2-(Dimethylamino)pyridine-5-boronic acid hydrate
- Product Name
- 2-(Dimethylamino)pyridine-5-boronic acid hydrate
- CAS No.
- 579525-46-5
- Chemical Name
- 2-(Dimethylamino)pyridine-5-boronic acid hydrate
- Synonyms
- 2-DiMethylaMino-5-pyridineboronic acid;2-(Dimethylamino)pyridine-5-boronicacid;5-Borono-2-(dimethylamino)pyridine hydrate;6-(dimethylamino)pyridin-3-yl-3-boronic acid;B-[6-(Dimethylamino)-3-pyridinyl]boronic acid;2-(Dimethylamino)pyridine-5-boronic acid 97%;B-[6-(Dimethylamino)-pyridin-3-yl]boronic acid;6-(DIMETHYLAMINO)PYRIDINE-3-BORONIC ACID HYDRATE;2-(DIMETHYLAMINO)PYRIDINE-5-BORONIC ACID HYDRATE;Boronic acid, B-[6-(dimethylamino)-3-pyridinyl]-
- CBNumber
- CB5457434
- Molecular Formula
- C7H11BN2O2
- Formula Weight
- 165.99
- MOL File
- 579525-46-5.mol
2-(Dimethylamino)pyridine-5-boronic acid hydrate Property
- Boiling point:
- 352.3±52.0 °C(Predicted)
- Density
- 1.19±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- solubility
- DMSO (Slightly), Methanol (Slightly)
- pka
- 4.21±0.10(Predicted)
- form
- Solid
- color
- Yellow
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- D479165
- Product name
- 6-(Dimethylamino)pyridine-3-boronicacid
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- OR2617
- Product name
- 2-(Dimethylamino)pyridine-5-boronicacid
- Purity
- 97%
- Packaging
- 1g
- Price
- $172
- Updated
- 2021/12/16
- Product number
- 8H60-1-75
- Product name
- 2-(Dimethylamino)pyridine-5-boronic acid
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
- Product number
- X0891
- Product name
- 6-(Dimethylamino)pyridine-3-boronicacid
- Packaging
- 1g
- Price
- $196
- Updated
- 2021/12/16
- Product number
- BOR0000862
- Product name
- 6-(DIMETHYLAMINO)PYRIDIN-3-YLBORONIC ACID
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $225.75
- Updated
- 2021/12/16
2-(Dimethylamino)pyridine-5-boronic acid hydrate Chemical Properties,Usage,Production
Uses
2-(Dimethylamino)pyridine-5-boronic acid, hydrade
Synthesis
26163-07-5
73183-34-3
579525-46-5
General procedure for the synthesis of 2-(dimethylamino)pyridine-5-boronic acid from 5-bromo-N,N-dimethylpyridin-2-amine and pinacol ester of bis(boronic acid): to a solution of 1,4-dioxane (20 mL) in 5-bromo-N,N-dimethylpyridin-2-amine (400 mg, 1.989 mmol), was added sequentially 4,4,4',4',5,5,5',5'-octa methyl-2,2'-bis(1,3,2-dioxaborolane) (606 mg, 2.387 mmol), PdCl2(dppf)-CH2Cl2 adduct (162 mg, 0.199 mmol) and potassium acetate (390 mg, 3.98 mmol). The reaction mixture was heated to 100 °C and stirred overnight under nitrogen protection. After completion of the reaction, the mixture was filtered and the filtrate was concentrated under vacuum to afford the crude product (6-(dimethylamino)pyridin-3-yl)boronic acid (420 mg, 0.496 mmol, 25% yield) as a brown oil.LCMS analysis showed the [M+H]+ peak at 167.1.
References
[1] Patent: WO2017/98440, 2017, A1. Location in patent: Page/Page column 170
2-(Dimethylamino)pyridine-5-boronic acid hydrate Preparation Products And Raw materials
Raw materials
Preparation Products
2-(Dimethylamino)pyridine-5-boronic acid hydrate Suppliers
- Tel
- +91-11-26135922 or +91-11-46160359
- Fax
- +91-11-26124735
- labex@labex.net
- Country
- India
- ProdList
- 391
- Advantage
- 55
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 2-(Dimethylamino)pyridine-5-boronic acid hydrate manufacturers
- Product
- 2-(Dimethylamino)pyridine-5-boronic acid hydrate 579525-46-5
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
- Product
- 2-(Dimethylamino)pyridine-5-boronic acid hydrate 579525-46-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-25