ChemicalBook > CAS DataBase List > 2,6-DICHLORODIPHENYLAMINE

2,6-DICHLORODIPHENYLAMINE

Product Name
2,6-DICHLORODIPHENYLAMINE
CAS No.
15307-93-4
Chemical Name
2,6-DICHLORODIPHENYLAMINE
Synonyms
EOS-60715;TIMTEC-BB SBB003229;Diclofenac Impurity 6;2,6-dichlorobisaniline;Meclofenamic acid IMP;,6-DICHLORODIPHENYLAMINE;2,6-DICHLORODIPHENYLAMINE;Meclofenamic acid Impurity;Diphenylamine,2,6-dichloro-;N-Phenyl-2,6-Dichloroanilie
CBNumber
CB5673405
Molecular Formula
C12H9Cl2N
Formula Weight
238.11
MOL File
15307-93-4.mol
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2,6-DICHLORODIPHENYLAMINE Property

Melting point:
50-53 °C(lit.)
Boiling point:
115 °C(Press: 0.01 Torr)
Density 
1.327±0.06 g/cm3(Predicted)
Flash point:
>230 °F
storage temp. 
2-8°C
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form 
Solid
pka
-2.57±0.40(Predicted)
color 
Pale brown
BRN 
2725987
InChI
InChI=1S/C12H9Cl2N/c13-10-7-4-8-11(14)12(10)15-9-5-2-1-3-6-9/h1-8,15H
InChIKey
HDUUZPLYVVQTKN-UHFFFAOYSA-N
SMILES
C1(NC2=CC=CC=C2)=C(Cl)C=CC=C1Cl
CAS DataBase Reference
15307-93-4(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,N
Risk Statements 
36/37/38-50/53-36/38
Safety Statements 
26-36-61-60
RIDADR 
UN 3077 9 / PGIII
WGK Germany 
3
HS Code 
29214200
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
75538
Product name
2,6-Dichlorodiphenylamine
Purity
analytical standard
Packaging
100mg
Price
$62.6
Updated
2025/07/31
TCI Chemical
Product number
D3778
Product name
2,6-Dichlorodiphenylamine
Purity
>98.0%(GC)
Packaging
25g
Price
$50
Updated
2025/07/31
TCI Chemical
Product number
D3778
Product name
2,6-Dichlorodiphenylamine
Purity
>98.0%(GC)
Packaging
250g
Price
$200
Updated
2025/07/31
TRC
Product number
D434060
Product name
N-(2,6-Dichlorophenyl)aniline
Packaging
5g
Price
$135
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD133300
Product name
(2,6-Dichlorophenyl)phenylamine
Packaging
1g
Price
$105
Updated
2021/12/16
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2,6-DICHLORODIPHENYLAMINE Chemical Properties,Usage,Production

Chemical Properties

Light brown powder

Uses

N-(2,6-Dichlorophenyl)aniline is an analog of Diclofenac (D436450), a nonsteroidal anti-inflammatory compound an decycloxygenase (COX) inhibitor.

Synthesis

146607-19-4

15307-93-4

The general procedure for the synthesis of 2,6-dichloro-N-phenylaniline from the compound (CAS:146607-19-4) was as follows: compound II (272 g, 0.92 mol) was added to a dry four-necked flask with toluene (800 g, 8.7 mol) and heated to 90 °C. Sodium hydroxide (total 14.8 g, 0.37 mol) was added in three portions under stirring, followed by refluxing the reaction mixture for 3 hours. After completion of the reaction, the mixture was cooled to below 80°C. 184 mL of distilled water was added to the reaction flask and the temperature was raised to 90 °C with continuous stirring for 1 hour. The reaction solution was transferred to a dispensing funnel and washed sequentially by adding 46 mL of water and 28 mL of hydrochloric acid. The washed organic phase was transferred to a distillation flask and toluene was removed by distillation under reduced pressure. Finally 203.4 g of light yellow solid product was obtained as N-(2,6-dichlorophenyl)aniline (Compound III) in 93% yield.

References

[1] Patent: CN106905178, 2017, A. Location in patent: Paragraph 0021; 0040; 0041

2,6-DICHLORODIPHENYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-DICHLORODIPHENYLAMINE Suppliers

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View Lastest Price from 2,6-DICHLORODIPHENYLAMINE manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
2,6-DICHLORODIPHENYLAMINE 15307-93-4
Price
US $0.00/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10000KGS
Release date
2025-05-07
Shaanxi Dideu New Materials Co. Ltd
Product
2,6-DICHLORODIPHENYLAMINE 15307-93-4
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000KGS
Release date
2025-03-29
Anhui Ruihan Technology Co., Ltd
Product
2,6-DICHLORODIPHENYLAMINE 15307-93-4
Price
US $80.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000tons
Release date
2023-09-11

15307-93-4, 2,6-DICHLORODIPHENYLAMINERelated Search:


  • 2,6-DICHLORODIPHENYLAMINE
  • 2,6-dichloro-N-phenylaniline
  • N-PHENYL-2,6-DICHLOROANILINE
  • TIMTEC-BB SBB003229
  • 2,6-dichlorobisaniline
  • 2,6 Dichloro di phenol amine
  • ,6-DICHLORODIPHENYLAMINE
  • Benzenamine, 2,6-dichloro-N-phenyl-
  • Diphenylamine,2,6-dichloro-
  • N-Phenyl-2,6-dichlorophenylaniline
  • 2,6-Dichlorophenylphenylamine
  • N-Phenyl-2,6-dichlorobenzenamine
  • N-(2,6-DICHLOROPHENYL)ANILINEDICLOFENAC SODIUM
  • N-(2,6-Dichlorophenyl)aniline
  • 2,6-Dichloro-N-phenylbenzamine
  • Diclofenac Desacetate Impurity
  • Meclofenamic acid Impurity
  • Meclofenamic acid IMP
  • EOS-60715
  • Diclofenac Impurity 6
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  • 2,6-Dichlorodiphenylamine&gt
  • 2,6-Dichloro-N-phenylbenzenamine
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  • 2,6-Dichlorodiphenylamine in methanol
  • 2,6-Dichlorodiphenylamine, 10 mM in DMSO
  • 15307-93-4
  • 15307-93-9
  • Cl2C6H3NHC6H5
  • Nitrogen Compounds
  • Organic Building Blocks
  • C11 to C37
  • Building Blocks
  • Amines
  • Amines
  • Building Blocks
  • C12
  • Chemical Synthesis
  • Nitrogen Compounds
  • Organic Building Blocks
  • Anilines, Aromatic Amines and Nitro Compounds
  • 15307-93-4