7-methoxy-2,3-dihydro-1H-inden-1-amine

Product Name: 7-methoxy-2,3-dihydro-1H-inden-1-amine
CAS No.: 1032279-33-6
Chemical Name: 7-methoxy-2,3-dihydro-1H-inden-1-amine
Synonyms: 2,3-dihydro-7-Methoxy-1H-inden-1-aMine;7-methoxy-2,3-dihydro-1H-inden-1-amine;1H-Inden-1-amine, 2,3-dihydro-7-methoxy-
CBNumber: CB52516368
Molecular Formula: C10H13NO
Formula Weight: 163.22
MOL File: 1032279-33-6.mol

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7-methoxy-2,3-dihydro-1H-inden-1-amine Property

Boiling point:: 264.3±40.0 °C(Predicted)
Density: 1.087±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 9.38±0.20(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Activate Scientific

Product number: AS8768
Product name: 7-Methoxy-2,3-dihydro-1h-inden-1-amine
Purity: 95+%
Packaging: 100mg
Price: $239
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0391618
Product name: 7-METHOXY-2,3-DIHYDRO-1H-INDEN-1-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $502.15
Updated: 2021/12/16

Crysdot

Product number: CD12185371
Product name: 7-Methoxy-2,3-dihydro-1H-inden-1-amine
Purity: 95+%
Packaging: 1g
Price: $886
Updated: 2021/12/16

Alichem

Product number: 1032279336
Product name: 7-Methoxy-2,3-dihydro-1H-inden-1-amine
Packaging: 1g
Price: $921.85
Updated: 2021/12/16

Crysdot

Product number: CD12185371
Product name: 7-Methoxy-2,3-dihydro-1H-inden-1-amine
Purity: 95+%
Packaging: 250mg
Price: $256
Updated: 2021/12/16

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7-methoxy-2,3-dihydro-1H-inden-1-amine Chemical Properties,Usage,Production

Synthesis

908108-58-7

1032279-33-6

Step A: Synthesis of racemic-7-methoxy-indan-1-ylamine A mixture of 7-methoxy-indan-1-one oxime (CAS 908108-58-7, containing (E)-oxime, CAS 179899-16-2) (22.3 g, 126 mmol) was reacted with nickel ryenne (11.26 g) in a mixture of solvents of tetrahydrofuran (570 mL) and methanol (570 mL) at 100 bar of hydrogen pressure at 60 °C for Hydrogenation reaction was carried out for 22 hours. Upon completion of the reaction, the catalyst was removed by filtration and washed with methanol and tetrahydrofuran. Subsequently, all volatiles were removed by vacuum distillation to afford 7-methoxy-1-indenamine as a brown oil (19.95 g, 97% yield, HPLC retention time 0.4 min). Mass spectrometry (ISP) analysis showed m/e = 164.2 [(M+H)+].

References

[1] Patent: US2010/63037, 2010, A1. Location in patent: Page/Page column 23
[2] Patent: US2009/227570, 2009, A1. Location in patent: Page/Page column 35
[3] Patent: US2008/146567, 2008, A1. Location in patent: Page/Page column 27-29

7-methoxy-2,3-dihydro-1H-inden-1-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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7-methoxy-2,3-dihydro-1H-inden-1-amine Suppliers

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1032279-33-6