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Methyl 2,4-dichlorophenylacetate

Product Name
Methyl 2,4-dichlorophenylacetate
CAS No.
55954-23-9
Chemical Name
Methyl 2,4-dichlorophenylacetate
Synonyms
47339;2,4-dcaa methyl ester;4-dichlorophenylacetate;METHYL 2,4-DICHLOROPHENYLACETATE;Methyl 2,4-dichlorobenzeneacetate;Methyl2,4-Dichlorophenylacetate>Methyl 2-(2,4-dichlorophenyl)acetate;Methyl 2,4-dichlorophenylacetate,99%;2,4-Dimethyl acetic acid methyl ester;methyl 2,4-dichlorophenylacetate solution
CBNumber
CB5191785
Molecular Formula
C9H8Cl2O2
Formula Weight
219.06
MOL File
55954-23-9.mol
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Methyl 2,4-dichlorophenylacetate Property

Boiling point:
153°C/27mmHg(lit.)
Density 
1.3295 (rough estimate)
refractive index 
1.539-1.542
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid
color 
Clear colorless to yellow
CAS DataBase Reference
55954-23-9(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn,N,F
Risk Statements 
22-67-65-62-51/53-48/20-38-11-66-36/38-36
Safety Statements 
24/25-62-61-36/37-33-29-16-9-26
RIDADR 
UN 2810 6.1/PG 3
HS Code 
29163900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H319Causes serious eye irritation

H336May cause drowsiness or dizziness

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
M2528
Product name
Methyl 2,4-Dichlorophenylacetate
Purity
>99.0%(GC)
Packaging
5g
Price
$40
Updated
2025/07/31
TCI Chemical
Product number
M2528
Product name
Methyl 2,4-Dichlorophenylacetate
Purity
>99.0%(GC)
Packaging
25g
Price
$120
Updated
2025/07/31
TRC
Product number
M301395
Product name
Methyl 2,4-Dichlorophenylacetate
Packaging
2.5g
Price
$65
Updated
2021/12/16
SynQuest Laboratories
Product number
2723-5-17
Product name
Methyl 2,4-dichlorophenylacetate
Purity
97%
Packaging
100g
Price
$136
Updated
2021/12/16
AK Scientific
Product number
F832
Product name
Methyl 2,4-Dichlorophenylacetate
Packaging
500g
Price
$360
Updated
2021/12/16
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Methyl 2,4-dichlorophenylacetate Chemical Properties,Usage,Production

Chemical Properties

clear colorless to yellow liquid

Synthesis

67-56-1

19719-28-9

55954-23-9

General procedure for the synthesis of methyl 2,4-dichlorophenylacetate from methanol and 2,4-dichlorophenylacetic acid: to a solution of 2,4-dichlorophenylacetic acid (3.5 g, 17.1 mmol) in methanol (100 mL) was slowly added concentrated sulfuric acid (20 drops). The reaction mixture was heated to reflux for 12 hours. Upon completion of the reaction, the solvent was removed by rotary evaporator under reduced pressure. The residue was diluted with cold water (50 mL) and extracted with ethyl acetate (3 x 50 mL). The organic layers were combined and washed sequentially with saturated sodium bicarbonate solution (50 mL) and saturated saline (50 mL), then dried with anhydrous sodium sulfate and filtered. The solvent was again removed by rotary evaporator under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography (eluent ratio 4:1 hexane/ethyl acetate) to afford methyl 2,4-dichlorophenylacetate (3.56 g, 95% yield) as a clear oil. The structure of the product was confirmed by 1H NMR (DMSO-d6): δ 7.40 (s, 1H), 7.22 (d, J=1.5 Hz, 2H), 3.74 (s, 2H), 3.71 (s, 3H).

References

[1] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 13, p. 2843 - 2866
[2] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 1, p. 245 - 249
[3] Patent: US2016/31892, 2016, A1. Location in patent: Paragraph 0195-0196
[4] ACS Medicinal Chemistry Letters, 2010, vol. 1, # 4, p. 145 - 149
[5] Bulletin of the Korean Chemical Society, 2010, vol. 31, # 8, p. 2315 - 2321

Methyl 2,4-dichlorophenylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2,4-dichlorophenylacetate Suppliers

J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
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TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
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81
Energy Chemical
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021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
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Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
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Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
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Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18729
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Sichuan Kulinan Technology Co., Ltd
Tel
400-1166-196 18981987031
Fax
028-84555506 800101999
Email
cdhxsj@163.com
Country
China
ProdList
11705
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57
Spectrum Chemical Manufacturing Corp.
Tel
021-021-021-67601398-809-809-809 15221380277
Fax
021-57711696
Email
marketing_china@spectrumchemical.com
Country
China
ProdList
9658
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60
Shanghai civi chemical technology co.,Ltd
Tel
86-21-34053660
Fax
86-21-34053661
Email
sale@labgogo.com
Country
China
ProdList
9865
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52
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View Lastest Price from Methyl 2,4-dichlorophenylacetate manufacturers

Henan Fengda Chemical Co., Ltd
Product
Methyl 2,4-dichlorophenylacetate 55954-23-9
Price
US $5.00-0.10/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-15
Career Henan Chemical Co
Product
Methyl (2,4-dichlorophenyl)acetate 55954-23-9
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200kg
Release date
2018-12-25

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