ChemicalBook > CAS DataBase List > 2-METHOXY-3-AMINO-4-PICOLINE

2-METHOXY-3-AMINO-4-PICOLINE

Product Name
2-METHOXY-3-AMINO-4-PICOLINE
CAS No.
76005-99-7
Chemical Name
2-METHOXY-3-AMINO-4-PICOLINE
Synonyms
2-METHOXY-3-AMINO-4-PICOLINE;2-Methoxy-4-Methylpyridin-3-aMine;2-Methoxy-4-methyl-3-pyridinamine;2-Methoxy-3-amino-4-methylpyridine;3-PyridinaMine, 2-Methoxy-4-Methyl-;2-Methoxy-4-methyl-pyridin-3-ylamine;2-METHOXY-3-AMINO-4-PICOLINE ISO 9001：2015 REACH
CBNumber
CB51076119
Molecular Formula
C7H10N2O
Formula Weight
138.17
MOL File
76005-99-7.mol
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2-METHOXY-3-AMINO-4-PICOLINE Property

Boiling point:
265℃
Density 
1.103
Flash point:
114℃
storage temp. 
Keep in dark place,Sealed in dry,Store in freezer, under -20°C
pka
4.99±0.18(Predicted)
Appearance
Light brown to brown Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M218958
Product name
2-Methoxy-4-methylpyridin-3-amine
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
M218958
Product name
2-Methoxy-4-methylpyridin-3-amine
Packaging
500mg
Price
$175
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA55650
Product name
3-Amino-2-methoxy-4-methylpyridine
Packaging
500mg
Price
$200
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA55650
Product name
3-Amino-2-methoxy-4-methylpyridine
Packaging
100mg
Price
$90
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA55650
Product name
3-Amino-2-methoxy-4-methylpyridine
Packaging
250mg
Price
$150
Updated
2021/12/16
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2-METHOXY-3-AMINO-4-PICOLINE Chemical Properties,Usage,Production

Synthesis

160590-36-3

76005-99-7

General procedure for the synthesis of 2-methoxy-3-amino-4-methylpyridine from 2-methoxy-3-nitro-4-methylpyridine: 1. a mixture of 4-methyl-2-methoxy-3-nitropyridine (4.5 g, 26.8 mmol), NH4Cl (7.16 g, 133.9 mmol) and iron powder (7.5 g, 133.9 mmol) in ethanol (50 mL) was stirred at 25°C. 2. the mixture was slowly heated to 90 °C and stirred continuously at that temperature for 2 hours. 3. upon completion of the reaction, the reaction mixture was filtered through a diatomaceous earth plug and the diatomaceous earth plug was washed with ethanol (50 mL). 4. The filtrates were combined and evaporated to dryness. 5. The residue was diluted with water (50 mL) and extracted with EtOAc (100 mL). 6. The organic layer was dried over Na2SO4 and evaporated to dryness to afford 2-methoxy-3-amino-4-methylpyridine as a solid (3.5 g, 81% yield). Product characterization: 1H NMR (CDCl3, 400MHz) δ 7.50-7.49 (1H, d, J = 5.2Hz), 6.62-6.61 (1H, d, J = 5.2Hz), 3.97 (3H, s), 3.79-3.69 (2H, br s), 2.15 (3H, s).

References

[1] Patent: US2013/5743, 2013, A1. Location in patent: Page/Page column 12
[2] Patent: WO2013/4617, 2013, A1. Location in patent: Page/Page column 29
[3] Chemical and Pharmaceutical Bulletin, 2008, vol. 56, # 6, p. 775 - 780

2-METHOXY-3-AMINO-4-PICOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-METHOXY-3-AMINO-4-PICOLINE manufacturers

Dideu Industries Group Limited
Product
2-METHOXY-3-AMINO-4-PICOLINE 76005-99-7
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-31

76005-99-7, 2-METHOXY-3-AMINO-4-PICOLINERelated Search:

2-(3-AMINO-2-METHOXY-6-METHYLPYRIDIN-4-YL)PROPAN-2-OL 2-METHOXY-4-(1-METHOXYVINYL)-6-METHYL-3-NITROPYRIDINE 2-METHOXY-3-AMINO-4-PICOLINE Ethanone, 1-(3-amino-2-methoxy-4-pyridinyl)-2,2,2-trifluoro- (9CI) 2-METHOXY-3-NITRO-4-PICOLINE 2-METHOXY-6-METHYL-3-NITROPYRIDINE-4-CARBOXALDEHYDE 2-METHOXY-3-(BOC-AMINO)-4-TRIFLUORO-ACETYLPYRIDINE 2,5-Dimethoxy-4-methyl-3-nitropyridine 2-METHOXY-3-NITROPYRIDINE-4-CARBOXALDEHYDE 2-METHOXY-4-METHYL-3-NITROPYRIDINE-5-BORONIC ACID PINACOL ESTER 5-Bromo-2-methoxy-4-methyl-3-nitropyridine 3-Amino-2-methoxy-6-methyl-4-pyridinecarboxylicacidethylester

  • 2-METHOXY-3-AMINO-4-PICOLINE
  • 2-Methoxy-4-methyl-3-pyridinamine
  • 2-Methoxy-4-Methylpyridin-3-aMine
  • 3-PyridinaMine, 2-Methoxy-4-Methyl-
  • 2-Methoxy-4-methyl-pyridin-3-ylamine
  • 2-METHOXY-3-AMINO-4-PICOLINE ISO 9001：2015 REACH
  • 2-Methoxy-3-amino-4-methylpyridine
  • 76005-99-7
  • Pyridine