ChemicalBook > CAS DataBase List > 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE

Product Name
2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
CAS No.
28004-63-9
Chemical Name
2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
Synonyms
AKOS B014677;TIMTEC-BB SBB007063;ART-CHEM-BB B014677;IFLAB-BB F1386-0069;CHEMBRDG-BB 5313490;5-(2,4-Dichlorophenyl);5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE;2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE;1,3,4-Thiadiazol-2-aMine, 5-(2,4-dichlorophenyl)-;5-(2,4-DICHLOROPHENYL)-[1,3,4]THIADIAZOL-2-YL-AMINE
CBNumber
CB6101543
Molecular Formula
C8H5Cl2N3S
Formula Weight
246.12
MOL File
28004-63-9.mol
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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Property

Melting point:
240-242℃ (ethanol water )
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
D435313
Product name
5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
500mg
Price
$130
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD113695
Product name
5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
500mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD113695
Product name
5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
1g
Price
$128
Updated
2021/12/16
Matrix Scientific
Product number
007785
Product name
5-(2,4-Dichlorophenyl)-[1,3,4]thiadiazol-2-yl-amine
Packaging
500mg
Price
$168
Updated
2021/12/16
AK Scientific
Product number
2698AB
Product name
5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
1g
Price
$172
Updated
2021/12/16
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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Chemical Properties,Usage,Production

Synthesis

6957-92-2

28004-63-9

General method: In step 2, the Schiff base intermediate was dissolved in 1,4-dioxane, iodine and potassium carbonate were added, and the cyclization reaction was carried out at 80 °C. The reaction mixture was refluxed for 4 hours and the progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by the addition of 5% sodium thiosulfate solution (20 ml). The target organic compounds in the reaction mixture were extracted with ethyl acetate. The organic phase was separated and collected and the solvent was removed by evaporation to give a solid product of 2-amino-5-(2,4-dichlorophenyl)-1,3,4-thiadiazole.

References

[1] Monatshefte fur Chemie, 2013, vol. 144, # 5, p. 681 - 686
[2] Bioorganic Chemistry, 2018, vol. 78, p. 201 - 209
[3] Archiv der Pharmazie, 2015, vol. 348, # 1, p. 10 - 22
[4] Turkish Journal of Chemistry, 2018, vol. 42, # 3, p. 839 - 858
[5] Indian Journal of Chemistry, 1970, vol. 8, p. 509 - 513

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Suppliers

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28004-63-9, 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLERelated Search:

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE 2-AMINO-5-(2-CHLOROPHENYL)-1,3,4-THIADIAZOLE 2-AMINO-5-PHENYL-1 3 4-THIADIAZOLE 96 2-AMINO-5-(4-CHLOROPHENYL)-1 3 4- 5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-YLAMINE HYDROCHLORIDE

  • AKOS B014677
  • 5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE
  • 5-(2,4-DICHLOROPHENYL)-[1,3,4]THIADIAZOL-2-YL-AMINE
  • TIMTEC-BB SBB007063
  • 5-(2,4-dichlorophenyl)-1,3,4-thiadiazol-2-amine(SALTDATA: FREE)
  • 1,3,4-Thiadiazol-2-aMine, 5-(2,4-dichlorophenyl)-
  • 5-(2,4-Dichlorophenyl)
  • CHEMBRDG-BB 5313490
  • IFLAB-BB F1386-0069
  • ART-CHEM-BB B014677
  • 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
  • 28004-63-9