METHANESULFONYL HYDRAZIDE

Uses

Product Name: METHANESULFONYL HYDRAZIDE
CAS No.: 10393-86-9
Chemical Name: METHANESULFONYL HYDRAZIDE
Synonyms: Methanesulphonyl hydrazide;Mesyl hydrazide;Methylsulfonyl hydrazide;METHANESULFONYL HYDRAZIDE;N-Methanesulfonylhydrazine;Methanesulfonic acid, hydrazide;METHANESULFONYL HYDRAZIDE ISO 9001：2015 REACH
CBNumber: CB5421413
Molecular Formula: CH6N2O2S
Formula Weight: 110.14
MOL File: 10393-86-9.mol

More

Less

METHANESULFONYL HYDRAZIDE Property

Melting point:: 46-48°C
Boiling point:: 229.0±23.0 °C(Predicted)
Density: 1.401±0.06 g/cm3(Predicted)
storage temp.: Storage temp. 2-8°C
pka: 9.55±0.40(Predicted)
Appearance: White to off-white Solid
Sensitive: Moisture Sensitive
BRN: 1747374
InChI: InChI=1S/CH6N2O2S/c1-6(4,5)3-2/h3H,2H2,1H3
InChIKey: VKHZYWVEBNIRLX-UHFFFAOYSA-N
SMILES: CS(NN)(=O)=O

More

Less

Safety

Hazard Codes: Xn
Risk Statements: 36/37/38-22
Safety Statements: 15-26-36
RIDADR: 1325
HazardClass: 4.1
PackingGroup: II

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H228Flammable solid

H242Heating may cause a fire

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P220Keep/Store away from clothing/…/combustible materials.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

More

Less

N-Bromosuccinimide Price

TRC

Product number: M287640
Product name: Methanesulfonohydrazide
Packaging: 100mg
Price: $65
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0165308
Product name: METHANESULFONYL HYDRAZIDE
Purity: 98.00%
Packaging: 250G
Price: $5197.5
Updated: 2021/12/16

Ambeed

Product number: A352253
Product name: Methanesulfonohydrazide
Purity: 98%
Packaging: 250mg
Price: $33
Updated: 2021/12/16

Ambeed

Product number: A352253
Product name: Methanesulfonohydrazide
Purity: 98%
Packaging: 1g
Price: $90
Updated: 2021/12/16

Ambeed

Product number: A352253
Product name: Methanesulfonohydrazide
Purity: 98%
Packaging: 5g
Price: $311
Updated: 2021/12/16

More

Less

METHANESULFONYL HYDRAZIDE Chemical Properties,Usage,Production

Uses

Methanesulfonyl hydrazine belongs to the acyl hydrazine class of organic compounds. It is an organic raw material that is widely used in organic synthesis.

Synthesis

124-63-0

10393-86-9

The general procedure for the synthesis of methanesulfonyl hydrazine from methanesulfonyl chloride is as follows: 0.12 mol of ethanol solution of methanesulfonyl chloride was slowly added dropwise to an ethanol solution containing 0.62 mol of hydrazine hydrate, and the temperature of the reaction was maintained at 10-12 °C. After the dropwise addition, the reaction mixture was stirred at room temperature for 1 hour. After completion of the reaction, the solvent was removed by distillation under reduced pressure. Subsequently, the viscous residue was transferred to the ether phase over a period of 5 days using sequential extraction. Next, the ether was removed using a rotary evaporator. The final product was recrystallized by methyl acetate and allowed to stand at low temperature for several weeks until crystals precipitated.

References

[1] Helvetica Chimica Acta, 1989, vol. 72, p. 1383 - 1389
[2] Journal of Molecular Structure, 2015, vol. 1100, p. 464 - 474
[3] Canadian Journal of Chemistry, 1956, vol. 33, p. 1250,1255
[4] Tetrahedron, 1959, vol. 7, p. 305,308
[5] Synthesis, 1993, # 5, p. 490 - 496

METHANESULFONYL HYDRAZIDE Preparation Products And Raw materials

Raw materials

Preparation Products

Ambroxol

More

Less

METHANESULFONYL HYDRAZIDE Suppliers

China 58 Germany 2 India 2 Switzerland 1 United Kingdom 1 United States 7 Global 71

PharmaBlock Sciences (Nanjing),Inc.

Tel: 025-86918202 4000255188
Fax: 86-025-86918232
Email: sales@pharmablock.com
Country: China
ProdList: 5000
Advantage: 55

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
Fax: 021-64823266
Email: chenyj@titansci.com
Country: China
ProdList: 14101
Advantage: 59

Aloespharm Co., Ltd.

Tel: 021-20960837
Fax: 021-20960837
Email: market@aloespharm.com
Country: China
ProdList: 1302
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 42446
Advantage: 60

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

Shanghai Send Pharmaceutical Technology Co., Ltd.

Tel: 021-58088081 Q2635253576
Fax: QQ3382968513
Email: hailey@shsendpharm.com
Country: China
ProdList: 2081
Advantage: 55

Chengdu RunZeBenTu Chemical Co., Ltd

Tel: 028-88469284 18000562381
Email: rzbtsj@163.com
Country: China
ProdList: 9951
Advantage: 56

skychemical Co.Ltd

Tel: 021-20960837,QQ1332204249
Fax: 021-20960837
Email: sales@skychemical.com
Country: China
ProdList: 3341
Advantage: 55

Changzhou Hopschain Chemical Co.,Ltd.

Tel: 0519-85528066 13775048983
Fax: 0519-85528066
Email: sales@hopschem.com
Country: China
ProdList: 31553
Advantage: 55

10393-86-9, METHANESULFONYL HYDRAZIDERelated Search:

Benzenesulfonyl hydrazide 4,4'-Oxybis(benzenesulfonyl hydrazide) N-Methyl-p-toluenesulfonamide 4-Methylbenzenesulfonhydrazide DIAZALD(R)-N-METHYL-13C DANSYL HYDRAZINE Diazald-N-methyl-13C-N-methyl-d3 4-METHOXYBENZENESULFONYL HYDRAZIDE 2,4,6-TRIISOPROPYLBENZENESULFONYL HYDRAZIDE 2,4,6-Trimethylbenzenesulfonyl hydrazide 1,3-DIPHENYLACETONE P-TOLUENESULFONYLHYDRAZONE 2,4,5-TRICHLOROBENZENESULFONYL HYDRAZIDE BENZALDEHYDE TOSYLHYDRAZONE 4-BROMOBENZENESULFONOHYDRAZIDE 1,2-Bis(p-tolylsulfonyl)hydrazine, N,Nμ-Ditosylhydrazine, 4-Methylbenzenesulfonic acid 2-[(4-methylphenyl)sulfonyl]hydrazide 2-NITROBENZALDEHYDE TOSYLHYDRAZONE METHANESULFONYL HYDRAZIDE 10MG [R] N-[4-(HYDRAZINOSULFONYL)PHENYL]ACETAMIDE

METHANESULFONYL HYDRAZIDE

Mesyl hydrazide

Methanesulphonyl hydrazide

Methanesulfonic acid, hydrazide

METHANESULFONYL HYDRAZIDE ISO 9001：2015 REACH

Methylsulfonyl hydrazide

N-Methanesulfonylhydrazine

10393-86-9

CH6N2O2S