3-CHLORO-4-METHOXYBENZALDEHYDE
- Product Name
- 3-CHLORO-4-METHOXYBENZALDEHYDE
- CAS No.
- 4903-09-7
- Chemical Name
- 3-CHLORO-4-METHOXYBENZALDEHYDE
- Synonyms
- 40903-09-7;AKOS B029259;TIMTEC-BB SBB003854;CHEMBRDG-BB 6945816;3-chloroanisaldehyde;3-CHLORO-P-ANISALDEHYDE;3-CHLORO-4-METHOXYBENZALDEHYDE;3-Chloro-p-anisaldehyde;4-Methoxy-3-chlorobenzaldehyde;3-CHLORO-P-ANISALDEHYDE, 98+% GC
- CBNumber
- CB5728000
- Molecular Formula
- C8H7ClO2
- Formula Weight
- 170.59
- MOL File
- 4903-09-7.mol
3-CHLORO-4-METHOXYBENZALDEHYDE Property
- Melting point:
- 56-60 °C (lit.)
- Boiling point:
- 128 °C(Press: 5 Torr)
- Density
- 1.244±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- color
- White to Almost white
- Sensitive
- Air Sensitive
- CAS DataBase Reference
- 4903-09-7(CAS DataBase Reference)
Safety
- Safety Statements
- 22-24/25
- WGK Germany
- 3
- HS Code
- 29130000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 565040
- Product name
- 3-Chloro-4-methoxybenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $73.81
- Updated
- 2025/07/31
- Product number
- 565040
- Product name
- 3-Chloro-4-methoxybenzaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $178.6
- Updated
- 2025/07/31
- Product number
- C1797
- Product name
- 3-Chloro-p-anisaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $50
- Updated
- 2025/07/31
- Product number
- C1797
- Product name
- 3-Chloro-p-anisaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $143
- Updated
- 2025/07/31
- Product number
- C368965
- Product name
- 3-Chloro-4-methoxybenzenecarbaldehyde
- Packaging
- 10mg
- Price
- $60
- Updated
- 2021/12/16
3-CHLORO-4-METHOXYBENZALDEHYDE Chemical Properties,Usage,Production
Uses
3-Chloro-4-methoxybenzaldehyde is mainly used in organic synthesis, as a drug intermediate and chemical reagent, and is widely used in pharmaceuticals, materials science and other fields.
Synthesis
2420-16-8
74-88-4
4903-09-7
Potassium carbonate (K2CO3, 7.6 g, 55.238 mmol) was added to a stirred solution of 3-chloro-4-hydroxybenzaldehyde (2.9 g, 18.412 mmol) in N,N-dimethylformamide (DMF, 30 mL). Iodomethane (CH3I, 7.80 g, 55.238 mmol) was added slowly and dropwise at room temperature under inert atmosphere. After the dropwise addition, the reaction mixture was heated to 80 °C and stirred continuously for 1 hour. Upon completion of the reaction, the reaction was quenched with deionized water (20 mL) and subsequently extracted with ethyl acetate (EtOAc, 2 x 50 mL). The organic phases were combined, washed sequentially with deionized water and saturated saline, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography to afford 3-chloro-4-methoxybenzaldehyde (2.78 g, 93% yield) as a yellow solid.
References
[1] Patent: US2003/176481, 2003, A1
[2] Patent: WO2009/158393, 2009, A1. Location in patent: Page/Page column 113-114
[3] Patent: US6313146, 2001, B1
[4] Patent: US6582351, 2003, B1
3-CHLORO-4-METHOXYBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-CHLORO-4-METHOXYBENZALDEHYDE Suppliers
- Tel
- --
- Fax
- --
- chemcontrol@nextra.sk
- Country
- Slovakia
- ProdList
- 6700
- Advantage
- 60
View Lastest Price from 3-CHLORO-4-METHOXYBENZALDEHYDE manufacturers
- Product
- 3-Chloro-p-anisaldehyde 4903-09-7
- Price
- US $0.00-0.00/g
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-15