ChemicalBook > CAS DataBase List > 2-BROMO-5-IODOANISOLE

2-BROMO-5-IODOANISOLE

Product Name: 2-BROMO-5-IODOANISOLE
CAS No.: 755027-18-0
Chemical Name: 2-BROMO-5-IODOANISOLE
Synonyms: 2-BROMO-5-IODOANISOLE;2-Bromo-5-iodoanisole 98%;2-bromo-5-iodophenyl ether;2-iodine-5-bromophenyl ether;2-BroMo-5-iodophenyl Methyl ether;Benzene, 1-broMo-4-iodo-2-Methoxy-;1-Bromo-4-iodo-2-methoxybenzene, 2-Bromo-5-iodophenyl methyl ether
CBNumber: CB5125368
Molecular Formula: C7H6BrIO
Formula Weight: 312.93
MOL File: 755027-18-0.mol

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2-BROMO-5-IODOANISOLE Property

Boiling point:: 293.7±20.0 °C(Predicted)
Density: 2.062
storage temp.: Keep in dark place,Sealed in dry,2-8°C
form: crystalline needles
color: Faint yellow

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Safety

Hazard Codes: Xi
Hazard Note: Irritant
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B688943
Product name: 1-Bromo-4-iodo-2-methoxybenzene
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Oakwood

Product number: 062593
Product name: 2-Bromo-5-iodoanisole
Packaging: 250mg
Price: $9
Updated: 2021/12/16

AK Scientific

Product number: V2185
Product name: 2-Bromo-5-iodoanisole
Packaging: 10g
Price: $90
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB64625
Product name: 2-bromo-5-iodoanisole
Packaging: 25g
Price: $106.25
Updated: 2021/12/16

Ark Pharm

Product number: AK-72575
Product name: 1-Bromo-4-iodo-2-methoxybenzene
Purity: 97%
Packaging: 25g
Price: $109
Updated: 2021/12/16

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2-BROMO-5-IODOANISOLE Chemical Properties,Usage,Production

Synthesis

19056-40-7

755027-18-0

4-Bromo-3-methoxyaniline (102 mg, 0.50 mmol) was used as starting material and dissolved in concentrated hydrochloric acid (10 mL) at 0 °C. Subsequently, an aqueous solution of sodium nitrite (NaNO2, 45 mg, 0.65 mmol) (5 mL) was slowly added, the reaction temperature was maintained at 0 °C and the reaction was stirred for 1 hour. Next, an aqueous solution of potassium iodide (KI, 249 mg, 1.5 mmol) (5 mL) was added, and the reaction mixture was gradually warmed to room temperature and stirred overnight. After completion of the reaction, the product was extracted with ethyl acetate. The organic phase was washed sequentially with water and 10% sodium thiosulfate (Na2S2O3) solution, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated to give 147 mg of 2-bromo-5-iodoanisole in 94% yield. The product was analyzed by mass spectrometry (ESI), m/e 332 (M + 20)+; nuclear magnetic resonance hydrogen spectrum (1H NMR, 300 MHz, DMSO-d6) δ 7.39 (d, J = 1.87 Hz, 1H), 7.34 (d, J = 8.11 Hz, 1H), 7.24 (dd, J = 8.11, 1.87 Hz, 1H), 3.86 (s 3H).

References

[1] European Journal of Organic Chemistry, 2018, vol. 2018, # 38, p. 5312 - 5322
[2] Patent: WO2004/76424, 2004, A1. Location in patent: Page 79
[3] Journal of the American Chemical Society, 2018,
[4] Patent: WO2007/37187, 2007, A1. Location in patent: Page/Page column 127-128
[5] Patent: WO2008/57208, 2008, A2. Location in patent: Page/Page column 50

2-BROMO-5-IODOANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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China 112 India 4 Switzerland 1 United Kingdom 5 United States 8 Global 130

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View Lastest Price from 2-BROMO-5-IODOANISOLE manufacturers

Career Henan Chemical Co

Product: 2-BROMO-5-IODOANISOLE 755027-18-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

755027-18-0, 2-BROMO-5-IODOANISOLERelated Search:

2-Bromo-3-iodoanisole 4-Bromo-2-iodoanisole 4-BROMO-3-IODOANISOLE 3-Bromo-2-iodoanisole 2-Bromo-4-iodoanisole 2-BROMO-5-IODOPHENOL 2-BROMO-5-IODOANISOLE

2-BROMO-5-IODOANISOLE

Benzene, 1-broMo-4-iodo-2-Methoxy-

1-Bromo-4-iodo-2-methoxybenzene, 2-Bromo-5-iodophenyl methyl ether

2-BroMo-5-iodophenyl Methyl ether

2-Bromo-5-iodoanisole 98%

2-bromo-5-iodophenyl ether

2-iodine-5-bromophenyl ether

755027-18-0

55027-18-0

Anisoles, Alkyloxy Compounds & Phenylacetates

Bromine Compounds

Iodine Compounds

Aromatic Halides (substituted)