(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE

Product Name: (R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE
CAS No.: 163831-65-0
Chemical Name: (R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE
Synonyms: CicalcetImpurityBHCl;Cinacalcet Impurity B HCl;Cinacalcet Impurity B (HCl salt form);(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMI&;N-benzyl-1-(1-naphthyl)ethylamine hydrochloride;(R)-N-BENZYL 1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE;benzyl-(1-naphthalen-1-yl-ethyl)-amine hydrochloride;(R)-N-[1-(1-NAPHTHYL)ETHYL]BENZYLAMINE HYDROCHLORIDE;(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE;(R)-N-Benzyl-1-(naphthalen-1-yl)ethanamine hydrochloride
CBNumber: CB5125005
Molecular Formula: C19H20ClN
Formula Weight: 297.82
MOL File: 163831-65-0.mol

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(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE Property

Melting point:: 259-261 °C(lit.)
storage temp.: Inert atmosphere,Room Temperature

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 3146CW
Product name: (R)-(-)-N-Benzyl-1-(1-naphthyl)ethylaminehydrochloride
Packaging: 250mg
Price: $149
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CCH0007177
Product name: (R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE
Purity: 95.00%
Packaging: 5MG
Price: $500.12
Updated: 2021/12/16

AK Scientific

Product number: 3146CW
Product name: (R)-(-)-N-Benzyl-1-(1-naphthyl)ethylaminehydrochloride
Packaging: 1g
Price: $281
Updated: 2021/12/16

Crysdot

Product number: CD12135812
Product name: (R)-N-Benzyl-1-(naphthalen-1-yl)ethanaminehydrochloride
Purity: 95+%
Packaging: 250mg
Price: $388
Updated: 2021/12/16

Alichem

Product number: 163831650
Product name: (R)-N-Benzyl-1-(naphthalen-1-yl)ethanaminehydrochloride
Packaging: 250mg
Price: $435.12
Updated: 2021/12/16

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(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

82572-04-1

4657-12-9

163831-65-0

GENERAL METHOD: (R)-1-(1-naphthalenyl)ethylamine hydrochloride (1 mmol) was dissolved in methanol (10 mL), and benzaldehyde sodium bisulfite adduct (1.12 mmol) was added. Sodium cyanoborohydride (NaCNBH3, 2.5 mmol) was slowly added to the resulting suspension and the reaction mixture was stirred at room temperature for 20 hours. After completion of the reaction, the solvent was removed by evaporation to obtain the residue. The residue was partitioned with 5N NaOH solution and ethyl acetate (EtOAc). The aqueous phase was further extracted with EtOAc and the organic phases were combined, dried over anhydrous sodium sulfate and the solvent was evaporated to give the crude product. The crude product was dissolved in ether (Et2O) and treated with 0.6N ether-HCl solution. The resulting suspension was cooled at 0°C for 13 h. The precipitated white solid was collected by filtration and dried in vacuum to afford the target product (R)-N-benzyl-1-(naphthalen-1-yl)ethanamine hydrochloride.

References

[1] Tetrahedron Letters, 2014, vol. 55, # 15, p. 2548 - 2550

(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE Suppliers

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163831-65-0, (R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDERelated Search:

(R)-(+)-1-(1-Naphthyl)ethylamine hydrochloride Cinacalcet IMpurity 7 1-NAPHTHALEN-2-YL-ETHYLAMINE (E)-m-(trifluoromethyl)cinnamic acid Cinacalcet Impurity 38 HCl 4-(TRIFLUOROMETHYL)HYDROCINNAMIC ACID Cinacalcet Impurity B (R)-1-(Naphthalen-2-yl)ethanamine hydrochloride (1R)-1-(5-methylnaphthalen-1-yl)ethan-1-amine Cinacalcet IMpurity 3 Cinacalcet Impurity 46 3-(4-TRIFLUOROMETHYL-PHENYL)-PROPAN-1-OL Methanesulfonic acid 3-(3-trifluoroMethylphenyl)propyl ester cinacalcet iMpurity 4 N-(1-(naphthalen-1-yl)ethyl)forMaMide Cinacalcet impurity C Cinacalcet Impurity 45 Cinacalcet Impurity 39 (Mixture of Diastereomers)

(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMI&

N-benzyl-1-(1-naphthyl)ethylamine hydrochloride

(R)-(-)-N-BENZYL-1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE

(R)-N-BENZYL 1-(1-NAPHTHYL)ETHYLAMINE HYDROCHLORIDE

(R)-N-[1-(1-NAPHTHYL)ETHYL]BENZYLAMINE HYDROCHLORIDE

Cinacalcet Impurity B (HCl salt form)

(R)-N-Benzyl-1-(naphthalen-1-yl)ethanamine hydrochloride

Cinacalcet Impurity B HCl

benzyl-(1-naphthalen-1-yl-ethyl)-amine hydrochloride

Cinacalcet Impurity B-HClQ: What is Cinacalcet Impurity B-HCl Q: What is the CAS Number of Cinacalcet Impurity B-HCl Q: What is the storage condition of Cinacalcet Impurity B-HCl Q: What are the applications of Cinacalcet Impurity B-HCl

CicalcetImpurityBHCl

163831-65-0

C10H7CHCH3NHCH2C6H5HCl

C19H19NClH

Chiral Resolving Reagents

Chiral Resolution Reagents

Asymmetric Synthesis