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(1H-IMIDAZOL-4-YL)METHANAMINE

Product Name
(1H-IMIDAZOL-4-YL)METHANAMINE
CAS No.
13400-46-9
Chemical Name
(1H-IMIDAZOL-4-YL)METHANAMINE
Synonyms
4-(AMinoMethyl)iMidazole;1H-IMIDAZOLE-5-METHANAMINE;4-aminomethyl-1H-imidazole;(1H-imidazol-5-yl)methanamine;(1H-IMIDAZOL-4-YL)METHANAMINE;1H-IMIDAZOL-4-YL)METHANAMINEV;1-(1H-imidazol-5-yl)methanamine;1-(1H-imidazol-4-yl)methanamine;C-(1H-Imidazol-4-yl)-methylamine;C-(1H-Imidazol-4(5)-yl)-methylamine
CBNumber
CB5726329
Molecular Formula
C4H7N3
Formula Weight
97.12
MOL File
13400-46-9.mol
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(1H-IMIDAZOL-4-YL)METHANAMINE Property

Boiling point:
341.9±17.0 °C(Predicted)
Density 
1.199±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
14.33±0.10(Predicted)
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Safety

Hazard Codes 
Xi
HS Code 
2933299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific
Product number
144345
Product name
(1H-Imidazol-4-yl)methanamine
Purity
95%
Packaging
1g
Price
$607
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0148947
Product name
1H-IMIDAZOL-4-YLMETHYLAMINE
Purity
95.00%
Packaging
1G
Price
$768.88
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0148947
Product name
1H-IMIDAZOL-4-YLMETHYLAMINE
Purity
95.00%
Packaging
5G
Price
$1413.15
Updated
2021/12/16
Matrix Scientific
Product number
144345
Product name
(1H-Imidazol-4-yl)methanamine
Purity
95%
Packaging
5g
Price
$1702
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0148947
Product name
1H-IMIDAZOL-4-YLMETHYLAMINE
Purity
95.00%
Packaging
10G
Price
$2207.51
Updated
2021/12/16
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(1H-IMIDAZOL-4-YL)METHANAMINE Chemical Properties,Usage,Production

Synthesis

(1H-imidazol-4-yl)methanamine is prepared by adding hydroxylamine hydrochloride to a reaction mixture of 4-imidazolecarboxaldehyde, sodium carbonate and distilled water.
Experiment steps:Hydroxylamine hydrochloride (1.27 g, 18.3 mmol) was added to a reaction mixture of 4-imidazolecarboxaldehyde (800 mg, 8.3 mmol), sodium carbonate (445 mg, 4.2mmol) and distilled water (14 ml) and was left to react overnight at room temperature with stirring. The resultant mixture was then concentrated in vacuo to 3 ml and placed in an ice bath for precipitation to occur. Solid formed was collected by filtration, dissolved and recrystallized in ethanol to afford the colourless powder oxime, 1H-imidazole-4-carbaldehyde oxime (330 mg). Acetyl chloride (1.06 ml) was added dropwise into methanol (39 ml) in a round bottom flask at 0 °C under nitrogen purge and left to stir for 30 minutes. The oxime was then added into the reaction mixture followed by addition of palladium on carbon, 5% (296 mg, 2.40 mmol). The reaction mixture was hydrogenated at atmospheric pressure overnight. The resultant mixture was then filtered through celite pad, washed with methanol (30 ml) where the filtrate was then collected and concentrated in vacuo to give (1H-imidazol-4-yl)methanamine as a colourless powder (274 mg, 34%).

(1H-IMIDAZOL-4-YL)METHANAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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13400-46-9, (1H-IMIDAZOL-4-YL)METHANAMINERelated Search:


  • (1H-IMIDAZOL-4-YL)METHANAMINE
  • C-(1H-Imidazol-4-yl)-methylamine
  • 1H-IMIDAZOLE-5-METHANAMINE
  • 1H-IMIDAZOL-4-YL)METHANAMINEV
  • 4-(AMinoMethyl)iMidazole
  • 1H-iMidazole-5-MethanaMine(HCl salt)
  • C-(1H-Imidazol-4(5)-yl)-methylamine
  • 4-aminomethyl-1H-imidazole
  • (1H-imidazol-5-yl)methanamine
  • 1-(1H-imidazol-4-yl)methanamine
  • 1-(1H-imidazol-5-yl)methanamine
  • 13400-46-9
  • pharmacetical