3-AMINO-5-BROMO-PYRIDIN-2-OL

Product Name: 3-AMINO-5-BROMO-PYRIDIN-2-OL
CAS No.: 98786-86-8
Chemical Name: 3-AMINO-5-BROMO-PYRIDIN-2-OL
Synonyms: 3-Amino-5-bromo-2-pyridinol;3-AMINO-5-BROMO-PYRIDIN-2-OL;3-Amino-5-bromo-2-hydroxypyrid;3-Amino-5-bromo-1H-pyridin-2-one;3-AMino-5-broMopyridin-2(1H)-one;3-Amino-5-bromo-2(1H)-pyridinone;3-amino-2-hydro-5-bromo pyridine;5-bromo-2-hydroxy-3-aminopyridine;3-AMINO-5-BROMO-2-HYDROXYPYRIDINE;2-Pyridinol,3-amino-5-bromo- (6CI)
CBNumber: CB5742473
Molecular Formula: C5H5BrN2O
Formula Weight: 189.01
MOL File: 98786-86-8.mol

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3-AMINO-5-BROMO-PYRIDIN-2-OL Property

Melting point:: 182-184 °C
Boiling point:: 295.1±40.0 °C(Predicted)
Density: 1.826±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 11.81±0.10(Predicted)
form: Solid
Appearance: Off-white to gray Solid
InChI: InChI=1S/C5H5BrN2O/c6-3-1-4(7)5(9)8-2-3/h1-2H,7H2,(H,8,9)
InChIKey: ULOVLVWNSQNABA-UHFFFAOYSA-N
SMILES: C1(=O)NC=C(Br)C=C1N

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: A594475
Product name: 3-Amino-5-bromo-2-hydroxypyridine
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: A594475
Product name: 3-Amino-5-bromo-2-hydroxypyridine
Packaging: 250mg
Price: $55
Updated: 2021/12/16

AK Scientific

Product number: W9855
Product name: 3-Amino-5-bromo-2-hydroxypyridine
Packaging: 250mg
Price: $14
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA55530
Product name: 3-Amino-5-bromo-2-hydroxypyridine
Packaging: 250mg
Price: $72.5
Updated: 2021/12/16

Matrix Scientific

Product number: 073538
Product name: 3-Amino-5-bromopyridin-2-ol
Purity: 95+%
Packaging: 1g
Price: $90
Updated: 2021/12/16

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3-AMINO-5-BROMO-PYRIDIN-2-OL Chemical Properties,Usage,Production

Chemical Properties

Pale yellow to light brown solid

Synthesis

15862-34-7

98786-86-8

The general procedure for the synthesis of 3-amino-5-bromopyridin-2-one from 5-bromo-2-hydroxy-3-nitropyridine was as follows: a mixture of 5-bromo-3-nitropyridin-2-ol (1.26 g, 4.6 mmol) and tin chloride dihydrate (3.91 g, 17.3 mmol) in ethyl acetate (19.3 mL) was heated and reacted for 20 hours at 50 °C. After completion of the reaction, the mixture was cooled to room temperature, diluted with ethyl acetate (100 mL) and washed with saturated saline. After separation of the aqueous layer, the aqueous layer was extracted several times with ethyl acetate (5 x 50 mL). All organic layers were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 580 mg (53% yield) of the black solid product 3-amino-5-bromopyridin-2-one, which can be used directly in subsequent reactions without further purification.

References

[1] Patent: US2005/256137, 2005, A1. Location in patent: Page/Page column 10
[2] Yakugaku Zasshi, 1951, vol. 71, p. 169,172
[3] Chem.Abstr., <1952> 8108,
[4] Chemical and Pharmaceutical Bulletin, 1959, vol. 7, p. 720,724
[5] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999, vol. 38, # 9, p. 1036 - 1040

3-AMINO-5-BROMO-PYRIDIN-2-OL Preparation Products And Raw materials

Raw materials

Sodium chloride 2-Amino-5-bromopyridine Nitric acid Iron Sulfuric acid

Preparation Products

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3-AMINO-5-BROMO-PYRIDIN-2-OL Suppliers

China 97 Europe 1 France 1 India 4 United Kingdom 2 United States 13 Global 118

Nanjing Duolong Bio-tech Co.,Ltd.

Tel: 18905173768
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ShangHai AmK Pharmaceutical Technology Co., Ltd.

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Alfa Aesar

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JinYan Chemicals(ShangHai) Co.,Ltd.

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Pure Chemistry Scientific Inc.

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Tetranov Biopharm

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Accela ChemBio Co.,Ltd.

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Shanghai Hanhong Scientific Co.,Ltd.

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China Langchem Inc.

Tel: 0086-21-58956006
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View Lastest Price from 3-AMINO-5-BROMO-PYRIDIN-2-OL manufacturers

Dideu Industries Group Limited

Product: 3-AMINO-5-BROMO-PYRIDIN-2-OL 98786-86-8
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-09-26

Zhuozhou Wenxi import and Export Co., Ltd

Product: 3-AMINO-5-BROMO-PYRIDIN-2-OL 98786-86-8
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-11

Career Henan Chemical Co

Product: 3-AMINO-5-BROMO-PYRIDIN-2-OL 98786-86-8
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-01-09

98786-86-8, 3-AMINO-5-BROMO-PYRIDIN-2-OLRelated Search:

5-BROMO-2-METHYLPYRIDIN-3-AMINE 3-AMINO-5-BROMO-2-METHOXYPYRIDINE 2-Hydroxy-5-bromopyridine 3-Amino-5-bromopyridine 3-AMINO-5-BROMO-PYRIDIN-4-OL 3-AMINO-6-BROMO-PYRIDIN-2-OL

3-AMINO-5-BROMO-2-HYDROXYPYRIDINE

3-AMINO-5-BROMO-PYRIDIN-2-OL

2-Pyridinol,3-amino-5-bromo- (6CI)

3-Amino-5-bromo-2(1H)-pyridinone

3-AMino-5-broMopyridin-2(1H)-one

3-Amino-5-bromo-1H-pyridin-2-one

3-Amino-5-bromo-2-hydroxypyridine≥ 97% (HPLC)

3-Amino-5-bromo-2-pyridinol

3-Amino-5-bromo-2-hydroxypyridine 98%

5-bromo-2-hydroxy-3-aminopyridine

3-AMINO-5-BROMO-PYRIDIN-2-OL ISO 9001：2015 REACH

3-Amino-5-bromo-2-hydroxypyrid

3-amino-2-hydro-5-bromo pyridine

98786-86-8

C5H5N2OBr

Heterocycle-Pyridine series