ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE

Product Name: ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE
CAS No.: 81803-60-3
Chemical Name: ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE
Synonyms: ethyl imidazo(1,5)-pyridine-3-carboxylate;Ethyl 3-Imidazo[1,5-a]pyridinecarboxylate;ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE;ethyl 1H-imidazo[1,5-a]pyridine-3-carboxylate;Imidazo[1,5-a]pyridine-3-carboxylic acid ethyl ester
CBNumber: CB52454620
Molecular Formula: C10H10N2O2
Formula Weight: 190.2
MOL File: 81803-60-3.mol

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ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE Property

Density: 1.22±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 3.98±0.30(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: E940180
Product name: EthylImidazo[1,5-A]pyridine-3-carboxylate
Packaging: 500mg
Price: $285
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0392644
Product name: ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $497.93
Updated: 2021/12/16

Chemenu

Product number: CM123865
Product name: ethylimidazo[1,5-a]pyridine-3-carboxylate
Purity: 95+%
Packaging: 100mg
Price: $54
Updated: 2021/12/16

Chemenu

Product number: CM123865
Product name: ethylimidazo[1,5-a]pyridine-3-carboxylate
Purity: 95+%
Packaging: 250mg
Price: $69
Updated: 2021/12/16

Chemenu

Product number: CM123865
Product name: ethylimidazo[1,5-a]pyridine-3-carboxylate
Purity: 95+%
Packaging: 1g
Price: $206
Updated: 2021/12/16

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ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

46460-25-7

81803-60-3

General procedure for the synthesis of ethyl imidazo[1,5-a]pyridine-3-carboxylate from ethyl 2-oxo-2-((pyridin-2-ylmethyl)amino)acetate: ethyl [(pyridin-2-ylmethyl)carbamoyl]formate (1.00 g, 4.80 mmol, 1.00 equiv) and phosphorus pentoxide (3.41 g, 24.02 mmol, 5.00 equiv) were dissolved in phosphoryl chloride (30 mL). ) were dissolved in phosphoryl chloride (30 mL) and the reaction was stirred at 110°C for 5 hours. After completion of the reaction, the mixture was concentrated under reduced pressure. The residue was purified by silica gel column chromatography with ethyl acetate/petroleum ether (1:1, v/v) as eluent. 635 mg (70% yield) of the target product, ethyl imidazo[1,5-a]pyridine-3-carboxylate, was finally obtained as a yellow solid.LC-MS (ESI, m/z): 191 [M + H]+.

References

[1] Patent: WO2015/25025, 2015, A1. Location in patent: Page/Page column 411; 412
[2] Patent: WO2008/85302, 2008, A1. Location in patent: Page/Page column 96
[3] Organic Letters, 2013, vol. 15, # 9, p. 2290 - 2293
[4] Synthesis (Germany), 2016, vol. 48, # 23, p. 4269 - 4277

ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE Suppliers

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81803-60-3, ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATERelated Search:

Ethyl 6-broMoisoquinoline-3-carboxylate ethyl iMidazo[1,2-b]pyridazine-2-carboxylate Imidazo[1,2-a]pyridine-7-methanol (9CI) IMIDAZO[1,2-A]PYRIDINE-6-CARBONITRILE Imidazo[1,5-a]pyridine Imidazo[1,2-b]pyridazine Imidazo[1,2-a]pyridine-7-carboxylic acid (9CI) Imidazo[1,2-a]pyridine-6-boronic acid IMIDAZO[1,2-B]PYRIDAZIN-6-AMINE IMIDAZO[1,2-A]PYRIDIN-8-YLAMINE IMIDAZO[1,5-A]PYRIDINE-1-CARBOXYLIC ACID ETHYL ESTER Imidazo[1,5-a]pyridine-1-carboxaldehyde (9CI) Ethyl iMidazo[1,5-a]pyridine-8-carboxylate ethyl iMidazo[1,5-a]pyridine-7-carboxylate ETHYL4-METHYL-1H-IMIDAZOLE-2-CARBOXYLATE 4-METHYL-1H-IMIDAZOLE-2-CARBOXYLICACID ETHYL 1-METHYL-1H-IMIDAZOLE-2-CARBOXYLATE ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE

ETHYL IMIDAZO[1,5-A]PYRIDINE-3-CARBOXYLATE

Imidazo[1,5-a]pyridine-3-carboxylic acid ethyl ester

ethyl imidazo(1,5)-pyridine-3-carboxylate

ethyl 1H-imidazo[1,5-a]pyridine-3-carboxylate

Ethyl 3-Imidazo[1,5-a]pyridinecarboxylate

81803-60-3