4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane
- Product Name
- 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane
- CAS No.
- 890042-13-4
- Chemical Name
- 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane
- Synonyms
- (Triphenyl-2-yl) boric acid pinacol ester;(Triphenylen-2-yl)boronic acid pinacol ester;(Triphenylene-2-yl) boronic acid pinacol ester;1,3, 2-Dioxaborane-4,4,5,5-tetramethyl-2-(2-triphenylene);4,4,5,5-TetraMethyl-2-triphenylen-2-yl-[1,3,2]dioxaborolane;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)triphenylene;1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(2-triphenylenyl)-;4,4,5,5-TetraMethyl-2-triphenylen-2-yl-[1,3,2]dioxaborolane (TPE);4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane
- CBNumber
- CB52666544
- Molecular Formula
- C24H23BO2
- Formula Weight
- 354.25
- MOL File
- 890042-13-4.mol
4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane Property
- Melting point:
- 174.0 to 178.0 °C
- Boiling point:
- 544.9±19.0 °C(Predicted)
- Density
- 1.16±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Orange to Green
Safety
- HS Code
- 2931900090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- T3322
- Product name
- 4,4,5,5-Tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 1g
- Price
- $178
- Updated
- 2024/03/01
- Product number
- T3322
- Product name
- 4,4,5,5-Tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 5g
- Price
- $615
- Updated
- 2024/03/01
- Product number
- T889740
- Product name
- 4,4,5,5-Tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 6270AL
- Product name
- 4,4,5,5-Tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane
- Packaging
- 5g
- Price
- $938
- Updated
- 2021/12/16
- Product number
- A639577
- Product name
- 4,4,5,5-Tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane
- Purity
- 95+%
- Packaging
- 1g
- Price
- $32
- Updated
- 2021/12/16
4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane Chemical Properties,Usage,Production
Uses
4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly for laboratory research and development Process and chemical production process.
Synthesis
In a nitrogen atmosphere, 100 g (326 mmol) of 2-bromotriphenylene was dissolved in dimethylformamide(Pinacolato diboron) 99.2 (manufactured by Wako Pure Chemical Industries, Ltd.) was dissolved in 1,000 mL of dimethylformamide (DMF)G (391 mmol) and 1,1'-bis (diphenylphosphine) ferrocene) dichloropalladium (II) (1,1-Bis (diphenylphosphine) ferrocene) dichloropalladium (II)) 2.66 g (3.26 mmol) and potassium acetate 80 g (815 mmol) of potassium acetate were added and the mixture was refluxed by heating at 150 DEG C for 5 hours. After completing the reaction,Water was added to the solution, the mixture was filtered, and then dried in a vacuum oven. The thus obtained residue was purified by flash column chromatographyTo obtain 113 g (98%) of the compound I-1. HRMS (70 eV, EI +): m / z Calcd for C24H23BO2: 354.1791, found
4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane Preparation Products And Raw materials
Raw materials
Preparation Products
4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane Suppliers
- Tel
- 03-36680489
- Fax
- 03-3668-0520
- Sales-JP@TCIchemicals.com
- Country
- Japan
- ProdList
- 28387
- Advantage
- 80
View Lastest Price from 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane manufacturers
- Product
- 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane 890042-13-4
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-09-25
- Product
- 4,4,5,5-tetramethyl-2-(triphenylen-2-yl)-1,3,2-dioxaborolane 890042-13-4
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99.9%
- Supply Ability
- 30000 Kg
- Release date
- 2023-11-09
- Product
- 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane 890042-13-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons/month
- Release date
- 2020-01-08