1,4-DIIODO-2,5-DIMETHOXYBENZENE
- Product Name
- 1,4-DIIODO-2,5-DIMETHOXYBENZENE
- CAS No.
- 51560-21-5
- Chemical Name
- 1,4-DIIODO-2,5-DIMETHOXYBENZENE
- Synonyms
- 4-DIIODO-2;1,4-Diiodo-2,5-dimethoxybenzen;2,5-DIMETHOXY-1,4-DIIODOBENZENE;2,5-DIIODO-1,4-DIMETHOXYBENZENE;1,4-DIIODO-2,5-DIMETHOXYBENZENE;2,5-diiodo-p-phenyldimethyl ether;Benzene, 1,4-diiodo-2,5-dimethoxy-;1,4-diiodo-2,5-bis(methoxy)benzene;2,5-Diiodo-1,4-dimethoxybenzene 2,5-Dimethoxy-1,4-diiodobenzene
- CBNumber
- CB5235719
- Molecular Formula
- C8H8I2O2
- Formula Weight
- 389.96
- MOL File
- 51560-21-5.mol
1,4-DIIODO-2,5-DIMETHOXYBENZENE Property
- Melting point:
- 171 °C
- Boiling point:
- 382.9±42.0 °C(Predicted)
- Density
- 2.147±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- form
- powder to crystal
- color
- White to Light yellow
Safety
- Hazard Codes
- Xi
- Hazard Note
- Irritant
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D5590
- Product name
- 1,4-Diiodo-2,5-dimethoxybenzene
- Packaging
- 1G
- Price
- $62
- Updated
- 2025/07/31
- Product number
- D5590
- Product name
- 1,4-Diiodo-2,5-dimethoxybenzene
- Packaging
- 5G
- Price
- $184
- Updated
- 2025/07/31
- Product number
- D455178
- Product name
- 1,4-Diiodo-2,5-dimethoxybenzene
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- J50931
- Product name
- 1,4-Diiodo-2,5-dimethoxybenzene
- Packaging
- 5g
- Price
- $155
- Updated
- 2021/12/16
- Product number
- W6643
- Product name
- 1,4-Diiodo-2,5-dimethoxybenzene
- Packaging
- 1g
- Price
- $74
- Updated
- 2021/12/16
1,4-DIIODO-2,5-DIMETHOXYBENZENE Chemical Properties,Usage,Production
Synthesis
150-78-7
51560-21-5
General procedure for the synthesis of 1,4-diiodo-2,5-dimethoxybenzene from 1,4-dimethoxybenzene: 1,4-dimethoxybenzene (2.70 g, 20.0 mmol) was dissolved in methanol (25 mL) and stirred for 10 min according to Ko et al. Iodine (6.38 g, 25.0 mmol) was subsequently added to the mixture. The reaction mixture was heated at 70°C for 4 hours. Upon completion of the reaction, the mixture was poured into a solution of water (50 mL) containing sodium thiosulfate (5.00 g, 31.6 mmol). The resulting solution was filtered and the precipitate was washed with methanol (20 mL) and then dissolved in dichloromethane (20 mL). After filtration through a sintered funnel, the filtrate was evaporated in vacuum to afford the target product 1,4-diiodo-2,5-dimethoxybenzene as a white solid (7.52 g, 97% yield).1H NMR (400 MHz; CDCl3) δ 3.82 (6H, s, OCH3), 7.19 (2H, s, Ar-H).The 1H NMR data were in agreement with the literature values.
References
[1] Patent: WO2018/47101, 2018, A1. Location in patent: Page/Page column 68; 73
[2] Synthetic Communications, 2002, vol. 32, # 20, p. 3233 - 3239
[3] Patent: CN107573251, 2018, A. Location in patent: Page/Page column 2; 5; 6
[4] Chemistry Letters, 1988, # 5, p. 795 - 798
[5] Macromolecules, 2015, vol. 48, # 15, p. 5155 - 5161
1,4-DIIODO-2,5-DIMETHOXYBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,4-DIIODO-2,5-DIMETHOXYBENZENE manufacturers
- Product
- 1,4-Diiodo-2,5-dimethoxybenzene 51560-21-5
- Price
- US $2.00-5.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons
- Release date
- 2025-07-10
- Product
- 1,4-DIIODO-2,5-DIMETHOXYBENZENE 51560-21-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-12