ChemicalBook > CAS DataBase List > 1,4-Bis(dimethylsilyl)benzene

1,4-Bis(dimethylsilyl)benzene

Product Name
1,4-Bis(dimethylsilyl)benzene
CAS No.
2488-01-9
Chemical Name
1,4-Bis(dimethylsilyl)benzene
Synonyms
DK235;214773;DKFELEX0088;1,4-Bis(dimethyL;p-Bis(dimethysilyl)benzene;P-BIS(DIMETHYLSILYL)BENZENE;1,4-BIS(DIMETHYLSILYL)BENZENE;p-phenylenebis(dimethyl-silan;1,4-Phenylenbis[dimethylsilan;P-PHENYLENEBIS(DIMETHYLSILANE)
CBNumber
CB5246168
Molecular Formula
C10H18Si2
Formula Weight
194.42
MOL File
2488-01-9.mol
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1,4-Bis(dimethylsilyl)benzene Property

Melting point:
115 °C
Boiling point:
213-214 °C(lit.)
Density 
0.874 g/mL at 25 °C(lit.)
refractive index 
n20/D 1.502(lit.)
Flash point:
185 °F
storage temp. 
Inert atmosphere,Room Temperature
form 
clear liquid
color 
Colorless to Light yellow
Specific Gravity
0.872
Hydrolytic Sensitivity
3: reacts with aqueous base
BRN 
1072658
InChI
InChI=1S/C10H18Si2/c1-11(2)9-5-7-10(8-6-9)12(3)4/h5-8,11-12H,1-4H3
InChIKey
KQERVIARWMHFOS-UHFFFAOYSA-N
SMILES
C1([SiH](C)C)=CC=C([SiH](C)C)C=C1
CAS DataBase Reference
2488-01-9(CAS DataBase Reference)
NIST Chemistry Reference
1,4-Bis(dimethylsilyl)benzene(2488-01-9)
EPA Substance Registry System
Silane, 1,4-phenylenebis[dimethyl- (2488-01-9)
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Safety

Hazard Codes 
Xn
Risk Statements 
22
Safety Statements 
26-36/37/39-36/37-23
RIDADR 
1993
WGK Germany 
3
RTECS 
VV4830000
TSCA 
Yes
HS Code 
29319000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

H302Harmful if swallowed

H313May be harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
483192
Product name
1,4-Bis(dimethylsilyl)benzene
Purity
97%
Packaging
5ML
Price
$193
Updated
2023/06/20
TCI Chemical
Product number
B4748
Product name
1,4-Bis(dimethylsilyl)benzene
Purity
>98.0%(GC)
Packaging
5mL
Price
$76
Updated
2024/03/01
TCI Chemical
Product number
B4748
Product name
1,4-Bis(dimethylsilyl)benzene
Purity
>98.0%(GC)
Packaging
25mL
Price
$226
Updated
2024/03/01
Chem-Impex
Product number
40491
Product name
1,4-Bis(dimethylsilyl)benzene,98%(GC)
Purity
98%(GC)
Packaging
25ML
Price
$273.28
Updated
2021/12/16
Chem-Impex
Product number
40491
Product name
1,4-Bis(dimethylsilyl)benzene,≥98%(GC)
Purity
≥98%(GC)
Packaging
5ML
Price
$73.38
Updated
2021/12/16
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1,4-Bis(dimethylsilyl)benzene Chemical Properties,Usage,Production

Synthesis

In a 1000 mL reaction flask, Put in xylene 230g, Sodium metal 47g, TDA-1 0.37g, Warm up to 100110°C, Insulation 0.5h, and Turn on stirring. After stirring for 1 hour, all the sodium was made into sodium sand, and a Sodium sand mixture was formed. After 73.5 g of p-dichlorobenzene and 100 g of xylene were mixed and dissolved, Then add 96.5g of dimethylchlorosilane Formed a mixture; the mixture was added to a constant-pressure funnel. The liquid droplets in the constant pressure funnel are added to the sodium sand mixture. Dropping about 5h to complete, the reaction was completed by keeping it at 100-110°C for 2 hours. After the reaction, Cool the reaction system to 5-15°C. Then, add 280 mL of water from the constant pressure funnel. Stirring 1h, Stand for 1h, Then separate the lower brine phase, The upper organic phase is taken as the crude 1,4-bis (dimethylsilyl) benzene. The upper organic phase is entered into the distillation flask, and the temperature in the control bottle is below 120°C. Vacuum distillation,92 g of 1,4-Bis(dimethylsilyl)benzene was obtained; the yield is 95%.

1,4-Bis(dimethylsilyl)benzene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,4-Bis(dimethylsilyl)benzene manufacturers

Career Henan Chemical Co
Product
1,4-Bis(dimethylsilyl)benzene 2488-01-9
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2019-12-30

2488-01-9, 1,4-Bis(dimethylsilyl)benzeneRelated Search:


  • 1,4-phenylenebis(dimethyl-silan
  • 214773
  • p-Bis(dimethysilyl)benzene
  • p-phenylenebis(dimethyl-silan
  • Silane, 1,4-phenylenebis[dimethyl-
  • Silane, p-phenylenebis(dimethyl-
  • 1,4-BIS(DIMETHYLSILYL)BENZENE
  • 1,4 BIS(DIMETHYLSILYL)BENZENE MIN
  • 1,4-phenylenebis[dimethylsilane]
  • P-PHENYLENEBIS(DIMETHYLSILANE)
  • P-BIS(DIMETHYLSILYL)BENZENE
  • 1,4-Bis(dimethylsilyl)benzene, 97+%
  • [4-(Dimethylsilyl)phenyl]dimethylsilane
  • 1,4-Phenylenbis[dimethylsilan
  • 1,4-Bis(dimethyL
  • Benzene, 1,4-bis(dimethylsilyl)-
  • DK235
  • DKFELEX0088
  • 2488-01-9
  • 2488-1-9
  • C6H4SiHCH322
  • Organometallic Reagents
  • Others
  • Organosilicon