1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

Product Name: 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
CAS No.: 57616-69-0
Chemical Name: 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
Synonyms: CEDI-010;(3-Chloropropyl)pyrrolidine Hydrochloride;N-(3-Chloropropyl)pyrrolidine Hydrochloride;1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
CBNumber: CB5361951
Molecular Formula: C7H15Cl2N
Formula Weight: 184.11
MOL File: 57616-69-0.mol

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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Property

Melting point:: 134-136 °C
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: fused solid
color: Brown
InChI: InChI=1S/C7H14ClN.ClH/c8-4-3-7-9-5-1-2-6-9;/h1-7H2;1H
InChIKey: UUPCYQIIQHSPKR-UHFFFAOYSA-N
SMILES: C1CN(CCCCl)CC1.Cl

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Safety

HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C350965
Product name: (3-Chloropropyl)pyrrolidineHydrochloride
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C350965
Product name: (3-Chloropropyl)pyrrolidineHydrochloride
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: J94644
Product name: (3-Chloropropyl)pyrrolidineHCl
Packaging: 10g
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC74715
Product name: 1-(3-Chloropropyl)-pyrrolidine hydrochloride
Packaging: 2g
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC74715
Product name: 1-(3-Chloropropyl)-pyrrolidine hydrochloride
Packaging: 1g
Price: $60
Updated: 2021/12/16

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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

123-75-1

627-30-5

57616-69-0

165 mL (2 mol) of tetrandrine, 67 mL (1 mol) of 3-chloro-1-propanol and 200 mL of toluene were added sequentially to the reaction flask. The reaction mixture was heated to reflux temperature and maintained for 3 hours. Upon completion of the reaction, it was cooled to room temperature and the solid product was isolated. The solid was collected by diafiltration and the filter cake was washed with 20 mL of toluene. The temperature of the filtrate was controlled at about 75°C and 200 mL of thionyl chloride was slowly added dropwise. After the dropwise addition, the reaction was refluxed for 2 hours. At the end of the reaction, the mixture was cooled to room temperature and subsequently concentrated to dryness under reduced pressure. The resulting residue was recrystallized from anhydrous ethanol to give 105 g of the final white solid product N-(3-chloropropyl)pyrrole hydrochloride in 62.3% yield with a melting point of 169-173°C.

References

[1] Patent: US2013/85140, 2013, A1. Location in patent: Paragraph 0070; 0071

1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Suppliers

China 79 France 1 India 1 United Kingdom 2 United States 16 Global 99

Tianjin Derchemist Science & Technology Co., Ltd.

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Shanghai Raise Chemical Technology Co.,Ltd

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View Lastest Price from 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co

Product: 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE 57616-69-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1lg; 2kg; 5kg; 10kg; 100kg
Release date: 2019-08-31

57616-69-0, 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDERelated Search:

Pyrrolidine 1-(3-CHLOROPROPYL)-PYRROLIDINE 1-(3-CHLORO-3-PHENYLPROPYL)PYRROLIDINE HYDROCHLORIDE 5-CHLORO-6-((2-IMINOPYRROLIDIN-1-YL)METHYL)-5,6-DIHYDROPYRIMIDIN-4(3H)-ONE HYDROCHLORIDE 1-[(2,2-DICHLOROCYCLOPROPYL)METHYL]PYRROLIDINE 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

(3-Chloropropyl)pyrrolidine Hydrochloride

N-(3-Chloropropyl)pyrrolidine Hydrochloride

CEDI-010

57616-69-0

Amines and Anilines