-pyridinyl)-;1-(6-Fluoropyridin-3-yl)ethanone 95+%;Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI);Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) ISO 9001：2015 REACH
- CBNumber
- CB51063746
- Molecular Formula
- C7H6FNO
- Formula Weight
- 139.13
- MOL File
- 84331-14-6.mol
Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) Property
- Boiling point:
- 246.7±20.0℃ (760 Torr)
- Density
- 1.175±0.06 g/cm3 (20 ºC 760 Torr)
- Flash point:
- 103.0±21.8℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -2.23±0.10(Predicted)
- Appearance
- White to light yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- F596318
- Product name
- 1-(6-Fluoropyridin-3-yl)ethanone
- Packaging
- 25mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- PC404005
- Product name
- 1-(6-Fluoropyridin-3-yl)ethanone
- Purity
- 95+%
- Packaging
- 1g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- Y14604
- Product name
- 5-Acetyl-2-fluoropyridine
- Packaging
- 5g
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 076427
- Product name
- 1-(6-Fluoropyridin-3-yl)ethanone
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $416
- Updated
- 2021/12/16
- Product number
- HCH0353872
- Product name
- 1-(6-FLUOROPYRIDIN-3-YL)ETHANONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.55
- Updated
- 2021/12/16
Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) Chemical Properties,Usage,Production
Synthesis
774239-06-4
75-16-1
84331-14-6
To a cold solution (-78°C) of 6-fluoro-N-methoxy-N-methylnicotinamide (Method 38, 7.2 g, 39 mmol) in tetrahydrofuran (130 mL) was added slowly and dropwise methylmagnesium bromide (20 mL, 59 mmol, 3 M ether solution). The cooling bath was removed and the reaction mixture was allowed to gradually warm to room temperature with continuous stirring for 2 hours. Upon completion of the reaction, the reaction was quenched with 3 N hydrochloric acid solution and the layers were separated. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 3.8 g of 2-fluoro-5-acetylpyridine in 70% yield. The product was characterized by 1H NMR (CDCl3): δ 8.80 (s, 1H), 8.29-8.43 (m, 1H), 6.98-7.06 (m, 1H), 2.62 (s, 3H).
References
[1] Patent: WO2006/82392, 2006, A1. Location in patent: Page/Page column 116
[2] Patent: US2017/313683, 2017, A1. Location in patent: Paragraph 1251-1252
Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) manufacturers
- Product
- Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) 84331-14-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-19
- Product
- Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) 84331-14-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2019-12-25
- Product
- Ethanone, 1-(6-fluoro-3-pyridinyl)- (9CI) 84331-14-6
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-11-20