1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
- Product Name
- 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
- CAS No.
- 57616-69-0
- Chemical Name
- 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
- Synonyms
- CEDI-010;(3-Chloropropyl)pyrrolidine Hydrochloride;N-(3-Chloropropyl)pyrrolidine Hydrochloride;1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
- CBNumber
- CB5361951
- Molecular Formula
- C7H15Cl2N
- Formula Weight
- 184.11
- MOL File
- 57616-69-0.mol
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Property
- Melting point:
- 134-136 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- fused solid
- color
- Brown
- InChI
- InChI=1S/C7H14ClN.ClH/c8-4-3-7-9-5-1-2-6-9;/h1-7H2;1H
- InChIKey
- UUPCYQIIQHSPKR-UHFFFAOYSA-N
- SMILES
- C1CN(CCCCl)CC1.Cl
Safety
- HazardClass
- IRRITANT
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C350965
- Product name
- (3-Chloropropyl)pyrrolidineHydrochloride
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C350965
- Product name
- (3-Chloropropyl)pyrrolidineHydrochloride
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 038289
- Product name
- 1-(3-Chloropropyl)pyrrolidine hydrochloride
- Packaging
- 500mg
- Price
- $13
- Updated
- 2021/12/16
- Product number
- 038289
- Product name
- 1-(3-Chloropropyl)pyrrolidine hydrochloride
- Packaging
- 1g
- Price
- $19
- Updated
- 2021/12/16
- Product number
- FC74715
- Product name
- 1-(3-Chloropropyl)-pyrrolidine hydrochloride
- Packaging
- 1g
- Price
- $60
- Updated
- 2021/12/16
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
123-75-1
627-30-5
57616-69-0
165 mL (2 mol) of tetrandrine, 67 mL (1 mol) of 3-chloro-1-propanol and 200 mL of toluene were added sequentially to the reaction flask. The reaction mixture was heated to reflux temperature and maintained for 3 hours. Upon completion of the reaction, it was cooled to room temperature and the solid product was isolated. The solid was collected by diafiltration and the filter cake was washed with 20 mL of toluene. The temperature of the filtrate was controlled at about 75°C and 200 mL of thionyl chloride was slowly added dropwise. After the dropwise addition, the reaction was refluxed for 2 hours. At the end of the reaction, the mixture was cooled to room temperature and subsequently concentrated to dryness under reduced pressure. The resulting residue was recrystallized from anhydrous ethanol to give 105 g of the final white solid product N-(3-chloropropyl)pyrrole hydrochloride in 62.3% yield with a melting point of 169-173°C.
References
[1] Patent: US2013/85140, 2013, A1. Location in patent: Paragraph 0070; 0071
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Suppliers
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE manufacturers
- Product
- 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE 57616-69-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1lg; 2kg; 5kg; 10kg; 100kg
- Release date
- 2019-08-31