3',5'-Dichloroacetophenone

Product Name: 3',5'-Dichloroacetophenone
CAS No.: 14401-72-0
Chemical Name: 3',5'-Dichloroacetophenone
Synonyms: Ketoconazole Impurity 49;3',5'-Dichloroacetophenone;3',5'-dichloroacetophenone;1-Acetyl-3,5-dichlorobenzene;3,5-Dichlorophenacylchloride;Methyl 3,5-dichlorophenyl ketone;1-(3,5-dichlorophenyl)ethan-1-one;Methanone,(6-methylphenyl)phenyl-;Ethanone, 1-(3,5-dichlorophenyl)-;3',5'-Dichloroacetophenone≥ 98% (GC)
CBNumber: CB5444490
Molecular Formula: C8H6Cl2O
Formula Weight: 189.04
MOL File: 14401-72-0.mol

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3',5'-Dichloroacetophenone Property

Melting point:: 26 °C
Boiling point:: 82°C 0,1mm
Density: 1.304±0.06 g/cm3(Predicted)
refractive index: 1.5630 to 1.5670
storage temp.: Sealed in dry,Room Temperature
form: clear liquid
color: Colorless to Light yellow to Light orange
CAS DataBase Reference: 14401-72-0(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39-25/26
HS Code: 29147000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D5111
Product name: 3',5'-Dichloroacetophenone
Purity: >98.0%(GC)
Packaging: 1g
Price: $39
Updated: 2025/07/31

TCI Chemical

Product number: D5111
Product name: 3',5'-Dichloroacetophenone
Purity: >98.0%(GC)
Packaging: 5g
Price: $106
Updated: 2025/07/31

TRC

Product number: D474458
Product name: 1-(3,5-Dichlorophenyl)ethanone
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 070761
Product name: 3',5'-Dichloroacetophenone
Purity: 98%
Packaging: 1g
Price: $15
Updated: 2021/12/16

Matrix Scientific

Product number: 070761
Product name: 3',5'-Dichloroacetophenone
Purity: 98%
Packaging: 5g
Price: $45
Updated: 2021/12/16

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3',5'-Dichloroacetophenone Chemical Properties,Usage,Production

Chemical Properties

Light yellow liquid

Synthesis

3032-81-3

108-24-7

14401-72-0

General procedure for the synthesis of 1-(3,5-dichlorophenyl)ethanone from 3,5-dichloroiodobenzene (37.0 g, 136 mmol) and acetic anhydride: 3,5-dichloroiodobenzene, Pd2(dba)3 (1.5 g, 1.6 mmol), and lithium chloride (29.0 g, 682 mmol) were dissolved in 100 ml of DMF in a 500 ml round bottomed flask. Subsequently 64.0 ml of acetic anhydride and 47.0 ml of N-ethyl diisopropylamine were added to the reaction mixture. The reaction mixture was heated at 100°C for the reaction. After completion of the reaction, water was added to the mixture, extracted with ethyl acetate and the product was purified by column chromatography using ethyl acetate as eluent. 8 g of 1-(3,5-dichlorophenyl)ethanone was finally obtained.

References

[1] Patent: JP2015/212297, 2015, A. Location in patent: Paragraph 0106; 0107

3',5'-Dichloroacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

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3',5'-Dichloroacetophenone Suppliers

Americas 1 China 122 Europe 3 Germany 1 India 2 Japan 1 Ukraine 2 United Kingdom 9 United States 19 Global 160

J & K SCIENTIFIC LTD.

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Syntechem Co.,Ltd

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View Lastest Price from 3',5'-Dichloroacetophenone manufacturers

Career Henan Chemical Co

Product: 3',5'-Dichloroacetophenone 14401-72-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-05-23

14401-72-0, 3',5'-DichloroacetophenoneRelated Search:

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Methyl 3,5-dichlorophenyl ketone

1-(3,5-dichlorophenyl)ethan-1-one

1-Acetyl-3,5-dichlorobenzene

3',5'-Dichloroacetophenone≥ 98% (GC)

Ethanone, 1-(3,5-dichlorophenyl)-

Methanone,(6-methylphenyl)phenyl-

3',5'-dichloroacetophenone

Ketoconazole Impurity 49

3,5-Dichlorophenacylchloride

3′,5′-Dichloroacetophenone, CAS 14401-72-0

3',5'-Dichloroacetophenone

14401-72-0

Aromatic Acetophenones & Derivatives (substituted)

Adehydes, Acetals & Ketones

Chlorine Compounds