7-methoxy-2,3-dihydro-1H-inden-1-amine
- Product Name
- 7-methoxy-2,3-dihydro-1H-inden-1-amine
- CAS No.
- 1032279-33-6
- Chemical Name
- 7-methoxy-2,3-dihydro-1H-inden-1-amine
- Synonyms
- 2,3-dihydro-7-Methoxy-1H-inden-1-aMine;7-methoxy-2,3-dihydro-1H-inden-1-amine;1H-Inden-1-amine, 2,3-dihydro-7-methoxy-
- CBNumber
- CB52516368
- Molecular Formula
- C10H13NO
- Formula Weight
- 163.22
- MOL File
- 1032279-33-6.mol
7-methoxy-2,3-dihydro-1H-inden-1-amine Property
- Boiling point:
- 264.3±40.0 °C(Predicted)
- Density
- 1.087±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 9.38±0.20(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- AS8768
- Product name
- 7-Methoxy-2,3-dihydro-1h-inden-1-amine
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $239
- Updated
- 2021/12/16
- Product number
- CHM0391618
- Product name
- 7-METHOXY-2,3-DIHYDRO-1H-INDEN-1-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.15
- Updated
- 2021/12/16
- Product number
- CD12185371
- Product name
- 7-Methoxy-2,3-dihydro-1H-inden-1-amine
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $223
- Updated
- 2021/12/16
- Product number
- CD12185371
- Product name
- 7-Methoxy-2,3-dihydro-1H-inden-1-amine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $256
- Updated
- 2021/12/16
- Product number
- CD12185371
- Product name
- 7-Methoxy-2,3-dihydro-1H-inden-1-amine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $886
- Updated
- 2021/12/16
7-methoxy-2,3-dihydro-1H-inden-1-amine Chemical Properties,Usage,Production
Synthesis
908108-58-7
1032279-33-6
Step A: Synthesis of racemic-7-methoxy-indan-1-ylamine A mixture of 7-methoxy-indan-1-one oxime (CAS 908108-58-7, containing (E)-oxime, CAS 179899-16-2) (22.3 g, 126 mmol) was reacted with nickel ryenne (11.26 g) in a mixture of solvents of tetrahydrofuran (570 mL) and methanol (570 mL) at 100 bar of hydrogen pressure at 60 °C for Hydrogenation reaction was carried out for 22 hours. Upon completion of the reaction, the catalyst was removed by filtration and washed with methanol and tetrahydrofuran. Subsequently, all volatiles were removed by vacuum distillation to afford 7-methoxy-1-indenamine as a brown oil (19.95 g, 97% yield, HPLC retention time 0.4 min). Mass spectrometry (ISP) analysis showed m/e = 164.2 [(M+H)+].
References
[1] Patent: US2010/63037, 2010, A1. Location in patent: Page/Page column 23
[2] Patent: US2009/227570, 2009, A1. Location in patent: Page/Page column 35
[3] Patent: US2008/146567, 2008, A1. Location in patent: Page/Page column 27-29
7-methoxy-2,3-dihydro-1H-inden-1-amine Preparation Products And Raw materials
Raw materials
Preparation Products
7-methoxy-2,3-dihydro-1H-inden-1-amine Suppliers
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- Country
- India
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