ChemicalBook > CAS DataBase List > 2-Bromo-6-fluoronaphthalene
2-Bromo-6-fluoronaphthalene
- Product Name
- 2-Bromo-6-fluoronaphthalene
- CAS No.
- 324-41-4
- Chemical Name
- 2-Bromo-6-fluoronaphthalene
- Synonyms
- EOS-60456;2-Bromo-6-fluorophthalene;2-fluoro-6-bromonaphthalene;2-Bromo-6-fluoronaphthalene;Naphthalene, 2-bromo-6-fluoro-;5.2-Bromo-6-fluoro-naphthalene
- CBNumber
- CB5966521
- Molecular Formula
- C10H6BrF
- Formula Weight
- 225.06
- MOL File
- 324-41-4.mol
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2-Bromo-6-fluoronaphthalene Property
- Melting point:
- 64.0 to 68.0 °C
- Boiling point:
- 140°C/9mmHg(lit.)
- Density
- 1.563
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Light yellow to Light orange
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Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2903998090
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N-Bromosuccinimide Price
TCI Chemical
- Product number
- B5229
- Product name
- 2-Bromo-6-fluoronaphthalene
- Purity
- >97.0%(GC)
- Packaging
- 1g
- Price
- $165
- Updated
- 2025/07/31
TRC
- Product number
- B692703
- Product name
- 2-Bromo-6-fluoronaphthalene
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
TRC
- Product number
- B692703
- Product name
- 2-Bromo-6-fluoronaphthalene
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
Oakwood
- Product number
- 067631
- Product name
- 2-Bromo-6-fluoronaphthalene
- Purity
- 97%
- Packaging
- 250mg
- Price
- $20
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 1600-B-26
- Product name
- 2-Bromo-6-fluoronaphthalene
- Purity
- 96%
- Packaging
- 1g
- Price
- $40
- Updated
- 2021/12/16
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2-Bromo-6-fluoronaphthalene Chemical Properties,Usage,Production
Chemical Properties
white solid
Synthesis
87700-58-1
324-41-4
Step 2: In a dry reaction flask, 6-fluoro-2-naphthalenecarbonyl chloride (472 mg, 2.097 mmol) with AIBN (173 mg, 1.052 mmol) was dissolved in CBrCl3 (10 mL). The above solution was slowly added dropwise to a mixture containing 2-mercaptopyridine N-oxide sodium salt (981 mg, 6.58 mmol) and CBrCl3 (10 mL) under nitrogen protection at 100 °C over 30 min. After the dropwise addition, the reaction mixture was continued to be stirred at 100 °C for 15 min and subsequently cooled to room temperature. The reaction solution was quenched with deionized water (H2O) and extracted with ethyl acetate (EtOAc, 2 × 10 mL). The organic phases were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The crude product was purified by a Biotage fast chromatography system (elution gradient: 0-5% EtOAc/heptane; column: SNAP25) to afford the target compound 2-bromo-6-fluoronaphthalene (6b, 472 mg, 40% yield) as a white solid.1H NMR (400 MHz, MeOD) δ ppm: 7.34 (td, J = 8.84, 2.59 Hz, 1H), 7.49-7.57 (m, 1H), 7.60 (ddd, J = 8.78, 1.96, 0.69 Hz, 1H), 7.77 (d, J = 8.84 Hz, 1H), 7.87 (dd, J = 9.09, 5.56 Hz, 1H), 8.09 (d, J = 1.58 Hz, 1H).
References
[1] Patent: WO2011/61168, 2011, A1. Location in patent: Page/Page column 53
2-Bromo-6-fluoronaphthalene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Bromo-6-fluoronaphthalene manufacturers
Career Henan Chemical Co
- Product
- 2-Bromo-6-fluoronaphthalene 324-41-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-18
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