2,6-DICHLORODIPHENYLAMINE
- Product Name
- 2,6-DICHLORODIPHENYLAMINE
- CAS No.
- 15307-93-4
- Chemical Name
- 2,6-DICHLORODIPHENYLAMINE
- Synonyms
- EOS-60715;TIMTEC-BB SBB003229;Diclofenac Impurity 6;2,6-dichlorobisaniline;Meclofenamic acid IMP;,6-DICHLORODIPHENYLAMINE;2,6-DICHLORODIPHENYLAMINE;Meclofenamic acid Impurity;Diphenylamine,2,6-dichloro-;N-Phenyl-2,6-Dichloroanilie
- CBNumber
- CB5673405
- Molecular Formula
- C12H9Cl2N
- Formula Weight
- 238.11
- MOL File
- 15307-93-4.mol
2,6-DICHLORODIPHENYLAMINE Property
- Melting point:
- 50-53 °C(lit.)
- Boiling point:
- 115 °C(Press: 0.01 Torr)
- Density
- 1.327±0.06 g/cm3(Predicted)
- Flash point:
- >230 °F
- storage temp.
- 2-8°C
- solubility
- Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- -2.57±0.40(Predicted)
- color
- Pale brown
- BRN
- 2725987
- InChI
- InChI=1S/C12H9Cl2N/c13-10-7-4-8-11(14)12(10)15-9-5-2-1-3-6-9/h1-8,15H
- InChIKey
- HDUUZPLYVVQTKN-UHFFFAOYSA-N
- SMILES
- C1(NC2=CC=CC=C2)=C(Cl)C=CC=C1Cl
- CAS DataBase Reference
- 15307-93-4(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,N
- Risk Statements
- 36/37/38-50/53-36/38
- Safety Statements
- 26-36-61-60
- RIDADR
- UN 3077 9 / PGIII
- WGK Germany
- 3
- HS Code
- 29214200
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 75538
- Product name
- 2,6-Dichlorodiphenylamine
- Purity
- analytical standard
- Packaging
- 100mg
- Price
- $62.6
- Updated
- 2025/07/31
- Product number
- D3778
- Product name
- 2,6-Dichlorodiphenylamine
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $50
- Updated
- 2025/07/31
- Product number
- D3778
- Product name
- 2,6-Dichlorodiphenylamine
- Purity
- >98.0%(GC)
- Packaging
- 250g
- Price
- $200
- Updated
- 2025/07/31
- Product number
- D434060
- Product name
- N-(2,6-Dichlorophenyl)aniline
- Packaging
- 5g
- Price
- $135
- Updated
- 2021/12/16
- Product number
- FD133300
- Product name
- (2,6-Dichlorophenyl)phenylamine
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
2,6-DICHLORODIPHENYLAMINE Chemical Properties,Usage,Production
Chemical Properties
Light brown powder
Uses
N-(2,6-Dichlorophenyl)aniline is an analog of Diclofenac (D436450), a nonsteroidal anti-inflammatory compound an decycloxygenase (COX) inhibitor.
Synthesis
146607-19-4
15307-93-4
The general procedure for the synthesis of 2,6-dichloro-N-phenylaniline from the compound (CAS:146607-19-4) was as follows: compound II (272 g, 0.92 mol) was added to a dry four-necked flask with toluene (800 g, 8.7 mol) and heated to 90 °C. Sodium hydroxide (total 14.8 g, 0.37 mol) was added in three portions under stirring, followed by refluxing the reaction mixture for 3 hours. After completion of the reaction, the mixture was cooled to below 80°C. 184 mL of distilled water was added to the reaction flask and the temperature was raised to 90 °C with continuous stirring for 1 hour. The reaction solution was transferred to a dispensing funnel and washed sequentially by adding 46 mL of water and 28 mL of hydrochloric acid. The washed organic phase was transferred to a distillation flask and toluene was removed by distillation under reduced pressure. Finally 203.4 g of light yellow solid product was obtained as N-(2,6-dichlorophenyl)aniline (Compound III) in 93% yield.
References
[1] Patent: CN106905178, 2017, A. Location in patent: Paragraph 0021; 0040; 0041
2,6-DICHLORODIPHENYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-DICHLORODIPHENYLAMINE manufacturers
- Product
- 2,6-DICHLORODIPHENYLAMINE 15307-93-4
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-07
- Product
- 2,6-DICHLORODIPHENYLAMINE 15307-93-4
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-29
- Product
- 2,6-DICHLORODIPHENYLAMINE 15307-93-4
- Price
- US $80.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000tons
- Release date
- 2023-09-11