ChemicalBook > CAS DataBase List > 1,4-DIIODO-2,5-DIMETHOXYBENZENE

1,4-DIIODO-2,5-DIMETHOXYBENZENE

Product Name
1,4-DIIODO-2,5-DIMETHOXYBENZENE
CAS No.
51560-21-5
Chemical Name
1,4-DIIODO-2,5-DIMETHOXYBENZENE
Synonyms
4-DIIODO-2;1,4-Diiodo-2,5-dimethoxybenzen;2,5-DIMETHOXY-1,4-DIIODOBENZENE;2,5-DIIODO-1,4-DIMETHOXYBENZENE;1,4-DIIODO-2,5-DIMETHOXYBENZENE;2,5-diiodo-p-phenyldimethyl ether;Benzene, 1,4-diiodo-2,5-dimethoxy-;1,4-diiodo-2,5-bis(methoxy)benzene;2,5-Diiodo-1,4-dimethoxybenzene 2,5-Dimethoxy-1,4-diiodobenzene
CBNumber
CB5235719
Molecular Formula
C8H8I2O2
Formula Weight
389.96
MOL File
51560-21-5.mol
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1,4-DIIODO-2,5-DIMETHOXYBENZENE Property

Melting point:
171 °C
Boiling point:
382.9±42.0 °C(Predicted)
Density 
2.147±0.06 g/cm3(Predicted)
storage temp. 
2-8°C(protect from light)
form 
powder to crystal
color 
White to Light yellow
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2909309090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D5590
Product name
1,4-Diiodo-2,5-dimethoxybenzene
Packaging
1G
Price
$62
Updated
2025/07/31
TCI Chemical
Product number
D5590
Product name
1,4-Diiodo-2,5-dimethoxybenzene
Packaging
5G
Price
$184
Updated
2025/07/31
TRC
Product number
D455178
Product name
1,4-Diiodo-2,5-dimethoxybenzene
Packaging
500mg
Price
$130
Updated
2021/12/16
AK Scientific
Product number
J50931
Product name
1,4-Diiodo-2,5-dimethoxybenzene
Packaging
5g
Price
$155
Updated
2021/12/16
AK Scientific
Product number
W6643
Product name
1,4-Diiodo-2,5-dimethoxybenzene
Packaging
1g
Price
$74
Updated
2021/12/16
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1,4-DIIODO-2,5-DIMETHOXYBENZENE Chemical Properties,Usage,Production

Synthesis

150-78-7

51560-21-5

General procedure for the synthesis of 1,4-diiodo-2,5-dimethoxybenzene from 1,4-dimethoxybenzene: 1,4-dimethoxybenzene (2.70 g, 20.0 mmol) was dissolved in methanol (25 mL) and stirred for 10 min according to Ko et al. Iodine (6.38 g, 25.0 mmol) was subsequently added to the mixture. The reaction mixture was heated at 70°C for 4 hours. Upon completion of the reaction, the mixture was poured into a solution of water (50 mL) containing sodium thiosulfate (5.00 g, 31.6 mmol). The resulting solution was filtered and the precipitate was washed with methanol (20 mL) and then dissolved in dichloromethane (20 mL). After filtration through a sintered funnel, the filtrate was evaporated in vacuum to afford the target product 1,4-diiodo-2,5-dimethoxybenzene as a white solid (7.52 g, 97% yield).1H NMR (400 MHz; CDCl3) δ 3.82 (6H, s, OCH3), 7.19 (2H, s, Ar-H).The 1H NMR data were in agreement with the literature values.

References

[1] Patent: WO2018/47101, 2018, A1. Location in patent: Page/Page column 68; 73
[2] Synthetic Communications, 2002, vol. 32, # 20, p. 3233 - 3239
[3] Patent: CN107573251, 2018, A. Location in patent: Page/Page column 2; 5; 6
[4] Chemistry Letters, 1988, # 5, p. 795 - 798
[5] Macromolecules, 2015, vol. 48, # 15, p. 5155 - 5161

1,4-DIIODO-2,5-DIMETHOXYBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,4-DIIODO-2,5-DIMETHOXYBENZENE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
1,4-Diiodo-2,5-dimethoxybenzene 51560-21-5
Price
US $2.00-5.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons
Release date
2025-07-10
Career Henan Chemical Co
Product
1,4-DIIODO-2,5-DIMETHOXYBENZENE 51560-21-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-12

51560-21-5, 1,4-DIIODO-2,5-DIMETHOXYBENZENERelated Search:


  • 1,4-DIIODO-2,5-DIMETHOXYBENZENE
  • 2,5-DIIODO-1,4-DIMETHOXYBENZENE
  • 2,5-DIMETHOXY-1,4-DIIODOBENZENE
  • Benzene, 1,4-diiodo-2,5-dimethoxy-
  • 2,5-Diiodo-1,4-dimethoxybenzene 2,5-Dimethoxy-1,4-diiodobenzene
  • 1,4-diiodo-2,5-bis(methoxy)benzene
  • 1,4-Diiodo-2,5-dimethoxybenzen
  • 4-DIIODO-2
  • 2,5-diiodo-p-phenyldimethyl ether
  • 51560-21-5