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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE

Product Name
PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE
CAS No.
26822-37-7
Chemical Name
PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE
Synonyms
Nsc149999;N-Methyl-4-piperidone methodide;1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE;1,1-Dimethylpiperidin-1-ium-4-one iodide;1,1-DiMethyl-4-oxopiperidin-1-iuM iodide;1,1-Dimethyl-4-oxo-1-piperidinium iodide;PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE;N,N'-Dimethyl-4-oxopiperidine iodium salt, 97%
CBNumber
CB5839261
Molecular Formula
C7H14INO
Formula Weight
255.09663
MOL File
26822-37-7.mol
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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Property

Melting point:
174-179 °C (decomp)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM1007572
Product name
1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE
Purity
95.00%
Packaging
5MG
Price
$496.97
Updated
2021/12/16
Chemenu
Product number
CM179451
Product name
1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity
95%
Packaging
25g
Price
$569
Updated
2021/12/16
Crysdot
Product number
CD11155958
Product name
1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity
95+%
Packaging
25g
Price
$608
Updated
2021/12/16
Alichem
Product number
26822377
Product name
1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Packaging
25g
Price
$620.16
Updated
2021/12/16
Crysdot
Product number
CD11155958
Product name
1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity
95+%
Packaging
1g
Price
$57
Updated
2021/12/16
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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Chemical Properties,Usage,Production

Synthesis

1445-73-4

74-88-4

26822-37-7

Step 1: Preparation of 1,1-dimethyl-4-oxopiperidinium iodide Iodomethane (1.6 mL, 26.5 mmol) was slowly added dropwise to an acetone solution (10 mL) of N-methyl-4-piperidone (2.0 g, 17.6 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 1 hour. The resulting precipitate was collected by filtration and washed with cold acetone to afford 1,1-dimethyl-4-oxopiperidinium iodide as an off-white solid (4.0 g, 88% yield). Product characterization data: 1H NMR (D2O, 400 MHz): δ 3.38 (t, J = 5.8 Hz, 4H), 3.06 (s, 6H), 1.95-2.05 (m, 4H). LCMS (Method D): measured mass (M+ 128.2), retention time (Rt): 1.19 min, % peak area: 95.3% (maximum purity).

References

[1] Journal of Organic Chemistry, 2006, vol. 71, # 22, p. 8602 - 8609
[2] Journal of Organic Chemistry, 2014, vol. 79, # 8, p. 3358 - 3373
[3] Organic Process Research and Development, 2004, vol. 8, # 6, p. 939 - 941
[4] Angewandte Chemie - International Edition, 2008, vol. 47, # 32, p. 5968 - 5972
[5] Journal of the American Chemical Society, 2009, vol. 131, # 1, p. 357 - 367

PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Suppliers

China 21 France 1 India 3 United States 3 Global 28
Shanghai Hobor Chemical Co., Ltd
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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
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Amadis Chemical Company Limited
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MQ (shanghai) Pharmaceuticals Co., Ltd.
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Beijing Minruida Technology Co., Ltd.
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Birdo (Shanghai) Medical Technology Co., Ltd.
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Taizhou Nanfeng Pharmaceutical Research Institute
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Changzhou Kechem Bio-Scientific Co., LTD.
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Fuxin Pharmaceutical
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Bide Pharmatech Ltd.
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26822-37-7, PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDERelated Search:

PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE 1,1,2,3-TETRAMETHYL-4-OXOHEXAHYDROPYRIDINIUM IODIDE 1,1,3-TRIMETHYL-4-OXOPIPERIDINIUM, IODIDE

  • N-Methyl-4-piperidone methodide
  • Nsc149999
  • 1,1-DiMethyl-4-oxopiperidin-1-iuM iodide
  • 1,1-Dimethylpiperidin-1-ium-4-one iodide
  • N,N'-Dimethyl-4-oxopiperidine iodium salt, 97%
  • PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE
  • 1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE
  • 1,1-Dimethyl-4-oxo-1-piperidinium iodide
  • 26822-37-7
  • C7H14INO
  • C7H14NOI
  • C7H15INO