PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE

Product Name: PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE
CAS No.: 26822-37-7
Chemical Name: PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE
Synonyms: Nsc149999;N-Methyl-4-piperidone methodide;1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE;1,1-Dimethylpiperidin-1-ium-4-one iodide;1,1-DiMethyl-4-oxopiperidin-1-iuM iodide;1,1-Dimethyl-4-oxo-1-piperidinium iodide;PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE;N,N'-Dimethyl-4-oxopiperidine iodium salt, 97%
CBNumber: CB5839261
Molecular Formula: C7H14INO
Formula Weight: 255.09663
MOL File: 26822-37-7.mol

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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Property

Melting point:: 174-179 °C (decomp)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM1007572
Product name: 1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE
Purity: 95.00%
Packaging: 5MG
Price: $496.97
Updated: 2021/12/16

Chemenu

Product number: CM179451
Product name: 1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity: 95%
Packaging: 25g
Price: $569
Updated: 2021/12/16

Crysdot

Product number: CD11155958
Product name: 1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity: 95+%
Packaging: 25g
Price: $608
Updated: 2021/12/16

Alichem

Product number: 26822377
Product name: 1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Packaging: 25g
Price: $620.16
Updated: 2021/12/16

Crysdot

Product number: CD11155958
Product name: 1,1-Dimethyl-4-oxopiperidin-1-iumiodide
Purity: 95+%
Packaging: 1g
Price: $57
Updated: 2021/12/16

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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Chemical Properties,Usage,Production

Synthesis

1445-73-4

74-88-4

26822-37-7

Step 1: Preparation of 1,1-dimethyl-4-oxopiperidinium iodide Iodomethane (1.6 mL, 26.5 mmol) was slowly added dropwise to an acetone solution (10 mL) of N-methyl-4-piperidone (2.0 g, 17.6 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 1 hour. The resulting precipitate was collected by filtration and washed with cold acetone to afford 1,1-dimethyl-4-oxopiperidinium iodide as an off-white solid (4.0 g, 88% yield). Product characterization data: 1H NMR (D2O, 400 MHz): δ 3.38 (t, J = 5.8 Hz, 4H), 3.06 (s, 6H), 1.95-2.05 (m, 4H). LCMS (Method D): measured mass (M+ 128.2), retention time (Rt): 1.19 min, % peak area: 95.3% (maximum purity).

References

[1] Journal of Organic Chemistry, 2006, vol. 71, # 22, p. 8602 - 8609
[2] Journal of Organic Chemistry, 2014, vol. 79, # 8, p. 3358 - 3373
[3] Organic Process Research and Development, 2004, vol. 8, # 6, p. 939 - 941
[4] Angewandte Chemie - International Edition, 2008, vol. 47, # 32, p. 5968 - 5972
[5] Journal of the American Chemical Society, 2009, vol. 131, # 1, p. 357 - 367

PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE Suppliers

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26822-37-7, PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDERelated Search:

PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE 1,1,2,3-TETRAMETHYL-4-OXOHEXAHYDROPYRIDINIUM IODIDE 1,1,3-TRIMETHYL-4-OXOPIPERIDINIUM, IODIDE

N-Methyl-4-piperidone methodide

Nsc149999

1,1-DiMethyl-4-oxopiperidin-1-iuM iodide

1,1-Dimethylpiperidin-1-ium-4-one iodide

N,N'-Dimethyl-4-oxopiperidine iodium salt, 97%

PIPERIDINIUM, 1,1-DIMETHYL-4-OXO-, IODIDE

1,1-DIMETHYL-4-OXO-PIPERIDINIUM IODIDE

1,1-Dimethyl-4-oxo-1-piperidinium iodide

26822-37-7

C7H14INO

C7H14NOI

C7H15INO