ChemicalBook > CAS DataBase List > Fenazox

Fenazox

Product Name
Fenazox
CAS No.
61618-27-7
Chemical Name
Fenazox
Synonyms
Fenazox;Amfenac;NSC 309467;AMFENAC SODIUM;acetate hydrate;Fenazox USP/EP/BP;Amfenac Sodium Salt;Sodium aminophenate;Amfenac sodium hydrate;Amfenac-d5 Sodium Salt
CBNumber
CB5969698
Molecular Formula
C15H16NNaO4
Formula Weight
297.29
MOL File
61618-27-7.mol
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Fenazox Property

Melting point:
242-244°C
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
solubility 
Methanol (Slightly), Water (Slightly)
form 
Solid
color 
Yellow
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A576500
Product name
AmfenacSodiumHydrate
Packaging
50mg
Price
$80
Updated
2021/12/16
TRC
Product number
A576500
Product name
AmfenacSodiumHydrate
Packaging
100mg
Price
$115
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA17348
Product name
Amfenac sodium salt hydrate
Packaging
2g
Price
$120
Updated
2021/12/16
Matrix Scientific
Product number
094811
Product name
Sodium 2-(2-amino-3-benzoylphenyl)acetate hydrate
Purity
95+%
Packaging
5g
Price
$147
Updated
2021/12/16
AK Scientific
Product number
J52642
Product name
Amfenacsodiummonohydrate
Packaging
5g
Price
$150
Updated
2021/12/16
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Fenazox Chemical Properties,Usage,Production

Description

Amfenac sodium is a non-steroidal antiinflammatory agent structurally related to ketoprofen,suprofen(10) and tiaprofenic acid.It is reported to be effective in the short term treatment of rheumatoidarthritis,osteoarthritis and pain associated with minor surgical procedures.

Chemical Properties

Yellow Solid

Originator

A.H. Robins (USA)

Uses

Amfenac is an antibacterial agent

Uses

Fenazox is used in the synthetic preparation of amides via reductive amidation of esters, which is used in the synthesis of bio-active molecules and natural products.

Definition

ChEBI: A hydrate that is the monohydrate of the sodium salt of amfenac.

Manufacturing Process

7-Benzoylindolin-2-one:
Method A. A mixture of 2.5 g (0.0077 mole) of ethyl 2-acetamido-3- benzoylphenylacetate in 50 ml of 3 N hydrochloric acid was refluxed for one hour. The reaction mixture was filtered and the filtrate was poured into a mixture of ice and water. The precipitate was collected and recrystallized from acetone; yield of 7-benzoylindolin-2-one 1 g (55%); melting point 154°C.
Method B. A solution of 1.3 g (0.0044 mole) of 2-acetamido-3- benzoylphenylacetic acid in 15 ml of 3 N hydrochloric acid and 15 ml of acetic acid was refluxed for three hours. The cooled solution was poured into ice water and the 7-benzoylindolin-2-one which precipitated was collected and dried.
2-Amino-3-benzoylphenylacetic acid:
A mixture of 1.0 g (0.004 mole) of 7-benzoylindolin-2-one was added to 30 ml of 3 N sodium hydroxide and the basic solution was refluxed for 45 min under nitrogen. The mixture was filtered and the filtrate was neutralized with glacial acetic acid. The precipitate was filtered off, washed with water and dried. The 2-amino-3-benzoylbenzeneacetic acid melted at 122°C (dec.). The yield was 0.8 g (72%).

brand name

FENAZOX

Therapeutic Function

Antiinflammatory

General Description

Amfenac (Fenazox), its amide prodrug, nepafenac (Nevanac),and the related analog, bromofenac, are amphoteric becauseof the presence of an additional aromatic amine group.They are less likely to be absorbed into the general circulation.They are approved for use as topical ocular anti-inflammatoryagents for the treatment of postoperative ocular pain,inflammation, and posterior segment edema. The only observedside effects of these drugs are all related to tissuesaround the eye including abnormal ocular sensation, eye rednessand irritation, burning and stinging, and conjunctival orcornea edema.

Synthesis

The reaction of 1-aminoindolin- 2-one with phenylacetone in presence of acetic acid in refluxing ethanol gives 1-(α- methylphenethylidieneimino)indolin-2-one, which by reaction with refluxing ethanolic hydrogen chloride affords ethyl α-(2-methyl- 3-phenylindol-7-yl)acetate. The ozonolysis of this intermediate in acetic acid yields ethyl 2- acetamido-3-benzoylphenyl acetate, which is cyclized by refluxing with HCl in acetic acid to give 7-benzoylindolin-2-one. Alternatively, the hydrolysis of the ester ethyl α-(2-methyl-3- phenylindol-7-yl)acetate with KOH in refluxing water affords the corresponding acid, which can be ozonolyzed as before yielding 2-acetamido- 3-benzoylphenylacetic acid. This acid can be cyclized to 7-benzoyl-1,3-dihydro-indol-2-one by refluxing with HCl in acetic acid as before .

Fenazox Preparation Products And Raw materials

Raw materials

Preparation Products

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Fenazox Suppliers

Service Chemical Inc.
Tel
--
Fax
--
Email
sales@chemos-group.com
Country
Germany
ProdList
6350
Advantage
71
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View Lastest Price from Fenazox manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
Amfenac sodium/Fenazox 61618-27-7
Price
US $0.00-0.00/Kg/Drum
Min. Order
1KG
Purity
98.5%min
Supply Ability
500kg
Release date
2021-09-11
Zhuozhou Wenxi import and Export Co., Ltd
Product
Fenazox 61618-27-7
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
Fenazox 61618-27-7
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-08

61618-27-7, FenazoxRelated Search:


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  • AMFENAC SODIUM MONOHYDRATE
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  • 2-Amino-3-benzoylbenzeneacetic acid, monosodium salt, monohydrate
  • Amfenac sodium salt monohydrate
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  • Benzeneacetic acid, 2-amino-3-benzoyl-, sodium salt, monohydrate
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  • Sodium 2-(2-amino-3-benzoylphenyl)acetate hydrate
  • 2-AMino-3-benzoylbenzeneacetic Acid SodiuM Salt Hydrate
  • NSC 309467
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  • Amfenac sodium hydrate, >=99%
  • AMfenac sodiuM(Fenazox)
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  • acetate hydrate
  • Sodium 2-(2-amino-3-benzoylphenyl)
  • Benzeneacetic acid, 2-amino-3-benzoyl-, monosodium salt,monohydrate
  • Fenazox USP/EP/BP
  • Amfenac-d5 Sodium Salt
  • Amfenac Sodium SaltQ: What is Amfenac Sodium Salt Q: What is the CAS Number of Amfenac Sodium Salt Q: What is the storage condition of Amfenac Sodium Salt
  • Sodium aminophenate
  • 61618-27-7
  • 6168-27-7
  • C15H14NNaO4
  • C15H12NNaO3H2O
  • C15H12NO3H2ONa
  • C15H12NO3Na
  • C15H12NO3NaH2O
  • Amines
  • Aromatics
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