2,6-Dimethylbenzyl alcohol
- Product Name
- 2,6-Dimethylbenzyl alcohol
- CAS No.
- 62285-58-9
- Chemical Name
- 2,6-Dimethylbenzyl alcohol
- Synonyms
- RARECHEM AL BD 0363;6-Dimethylbenzyl alcohol;2,6-DIMETHYLBENZYL ALCOHOL;2,6-DIMETHYL-BENZENEMETHANOL;2,6-Dimethylbenzylalcohol,98%;(2,6-DIMETHYL-PHENYL)-METHANOL;Benzenemethanol, 2,6-dimethyl-;2,6-Dimethylbenzyl alcohol ,97%
- CBNumber
- CB5322097
- Molecular Formula
- C9H12O
- Formula Weight
- 136.19
- MOL File
- 62285-58-9.mol
2,6-Dimethylbenzyl alcohol Property
- Melting point:
- 81-82 °C(Solv: ligroine (8032-32-4))
- Boiling point:
- 120°C 12mm
- Density
- 1.002±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.38±0.10(Predicted)
- form
- Solid
Safety
- Safety Statements
- 24/25
- HS Code
- 29062990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D481050
- Product name
- (2,6-Dimethylphenyl)methanol
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FD50915
- Product name
- 2,6-Dimethylbenzyl alcohol
- Packaging
- 2g
- Price
- $89.16
- Updated
- 2021/12/16
- Product number
- X8348
- Product name
- 2,6-Dimethylbenzylalcohol
- Packaging
- 1g
- Price
- $38
- Updated
- 2021/12/16
- Product number
- FD50915
- Product name
- 2,6-Dimethylbenzyl alcohol
- Packaging
- 1g
- Price
- $55.7
- Updated
- 2021/12/16
- Product number
- FD50915
- Product name
- 2,6-Dimethylbenzyl alcohol
- Packaging
- 5G
- Price
- $183.75
- Updated
- 2021/12/16
2,6-Dimethylbenzyl alcohol Chemical Properties,Usage,Production
Chemical Properties
White solid
Synthesis
632-46-2
62285-58-9
Synthesis of 2,6-dimethylbenzyl alcohol: The synthesis of 2,6-dimethylbenzyl alcohol was carried out with reference to the method of Beaulieu et al. (2000) but the original method was unsuccessful, so it was changed to a different reducing agent. 2,6-dimethylbenzoic acid (1.00 g, 6.65 mmol) was suspended in anhydrous THF (10 mL) under nitrogen protection and a THF solution of BH3 (SMe2) was slowly added. The reaction mixture was heated under reflux conditions for 16 h. The reaction was subsequently quenched with saturated ammonium chloride solution (5 mL) and 2 M HCl (10 mL) (note: there was a violent gas release during the reaction). The organic layer was separated and the aqueous layer was extracted three times with ethyl acetate (45 mL each time). The organic extracts were combined, washed twice sequentially with saturated sodium bicarbonate solution (20 mL each time), dried over anhydrous Na2SO4, concentrated under reduced pressure, and finally purified by silica gel column chromatography to give 2,6-dimethylbenzyl alcohol (0.50 g, 51% yield) as a white solid.1H NMR (400 MHz, CDCl3): δ7.08 (m, 3H, Ph-H), δ7.08 (m, 3H, Ph-H), δ7.08 (m, 3H, 2H), δ7.08 (m, 3H, 2H, 2H). 4.70 (s, 2H, Ph-CH2), 4.05 (br s, 1H, OH), 2.40 (s, 6H, CH3).
References
[1] Bioorganic and Medicinal Chemistry, 1996, vol. 4, # 12, p. 2167 - 2178
[2] Patent: US2016/193181, 2016, A1. Location in patent: Paragraph 1161-1162
[3] Patent: WO2008/131368, 2008, A2. Location in patent: Page/Page column 116-117
[4] Tetrahedron, 2001, vol. 57, # 30, p. 6375 - 6382
[5] ChemMedChem, 2016, vol. 11, # 23, p. 2607 - 2620
2,6-Dimethylbenzyl alcohol Preparation Products And Raw materials
Raw materials
Preparation Products
2,6-Dimethylbenzyl alcohol Suppliers
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View Lastest Price from 2,6-Dimethylbenzyl alcohol manufacturers
- Product
- 2,6-Dimethylbenzyl alcohol 62285-58-9
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-12-21