1-chloro-5-nitro-isoquinoline
- Product Name
- 1-chloro-5-nitro-isoquinoline
- CAS No.
- 58142-97-5
- Chemical Name
- 1-chloro-5-nitro-isoquinoline
- Synonyms
- 1-chloro-5-nitro-isoquinoline;Isoquinoline, 1-chloro-5-nitro-
- CBNumber
- CB51519834
- Molecular Formula
- C9H5ClN2O2
- Formula Weight
- 208.6
- MOL File
- 58142-97-5.mol
1-chloro-5-nitro-isoquinoline Property
- Melting point:
- 183-184℃
- Boiling point:
- 376.8±27.0 °C(Predicted)
- Density
- 1.484
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 0.22±0.43(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C596710
- Product name
- 1-Chloro-5-nitroisoquinoline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- HCH0050292
- Product name
- 1-CHLORO-5-NITROISOQUINOLINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $933.24
- Updated
- 2021/12/16
- Product number
- HCH0050292
- Product name
- 1-CHLORO-5-NITROISOQUINOLINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1346.73
- Updated
- 2021/12/16
- Product number
- 073147
- Product name
- 1-Chloro-5-nitroisoquinoline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $700
- Updated
- 2021/12/16
- Product number
- W7135
- Product name
- 1-Chloro-5-nitroisoquinoline
- Packaging
- 1g
- Price
- $157
- Updated
- 2021/12/16
1-chloro-5-nitro-isoquinoline Chemical Properties,Usage,Production
Synthesis
57554-78-6
58142-97-5
GENERAL METHODS: To a stirred solution of acridazine N-oxide (CAS:57554-78-6) in anhydrous dichloromethane (0.1 M) was slowly added phosphorous trichloride (1.2 eq.) at 0 °C, followed by the addition of N,N-dimethylformamide (0.5 eq.) dropwise under argon protection. The reaction mixture was gradually warmed to 25 °C and stirred continuously for several hours until thin layer chromatography (TLC) showed completion of the reaction. After completion of the reaction, saturated aqueous sodium carbonate solution was slowly added and the pH was adjusted to 7~8. The reaction mixture was separated and the aqueous phase was thoroughly extracted with dichloromethane. The organic phases were combined, washed with saturated saline, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography using petroleum ether/ethyl acetate (80:1) as eluent.
References
[1] Tetrahedron Letters, 2014, vol. 55, # 51, p. 7130 - 7132
1-chloro-5-nitro-isoquinoline Preparation Products And Raw materials
Raw materials
Preparation Products
1-chloro-5-nitro-isoquinoline Suppliers
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- Country
- United States
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View Lastest Price from 1-chloro-5-nitro-isoquinoline manufacturers
- Product
- 1-chloro-5-nitro-isoquinoline 58142-97-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1lg; 2kg; 5kg; 10kg; 100kg
- Release date
- 2019-08-31