2-HYDROXYMETHYL-1,3-DIOXOLANE

Product Name: 2-HYDROXYMETHYL-1,3-DIOXOLANE
CAS No.: 5694-68-8
Chemical Name: 2-HYDROXYMETHYL-1,3-DIOXOLANE
Synonyms: 1,3-dioxane-2-methanol;1,3-Dioxolane-2-methanol;2-HYDROXYMETHYL-1,3-DIOXOLANE;2-HydroxyMethyl-1,3-dioxolaneC4H8O3
CBNumber: CB5439179
Molecular Formula: C4H8O3
Formula Weight: 104.1
MOL File: 5694-68-8.mol

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2-HYDROXYMETHYL-1,3-DIOXOLANE Property

Boiling point:: 97 °C
Density: 1.164±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 14.83±0.10(Predicted)
form: liquid
color: Colourless to light yellow
InChI: InChI=1S/C4H8O3/c5-3-4-6-1-2-7-4/h4-5H,1-3H2
InChIKey: ZAGUSKAXELYWCE-UHFFFAOYSA-N
SMILES: O1CCOC1CO

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Safety

RIDADR: UN1993
HS Code: 2909200090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: D495680
Product name: (1,3-Dioxolan-2-yl)methanol
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 2093AL
Product name: 2-Hydroxymethyl-1,3-dioxolane
Packaging: 10g
Price: $512
Updated: 2021/12/16

Ambeed

Product number: A220670
Product name: (1,3-Dioxolan-2-yl)methanol
Purity: 95%
Packaging: 250mg
Price: $20
Updated: 2021/12/16

Ambeed

Product number: A220670
Product name: (1,3-Dioxolan-2-yl)methanol
Purity: 95%
Packaging: 1g
Price: $58
Updated: 2021/12/16

ACHEMBLOCK

Product number: O33317
Product name: (1,3-dioxolan-2-yl)methanol
Purity: 97%
Packaging: 1G
Price: $100
Updated: 2021/12/16

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2-HYDROXYMETHYL-1,3-DIOXOLANE Chemical Properties,Usage,Production

Synthesis

71516-48-8

5694-68-8

General procedure for the synthesis of 1,3-dioxane-2-methanol from the compound (CAS: 71516-48-8): (66b) Preparation of 1,3-dioxan-2-ylmethanol: To a solution of 2-((benzyloxy)methyl)-1,3-dioxan-2-ylmethanol (3.01 g, 15.5 mmol) in methanol (100 mL), obtained in the previous step (66a), was Palladium hydroxide (20 wt% Pd (dry basis) carbon, wet (up to 50% water)) (300 mg) was added. The reaction mixture was stirred at room temperature for 15 hours under hydrogen atmosphere. Upon completion of the reaction, the gas in the reaction vessel was displaced with nitrogen, the catalyst was removed by filtration through diatomaceous earth and washed with methanol. The filtrate was concentrated and dried under reduced pressure to afford 1,3-dioxane-2-methanol (1.57 g, 97.3% yield) as a light yellow oil.1H NMR (400 MHz, CDCl3) δ ppm: 1.89 (1H, br s), 3.66-3.72 (2H, m), 3.88-4.08 (4H, m), 5.01 (1H, t, J = 3 Hz).

References

[1] Patent: US2007/10542, 2007, A1. Location in patent: Page/Page column 82

2-HYDROXYMETHYL-1,3-DIOXOLANE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-HYDROXYMETHYL-1,3-DIOXOLANE manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 2-HYDROXYMETHYL-1,3-DIOXOLANE 5694-68-8
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-03-19

5694-68-8, 2-HYDROXYMETHYL-1,3-DIOXOLANERelated Search:

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2-HYDROXYMETHYL-1,3-DIOXOLANE

1,3-Dioxolane-2-methanol

2-HydroxyMethyl-1,3-dioxolaneC4H8O3

1,3-dioxane-2-methanol

5694-68-8